Effectiveness of Soya Orotein Consumption on the Menopausal Symptoms among Women in Samayanallur at Madurai

Title : Effectiveness of soya protein consumption on the menopausal symptoms among women in Samayanallur at Madurai. Objective: To assess the level of menopausal symptoms among women in control and experimental group in Samayanallur at Madurai, to evaluate the effectiveness of soya protein consumption on menopausal symptoms among women in Samayanallur at Madurai, to find the association between menopausal symptoms with selected demographic variables in control and experimental group in Samayanallur at Madurai. Hypotheses : There is a significant difference in the level of menopausal symptoms before and after soya protein consumption among women in control and experimental group, there is a significant association between level of menopausal symptoms and selected demographic variable among women in control and experimental group. Conceptual Framework: It was based on Kenny’s outcome based theory. Methodology : Quasiexperimental – Non equivalent control group design. Menopausal women were selected by purposive sampling technique. This study was conducted in Samayanallur at Madurai. A total of 60 women were included in the study. 60grams soya bean given daily for 4 weeks. Results: Result showed that level of Menopausal symptoms among women in both groups. Experimental group post test mean was 10.6 standard deviation 3.70, Control group post test mean was 17.07 standard deviation 3.39. Experimental group post test mean was less than control group post test mean. ‘t’ value was 7.05, ‘p’ value was 0.000. Conclusion: Menopausal women who consuming soya protein 60grams daily had a statistically significant in reducing the level of menopausal symptoms

1,5-Dimethyl-3-oxo-2-phenyl-2,3-di­hy­dro-1H-pyrazol-4-aminium 2-hydroxy­benzoate

In the title salt, C11H14N3O+·C7H5O3 −, the phenyl ring of the cation is oriented at an angle of 67.0 (1)° with respect to the five-membered pyrazolone ring. The carboxyl­ate plane of the anion is twisted out from the plane of the aromatic ring at an angle of 13.7 (3)°. In the crystal, the cations form hydrogen-bonded dimers with an R 2 2(10) ring motif. The salicylate anion has an intra­molecular O—H⋯O hydrogen bond

Diethyl 1-benzyl-2,2-dioxo-4-phenyl-3,4,6,7,8,8a-hexa­hydro-1H-pyrrolo­[2,1-c][1,4]thia­zine-1,3-dicarboxyl­ate

In the title compound, C26H31NO6S, the five-membered pyrrolidine ring adopts an envelope conformation and the six-membered thia­zine ring is in a distorted chair conformation. The crystal packing is stabilized through an inter­molecular C—H⋯O inter­action, generating inversion-related R 2 2(10) ring motifs

Synthesis, spectroscopic and structural characterisation of two p-nitrobenzamide compounds: experimental and DFT study

Kazak, Canan/0000-0003-2475-8775; ARSLAN, N. Burcu/0000-0002-1880-1047WOS: 000349787900007The title molecules, N-(1,5-dimethyl-3-oxo-2-phenyl-1H-3-(2H)-pyrazolyl)4-nitrobenzamide (C18H16N4O4 center dot H2O) (I) and 2,2-dimethyl-3-(4-nitrobenzoyl)-5-(phenylamino)-2,3-dihydro-1,3,4-thiyadiazole (C17H16N4O3S) (II), were prepared and characterised by H-1 NMR, C-13 NMR, infrared spectroscopy (IR) and structural X-ray diffraction (XRD) techniques. The molecular geometries, vibrational frequencies of the title compounds in the ground state have been calculated by using the density functional theory (DFT) method with 6-31G(d) basis set, and compared with the experimental data. The calculated results showed that the optimised geometries from the DFT method agree with the X-ray structures well for both compounds. Theoretical calculations of harmonic vibration frequencies are in good agreement with experimental results. To determine conformational flexibility, the molecular energy profiles of the title compounds were obtained. Besides, molecular electrostatic potential (MEP), frontier molecular orbitals (FMO) analysis and thermodynamic properties of the title compounds were investigated by theoretical calculations