Operating characteristics of a hollow-cathode neutralizer for 5 and 8 centimeter-diameter electron bombardment mercury ion thrusters

Thin-tip 0.3-cm-outside-diameter hollow-cathode neutralizers were used to investigate causes of neutralizer tip erosion experienced in thruster endurance tests. Bell-jar tests indicated that neutralizers with new rolled tantalum foil inserts coated with an emissive mixture eroded very little over the neutral flow rates investigated (3 to 10 mA) for simulated 5- and 8-cm-diameter thruster neutralizer conditions. Tip erosion rates of neutralizers operated with no insert or emissive mixture increased by two orders of magnitude for both configurations as the neutral flow rate decreased. Spectroscopic analysis of the discharge plasma from neutralizers operated with inserts coated with the emissive mixture detected tungsten at all neutral flow rates for both thruster neutralizer conditions. The only source of tungsten was the tip. Therefore, detection of tungsten indicated neutralizer tip erosion. Barium, an element of the emissive mixture, was detected at low neutral flow rates for the 5-cm-diameter thruster neutralizer operating condition only

Texturing polymer surfaces by transfer casting

A technique for fabricating textured surfaces on polymers without altering their surface chemistries is described. A surface of a fluorocarbon polymer is exposed to a beam of ions to texture it. The polymer which is to be surface-roughened is then cast over the textured surface of the fluorocarbon polymer. After curing, the cast polymer is peeled off the textured fluorocarbon polymer, and the peeled off surface has negative replica of the textured surface. The microscopic surface texture provides large surface areas for adhesive bonding. In cardiovascular prosthesis applications the surfaces are relied on for the development of a thin adherent well nourished thrombus

Scanning-electron-microscopy observations and mechanical characteristics of ion-beam-sputtered surgical implant alloys

An electron bombardment ion thruster was used as an ion source to sputter the surfaces of orthopedic prosthetic metals. Scanning electron microscopy photomicrographs were made of each ion beam textured surface. The effect of ion texturing an implant surface on its bond to bone cement was investigated. A Co-Cr-W alloy and surgical stainless steel were used as representative hard tissue implant materials to determine effects of ion texturing on bulk mechanical properties. Work was done to determine the effect of substrate temperature on the development of an ion textured surface microstructure. Results indicate that the ultimate strength of the bulk materials is unchanged by ion texturing and that the microstructure will develop more rapidly if the substrate is heated prior to ion texturing

Development of a qualification standard for adhesives used in hybrid microcircuits

Improved qualification standards and test procedures for adhesives used in microelectronic packaging are developed. The test methods in specification for the Selection and Use of Organic Adhesives in Hybrid Microcircuits are reevaluated versus industry and government requirements. Four electrically insulative and four electrically conductive adhesives used in the assembly of hybrid microcircuits are selected to evaluate the proposed revised test methods. An estimate of the cost to perform qualification testing of an adhesive to the requirements of the revised specification is also prepared

Optical properties of ion beam textured metals

Copper, silicon, aluminum, titanium and 316 stainless steel were textured by 1000 eV xenon ions from an 8 cm diameter electron bombardment ion source. Simultaneously sputter-deposited tantalum was used to facilitate the development of the surface microstructure. Scanning electron microscopy of the ion textured surfaces revealed two types of microstructure. Copper, silicon, and aluminum developed a cone structure with an average peak-to-peak distance ranging from 1 micron for silicon to 6 microns for aluminum. Titanium and 316 stainless steel developed a serpentine ridge structure. The average peak-to-peak distance for both of these materials was 0.5 micron. Spectral reflectance was measured using an integrating sphere and a holraum reflectometer. Total reflectance for air mass 0 and 2, solar absorptance and total emittance normalized for a 425 K black body were calculated from the reflectance measurements

The inheritance of dynamic and deontic integrity constraints or: Does the boss have more rights?

In [18,23], we presented a language for the specification of static, dynamic and deontic integrity constraints (IC's) for conceptual models (CM's). An important problem not discussed in that paper is how IC's are inherited in a taxonomic network of types. For example, if students are permitted to perform certain actions under certain preconditions, must we repeat these preconditions when specializing this action for the subtype of graduate students, or are they inherited, and if so, how? For static constraints, this problem is relatively trivial, but for dynamic and deontic constraints, it will turn out that it contains numerous pitfalls, caused by the fact that common sense supplies presuppositions about the structure of IC inheritance that are not warranted by logic. In this paper, we unravel some of these presuppositions and show how to avoid the pitfalls. We first formulate a number of general theorems about the inheritance of necessary and/or sufficient conditions and show that for upward inheritance, a closure assumption is needed. We apply this to dynamic and deontic IC's, where conditions arepreconditions of actions, and show that our common sense is sometimes mistaken about the logical implications of what we have specified. We also show the connection of necessary and sufficient preconditions of actions with the specification of weakest preconditions in programming logic. Finally, we argue that information analysts usually assume constraint completion in the specification of (pre)conditions analogous to predicate completion in Prolog and circumscription in non-monotonic logic. The results are illustrated with numerous examples and compared with other approaches in the literature

Mechanical properties of ion-beam-textured surgical implant alloys

An electron-bombardment Hg ion thruster was used as an ion source to texture surfaces of materials used to make orthopedic and/or dental prostheses or implants. The materials textured include 316 stainless steel, titanium-6% aluminum, 4% vanadium, and cobalt-20% chromium, 15% tungsten. To determine the effect of ion texturing on the ultimate strength and yield strength, stainless steel and Co-Cr-W alloy samples were tensile tested to failure. Three types of samples of both materials were tested. One type was ion-textured (the process also heats each sample to 300 C), another type was simply heated to 300 C in an oven, and the third type was untreated. Stress-strain diagrams, 0.2% offset yield strength data, total elongation data, and area reduction data are presented. Fatigue specimens of ion textured and untextured 316 stainless steel and Ti-6% Al-4% V were tested. Included as an ion textured sample is a Ti-6% Al-4% V sample which was ion machined by means of Ni screen mask so as to produce an array of 140 mu m x 140 mu m x 60 mu m deep pits. Scanning electron microscopy was used to characterize the ion textured surfaces

Time-resolved X-ray microscopy of nanoparticle aggregates under oscillatory shear

Of all current detection techniques with nanometer resolution, only X-ray microscopy allows imaging nanoparticles in suspension. Can it also be used to investigate structural dynamics? When studying response to mechanical stimuli, the challenge lies in applying them with precision comparable to spatial resolution. In the first shear experiments performed in an X-ray microscope, we accomplished this by inserting a piezo actuator driven shear cell into the focal plane of a scanning transmission X-ray microscope (STXM). Thus shear-induced reorganization of magnetite nanoparticle aggregates could be demonstrated in suspension. As X-ray microscopy proves suitable for studying structural change, new prospects open up in physics at small length scales.Comment: submitted to J. Synchrot. Radia