1,127 research outputs found
A process for developing and validating performance assessment rubrics for laboratory techniques
PROBLEM
Achieving competence in technical skills is a key learning objective in the laboratory programs of our institution’s Pharmaceutical Science course. However, their assessment is often achieved through indirect outcome indicators since performance assessment through direct observation is time-consuming and there is a lack of validated, efficient and scalable methods.
PLAN
We report on our approach towards the development, validation and optimisation of a set of rubrics for the formative and summative assessment of common chemistry laboratory techniques. Efficiency and user-friendliness are key criteria in the rubric development.
Drawing on recent work by Seery et al. (2017) and Chen et al. (2013), we propose a four-stage process:
Rubric design based on practitioner input, literature sources and lab observations
Testing involving student self-assessment, peer evaluation and instructor assessment
Optimisation and validation based on assessment data, student and instructor feedback
Developing supporting procedures (e.g., instructor training).
ACTION AND EVALUATION
We have started implementation in two synthetic chemistry subjects, initially targeting rubrics for four techniques (reflux setup, thin-layer chromatography, vacuum filtration and recrystallisation).
Rubric evaluation will involve both quantitative (assessment data) and qualitative methods (surveys/focus groups with instructors and students, human ethics application in progress).
REFERENCES
Chen, H. J., She, J. L., Chou, C. C., Tsai, Y. M., & Chiu, M. H. (2013). Development and application of a scoring rubric for evaluating students’ experimental skills in organic chemistry: An instructional guide for teaching assistants. Journal of Chemical Education, 90(10), 1296–1302. https://doi.org/10.1021/ed101111g
Seery, M. K., Agustian, H. Y., Doidge, E. D., Kucharski, M. M., O’Connor, H. M., & Price, A. (2017). Developing laboratory skills by incorporating peer-review and digital badges. Chemistry Education Research and Practice, 18(3), 403–419. https://doi.org/10.1039/C7RP00003
System-size and centrality dependence of charged kaon and pion production in nucleus-nucleus collisions at 40A GeV and158A GeV beam energy
Measurements of charged pion and kaon production are presented in centrality
selected Pb+Pb collisions at 40A GeV and 158A GeV beam energy as well as in
semi-central C+C and Si+Si interactions at 40A GeV. Transverse mass spectra,
rapidity spectra and total yields are determined as a function of centrality.
The system-size and centrality dependence of relative strangeness production in
nucleus-nucleus collisions at 40A GeV and 158A GeV beam energy are derived from
the data presented here and published data for C+C and Si+Si collisions at 158A
GeV beam energy. At both energies a steep increase with centrality is observed
for small systems followed by a weak rise or even saturation for higher
centralities. This behavior is compared to calculations using transport models
(UrQMD and HSD), a percolation model and the core-corona approach.Comment: 32 pages, 14 figures, 4 tables, typo table II correcte
<Abstract of Published Report>Crystallization and Preliminary X-ray Diffraction Analysis of Monkey Dimeric Dihydrodiol Dehydrogenase.
Energy dependence of kaon-to-proton ratio fluctuations in central Pb+Pb collisions from = 6.3 to 17.3 GeV
Kaons and protons carry large parts of two conserved quantities, strangeness
and baryon number. It is argued that their correlation and thus also
fluctuations are sensitive to conditions prevailing at the anticipated
parton-hadron phase boundary. Fluctuations of the and
ratios have been measured for the first time by NA49 in central Pb+Pb
collisions at 5 SPS energies between = 6.3 GeV and 17.3 GeV.
Both ratios exhibit a change of sign in , a measure of
non-statistical fluctuations, around = 8 GeV. Below this
energy, is positive, indicating higher fluctuation
compared to a mixed event background sample, while for higher energies,
is negative, indicating correlated emission of kaons
and protons. The results are compared to UrQMD calculations which which give a
good description at the higher SPS energies, but fail to reproduce the
transition to positive values.Comment: 5 pages, 4 figure
Phase-space dependence of particle-ratio fluctuations in Pb+Pb collisions from 20A to 158A GeV beam energy
A novel approach, the identity method, was used for particle identification
and the study of fluctuations of particle yield ratios in Pb+Pb collisions at
the CERN Super Proton Synchrotron (SPS). This procedure allows to unfold the
moments of the unknown multiplicity distributions of protons (p), kaons (K),
pions () and electrons (e). Using these moments the excitation function of
the fluctuation measure [A,B] was measured, with A and
B denoting different particle types. The obtained energy dependence of
agrees with previously published NA49 results on the related
measure . Moreover, was found to depend
on the phase space coverage for [K,p] and [K,] pairs. This feature most
likely explains the reported differences between measurements of NA49 and those
of STAR in central Au+Au collisions
Antideuteron and deuteron production in mid-central Pb+Pb collisions at 158 GeV
Production of deuterons and antideuterons was studied by the NA49 experiment
in the 23.5% most central Pb+Pb collisions at the top SPS energy of
=17.3 GeV. Invariant yields for and were measured
as a function of centrality in the center-of-mass rapidity range .
Results for together with previously published
measurements are discussed in the context of the coalescence model. The
coalescence parameters were deduced as a function of transverse momentum
and collision centrality.Comment: 9 figure
Production of deuterium, tritium, and He in central Pb+Pb collisions at 20A, 30A, 40A, 80A, and 158A GeV at the CERN SPS
Production of , , and He nuclei in central Pb+Pb interactions was
studied at five collision energies ( 6.3, 7.6, 8.8, 12.3, and
17.3 GeV) with the NA49 detector at the CERN SPS. Transverse momentum spectra,
rapidity distributions, and particle ratios were measured. Yields are compared
to predictions of statistical models. Phase-space distributions of light nuclei
are discussed and compared to those of protons in the context of a coalescence
approach. The coalescence parameters and , as well as coalescence
radii for and He were determined as a function of transverse mass at
all energies.Comment: 22 pages, 29 figures, 8 tables, for submission to Phys. Rev.
Measurement of event-by-event transverse momentum and multiplicity fluctuations using strongly intensive measures and in nucleus-nucleus collisions at the CERN Super Proton Synchrotron
Results from the NA49 experiment at the CERN SPS are presented on
event-by-event transverse momentum and multiplicity fluctuations of charged
particles, produced at forward rapidities in central Pb+Pb interactions at beam
momenta 20, 30, 40, 80, and 158 GeV/c, as well as in systems of
different size (, C+C, Si+Si, and Pb+Pb) at 158 GeV/c. This publication
extends the previous NA49 measurements of the strongly intensive measure
by a study of the recently proposed strongly intensive measures of
fluctuations and . In the explored kinematic
region transverse momentum and multiplicity fluctuations show no significant
energy dependence in the SPS energy range. However, a remarkable system size
dependence is observed for both and , with the
largest values measured in peripheral Pb+Pb interactions. The results are
compared with NA61/SHINE measurements in collisions, as well as with
predictions of the UrQMD and EPOS models.Comment: 12 pages, 14 figures, to be submitted to PR
Proton -- Lambda Correlations in Central Pb+Pb Collisions at sqrt(s_{NN}) = 17.3 GeV
The momentum correlation between protons and lambda particles emitted from
central Pb+Pb collisions at sqrt(s_{NN}) = 17.3 GeV was studied by the NA49
experiment at the CERN SPS. A clear enhancement is observed for small relative
momenta (q_{inv} < 0.2 GeV). By fitting a theoretical model, which uses the
strong interaction between the proton and the lambda in a given pair, to the
measured data a value for the effective source size is deduced. Assuming a
static Gaussian source distribution we derive an effective radius parameter of
R_G = 3.02 \pm 0.20$(stat.)^{+0.44}_{-0.16}(syst.) fm.Comment: 14 pages, 9 figures, submitted to Phys. Rev.
Centrality dependence of proton and antiproton spectra in Pb+Pb collisions at 40A GeV and 158A GeV measured at the CERN SPS
The yields of (anti-)protons were measured by the NA49 Collaboration in
centrality selected Pb+Pb collisions at 40A GeV and 158A GeV. Particle
identification was obtained in the laboratory momentum range from 5 to 63 GeV/c
by the measurement of the energy loss dE/dx in the TPC detector gas. The
corresponding rapidity coverage extends 1.6 units from mid-rapidity into the
forward hemisphere. Transverse mass spectra, the rapidity dependences of the
average transverse mass, and rapidity density distributions were studied as a
function of collision centrality. The values of the average transverse mass as
well as the midrapidity yields of protons when normalized to the number of
wounded nucleons show only modest centrality dependences. In contrast, the
shape of the rapidity distribution changes significantly with collision
centrality, especially at 40A GeV. The experimental results are compared to
calculations of the HSD and UrQMD transport models.Comment: 25 pages, 12 figures, submitted to PR
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