28 research outputs found
Characterisation of structured and functionalisedparticles by small-angle X-ray scattering (SAXS)
A small- and wide-angle X-ray scattering (SWAXS) laboratory camera for simultaneously determining the size, morphology and crystallinity of nanoparticles
Die Röntgenkleinwinkelstreuung als Charakterisierungsmethode bei der Herstellung von Nanopartikeln
Characterization of Primary Particle Size and Crystallinity by Using Small and Wide-angle X-ray Scattering
Influence of the interelectrode distance on the production of nanoparticles by means of atmospheric pressure inert gas DC glow discharge
This work is aimed at investigating the influence of the inter-electrode spacing on the production rate and size of nanoparticles generated by evaporating a cathode on an atmospheric pressure dc glow discharge. Experiments are conducted in the configuration of two vertically aligned cylindrical electrodes in upward coaxial flow with copper as a consumable cathode and nitrogen as a carrier gas. A constant current of 0.5 A is delivered to the electrodes and the inter-electrode distance spanned from 0.5 to 10 mm. Continuous stable nanoparticle production is attained by optimal coaxial flow convection cooling of the cathode. Both the particle production rate and the primary particle size increase with the inter-electrode spacing up to nearly 5 mm and strongly decrease with an increasing inter-electrode distance beyond 5 mm. Production rates in the range of 1 mg h-1 of very small nanoparticles
Topological Insight into Superabsorbent Hydrogel Network Structures: a 1H Double-Quantum NMR Study
A sustainable route for antibacterial nanofinishing of textiles
In this paper, an aerosol-based process is shown for imparting antibacterial property to textiles. Metal nanoparticles (copper and silver) are produced by means of DC electrical discharges (glow and arc) between two electrodes in nitrogen at ambient pressure and passed through textile fabrics (cotton, polyester and lyocell) which act as filter media. The particle retention efficiency of the fabrics is measured in dependence of particle size and face velocity. The antibacterial performance of the fabrics treated with metal nanoparticles and its durability to wash is assessed according to industry standards. Loads of about 200 ppm (2x10-2 %wt.) of nanoparticles of copper or silver give strong antibacterial property but the colour and hand feeling of the fabrics are significantly affected. Nanosilver loads in the order of 50 ppm (5x10-3 %wt.) impart comparably high antibacterial property to the fabrics with no visible impact on colour and hand touching, and wash fastness is proven for 10 washes. Small silver nanoparticles (20 nm)