7 research outputs found

    Erosion Corrosion Behavior of Nanostructure Commercial Pure Titanium in Simulated Body Fluid

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    To date, ECAP technique have been successfully employed to produce Ultra-fine/Nanostructure grain materials, but some materials such as hexagonal closed-packed (HCP) alloys are difficult to process by ECAP at room temperature. In this work, Transmission Electron Microscopy (TEM), Vickers hardness test and Torsion test were employed to confirm the attainment of ultrafine/nanostructured grain (UFG/NSG) commercial pure titanium (CP-Ti) Titanium fabricated by ECAP as a sever plastic deformation process. The samples were pressed by ECAP (route BC) up to four passes at elevated temperature (400° C). Finally, the Erosion-Corrosion (E-C) behavior of ultrafine/nanostructured grain (UFG/NSG) Titanium in a simulated body fluid were investigated through weight loss measurement

    Influence of V and Zn in FeCrCuMnTi High-Entropy Alloys on Microstructures and Uniaxial Compaction Behavior Prepared by Mechanical Alloying

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    The densification behavior of FeCrCuMnTi (HEA1), FeCrCuMnTiV (HEA2), and FeCrCuMnTiVZn (HEA3) equiatomic high-entropy alloys (HEAs) was explored using different uniaxial quasi-static controlled compaction (1 mm/min). These HEAs were synthesized by mechanical alloying (MA, speed: 300 rpm, BPR: 10:1, time: 25 h). Various phase formations, structural characteristics (crystallite size, lattice strain, and lattice constant), thermo-dynamic calculations, powder surface morphologies, detailed microstructural evolutions, and chemical compositions were examined using X-ray diffraction, high-resolution scanning electron microscopy, and high-resolution transmission electron microscopy. The XRD results revealed the formation of multiple solid solutions (FCC, BCC, and HCP) due to the variation in entropy, and the presence of high-strength elements (Cr, Ti, and V) in the developed HEA alloys. The synthesized powders were consolidated into bulk green samples with different compaction pressures starting from 25 to 1100 MPa under as-milled and milled under stress recovery conditions (150 °C, 1 h). The incorporation of V in the FeCrCuMnTi HEA resulted in improved densification due to a greater reduction in particle size, and high configurational entropy. Furthermore, the stress-recovered powder samples produced more relative density owing to the elimination of lattice strain. Several linear and non-linear compaction models were applied to predict densification behavior. The non-linear Cooper and Eaton model produced the highest regression coefficients compared to the other models

    Erosion Corrosion Behavior of Nanostructure Commercial Pure Titanium in Simulated Body Fluid

    No full text
    To date, ECAP technique have been successfully employed to produce Ultra-fine/Nanostructure grain materials, but some materials such as hexagonal closed-packed (HCP) alloys are difficult to process by ECAP at room temperature. In this work, Transmission Electron Microscopy (TEM), Vickers hardness test and Torsion test were employed to confirm the attainment of ultrafine/nanostructured grain (UFG/NSG) commercial pure titanium (CP-Ti) Titanium fabricated by ECAP as a sever plastic deformation process. The samples were pressed by ECAP (route BC) up to four passes at elevated temperature (400° C). Finally, the Erosion-Corrosion (E-C) behavior of ultrafine/nanostructured grain (UFG/NSG) Titanium in a simulated body fluid were investigated through weight loss measurement
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