The Mars Sample Return Lab(s) - Lessons from the Past and Implications for the Future

It has been widely understood for many years that an essential component of a Mars Sample Return mission is a Sample Receiving Facility (SRF). The purpose of such a facility would be to take delivery of the flight hardware that lands on Earth, open the spacecraft and extract the sample container and samples, and conduct an agreed upon test protocol, while ensuring strict containment and contamination control of the samples while in the SRF. Any samples that are found to be non-hazardous (or are rendered non-hazardous by sterilization) would then be transferred to long-term curation. Although the general concept of an SRF is relatively straightforward, there has been considerable discussion about implementation planning

Astromaterials Acquisition and Curation Office (KT) Overview

The Astromaterials Acquisition and Curation Office has the unique responsibility to curate NASA's extraterrestrial samples - from past and forthcoming missions - into the indefinite future. Currently, curation includes documentation, preservation, physical security, preparation, and distribution of samples from the Moon, asteroids, comets, the solar wind, and the planet Mars. Each of these sample sets has a unique history and comes from a unique environment. The curation laboratories and procedures developed over 40 years have proven both necessary and sufficient to serve the evolving needs of a worldwide research community. A new generation of sample return missions to destinations across the solar system is being planned and proposed. The curators are developing the tools and techniques to meet the challenges of these new samples. Extraterrestrial samples pose unique curation requirements. These samples were formed and exist under conditions strikingly different from those on the Earth's surface. Terrestrial contamination would destroy much of the scientific significance of extraterrestrial materials. To preserve the research value of these precious samples, contamination must be minimized, understood, and documented. In addition, the samples must be preserved - as far as possible - from physical and chemical alteration. The elaborate curation facilities at JSC were designed and constructed, and have been operated for many years, to keep sample contamination and alteration to a minimum. Currently, JSC curates seven collections of extraterrestrial samples: (a)) Lunar rocks and soils collected by the Apollo astronauts, (b) Meteorites collected on dedicated expeditions to Antarctica, (c) Cosmic dust collected by high-altitude NASA aircraft,t (d) Solar wind atoms collected by the Genesis spacecraft, (e) Comet particles collected by the Stardust spacecraft, (f) Interstellar dust particles collected by the Stardust spacecraft, and (g) Asteroid soil particles collected by the Japan Aerospace Exploration Agency (JAXA) Hayabusa spacecraft Each of these sample sets has a unique history and comes from a unique environment. We have developed specialized laboratories and practices over many years to preserve and protect the samples, not only for current research but for studies that may be carried out in the indefinite future

Gale Crater - Why are We There and What do We Hope to Learn?

The Mars Science Laboratory Rover Curiosity is commencing a two-year investigation of Gale crater and Mt. Sharp, the craters prominent central mound. Gale is a 155 km, late Noachian/early Hesperian impact crater located near the dichotomy boundary separating the southern highlands from the northern plains. The central mound is composed of layered sedimentary rock, with upper and lower mound units separated by a prominent erosional unconformity. The lower mound is of particular interest, as it contains secondary minerals indicative of a striking shift from water-rich to water-poor conditions on early Mars. A key unknown in the history of Gale is the relationship between the sedimentary units in the mound and sedimentary sequences in the surrounding region. We employed orbital remote sensing data to determine if areas within a 1,000 km radius of Gale match the characteristics of sedimentary units in Mt. Sharp. Regions of interest were defined based on: the mound s inferred age, altitude range, and THEMIS nighttime brightness (a proxy for thermal inertia). Using orbital CTX, MOC and HiRISE images we examined all areas within our regions of interest for analogous geomorphic units in the same altitude ranges as the corresponding units in Mt. Sharp. The results are consistent with the hypothesis that sedimentary units in both the upper and lower sections of the Gale mound are related to nearby regional units located along the dichotomy boundary. This relationship supports an inferred geologic history that includes several episodes of widespread sedimentary deposition and erosion in the martian mid-latitudes. In this model Mt. Sharp is the remnant of regional sedimentary deposits that partially or completely filled the crater, became lithified, and were subsequently deeply eroded. Key questions that will be addressed by Curiosity include the compositions of the sediments, the modes of deposition, the mechanisms of lithification, and the nature of the erosion

Exposed Ice in the Northern Mid-Latitudes of Mars

Ice-Rich Layer: Polygonal features with dimensions of approximately 100 meters, bounded by cracks, are commonly observed on the martian northern plains. These features are generally attributed to thermal cracking of ice-rich sediments, in direct analogy to polygons in terrestrial polar regions. We mapped polygons in the northern mid-latitudes (30 to 65 N) using MOC and HiRISE images. Polygons are scattered across the northern plains, with a particular concentration in western Utopia Planitia. This region largely overlaps the Late Amazonian Astapus Colles unit, characterized by polygonal terrain and nested pits consistent with periglacial and thermokarst origins. Bright and Dark Polygonal Cracks: An examination of all MOC images (1997 through 2003) covering the study area demonstrated that, at latitudes of 55 to 65 N, most of the imaged polygons show bright bounding cracks. We interpret these bright cracks as exposed ice. Between 40 and 55 N, most of the imaged polygons show dark bounding cracks. These are interpreted as polygons from which the exposed ice has been removed by sublimation. The long-term stability limit for exposed ice, even in deep cracks, apparently lies near 55 N. Bright and Dark Spots: Many HiRISE and MOC frames showing polygons in the northern plains also show small numbers of bright and dark spots, particularly in western Utopia Planitia. Many of the spots are closely associated with collapse features suggestive of thermokarst. The spots range from tens to approximately 100 meters in diameter. The bright spots are interpreted as exposed ice, due to their prevalence on terrain mapped as ice rich. The dark spots are interpreted as former bright spots, which have darkened as the exposed ice is lost by sublimation. The bright spots may be the martian equivalents of pingos, ice-cored mounds found in periglacial regions on Earth. Terrestrial pingos from which the ice core has melted often collapse to form depressions similar to the martian dark spots. Future Observations: The SHARAD radar should be able to confirm the presence and measure the depth of the interpreted ice-rich layer that forms the Astapus Colles unit. If this layer is confirmed it will strengthen the interpretation of bright polygon cracks and bright spots as exposed ice. HiRISE images of the northern plains are showing unprecedented details of the polygonal cracks. Future HiRISE images that include bright spots, compared to MOC images taken years earlier, will illustrate the temporal stability of the spots. The CRISM spectrometer, with multiple spectral bands and a spatial resolution around 20 meters, should allow mineralogical identification of the material exposed in the polygonal bounding cracks and in the bright spots

MEPAG Recommendations for a 2018 Mars Sample Return Caching Lander - Sample Types, Number, and Sizes

The return to Earth of geological and atmospheric samples from the surface of Mars is among the highest priority objectives of planetary science. The MEPAG Mars Sample Return (MSR) End-to-End International Science Analysis Group (MEPAG E2E-iSAG) was chartered to propose scientific objectives and priorities for returned sample science, and to map out the implications of these priorities, including for the proposed joint ESA-NASA 2018 mission that would be tasked with the crucial job of collecting and caching the samples. The E2E-iSAG identified four overarching scientific aims that relate to understanding: (A) the potential for life and its pre-biotic context, (B) the geologic processes that have affected the martian surface, (C) planetary evolution of Mars and its atmosphere, (D) potential for future human exploration. The types of samples deemed most likely to achieve the science objectives are, in priority order: (1A). Subaqueous or hydrothermal sediments (1B). Hydrothermally altered rocks or low temperature fluid-altered rocks (equal priority) (2). Unaltered igneous rocks (3). Regolith, including airfall dust (4). Present-day atmosphere and samples of sedimentary-igneous rocks containing ancient trapped atmosphere Collection of geologically well-characterized sample suites would add considerable value to interpretations of all collected rocks. To achieve this, the total number of rock samples should be about 30-40. In order to evaluate the size of individual samples required to meet the science objectives, the E2E-iSAG reviewed the analytical methods that would likely be applied to the returned samples by preliminary examination teams, for planetary protection (i.e., life detection, biohazard assessment) and, after distribution, by individual investigators. It was concluded that sample size should be sufficient to perform all high-priority analyses in triplicate. In keeping with long-established curatorial practice of extraterrestrial material, at least 40% by mass of each sample should be preserved to support future scientific investigations. Samples of 15-16 grams are considered optimal. The total mass of returned rocks, soils, blanks and standards should be approximately 500 grams. Atmospheric gas samples should be the equivalent of 50 cubic cm at 20 times Mars ambient atmospheric pressure

Taurus Littrow Pyroclastic Deposit-An Optimum Feedstock for Lunar Oxygen

Future human habitation of the Moon will likely require the use of locally derived materials because of the high cost of transportation from Earth. Oxygen, extracted from oxides and silicates, is a potentially abundant lunar resource vital for life support and spacecraft propulsion. The anticipated costs of supplying all oxygen needs for a lunar base from Earth are high enough to warrant serious study of oxygen production from local resources. Over 20 different processes have been proposed for oxygen production on the Moon. Among the simplest and best studied of these processes is the reduction of oxides in lunar minerals and glass using hydrogen gas. Oxygen can be extracted from lunar soils and pyroclastic glass beads by exposing the samples to flowing hydrogen at subsolidus temperatures (approx. 1050 C). Total oxygen yield is directly correlated to the sample's abundance of FeO, but is not correlated to the abundance of any other oxide. Oxygen is extracted predominantly from FeO, with lesser contributions from TiO2 and SiO2. Oxygen yield is independent of soil maturity. All major FeO-bearing phases contribute oxygen, with extraction from ilmenite and glass significantly more efficient than from olivine and pyroxene. This study demonstrates that the optimum location for a lunar resources demonstration mission can be identified, and that the oxygen yield can be predicted, using a combination of high-resolution imaging and thermal-infrared data. A mission to Taurus Littrow will encounter a deposit at least 10 m in depth with few landing hazards, a uniform composition, and a predicted oxygen yield of approximately 3 wt. %, among the highest values on the Moon

Advanced Curation of Current and Future Extraterrestrial Samples

Curation of extraterrestrial samples is the critical interface between sample return missions and the international research community. Curation includes documentation, preservation, preparation, and distribution of samples. The current collections of extraterrestrial samples include: Lunar rocks / soils collected by the Apollo astronauts Meteorites, including samples of asteroids, the Moon, and Mars "Cosmic dust" (asteroid and comet particles) collected by high-altitude aircraft Solar wind atoms collected by the Genesis spacecraft Comet particles collected by the Stardust spacecraft Interstellar dust collected by the Stardust spacecraft Asteroid particles collected by the Hayabusa spacecraft These samples were formed in environments strikingly different from that on Earth. Terrestrial contamination can destroy much of the scientific significance of many extraterrestrial materials. In order to preserve the research value of these precious samples, contamination must be minimized, understood, and documented. In addition the samples must be preserved - as far as possible - from physical and chemical alteration. In 2011 NASA selected the OSIRIS-REx mission, designed to return samples from the primitive asteroid 1999 RQ36 (Bennu). JAXA will sample C-class asteroid 1999 JU3 with the Hayabusa-2 mission. ESA is considering the near-Earth asteroid sample return mission Marco Polo-R. The Decadal Survey listed the first lander in a Mars sample return campaign as its highest priority flagship-class mission, with sample return from the South Pole-Aitken basin and the surface of a comet among additional top priorities. The latest NASA budget proposal includes a mission to capture a 5-10 m asteroid and return it to the vicinity of the Moon as a target for future sampling. Samples, tools, containers, and contamination witness materials from any of these missions carry unique requirements for acquisition and curation. Some of these requirements represent significant advances over methods currently used. New analytical and screening techniques will increase the value of current sample collections. Improved web-based tools will make information on all samples more accessible to researchers and the public. Advanced curation of current and future extraterrestrial samples includes: Contamination Control - inorganic / organic Temperature of preservation - subfreezing / cryogenic Non-destructive preliminary examination - X-ray tomography / XRF mapping / Raman mapping Microscopic samples - handling / sectioning / transport Special samples - unopened lunar cores Informatics - online catalogs / community-based characterization

Taurus Littrow Pyroclastic Deposit: High-Yield Feedstock for Lunar Oxygen

Future human habitation of the Moon will likely require the use of locally derived materials because of the high cost of transportation from Earth. Oxygen, extracted from oxides and silicates, is a potentially abundant lunar resource vital for life support and spacecraft propulsion. The anticipated costs of supplying all oxygen needs for a lunar base from Earth are high enough to warrant serious study of oxygen production from local resources

Sampling Elysium lavas (13 deg N, 203 deg W)

The proposed Pathfinder landing site presents the opportunity to determine chemical and mineralogical compositions of an Elysium lava flow. The flow is part of a geologic unit of planetary significance. The proposed site appears suitable for landing, and lava surfaces should be accessible to the Pathfinder instruments. By analogy to terrestrial flood basalts, any lava analyzed by Pathfinder is likely to be representative of the entire Elysium province