18 research outputs found

    Synthesis and characterization of SiO2/Bi2WO6 based on biogenic silica synthesized by sol-gel method

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    SiO2/Bi2WO6 photocatalyst with Si/Bi/W=1:2:1 molar ratio was obtained by the sol-gel method from bismuth nitrate, sodium tungstate and biogenic silica from rice husk biomass followed by calcination. Bi2WO6 was used as a control sample. FT-IR, SEM, XRD, EDXRF, UV-Vis methods were used to systematically characterize the as-obtained materials. Photodegradation of Indigo Carmine in exposure to UV, sunlight and xenon light was studied to evaluate their photocatalytic activities in the presence of SiO2/Bi2WO6 and Bi2WO6. It was shown that the degradation degree of Indigo Carmine in the presence of SiO2/Bi2WO6 under the action of UV irradiation and sunlight reaches 36% and 14%, respectively. The SiO2/Bi2WO6 sample is stable during photocatalytic studies

    Individual Differences in Students’ Effort Source Beliefs Predict Their Judgments of Ability

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    A recent set of studies (Muenks, Miele, & Wigfield, 2016) introduced the concept of perceived effort source to better explain how students reason about the relation between effort and ability when evaluating the academic abilities of other students. These studies showed that participants who were induced to perceive effort as task-elicited (i.e., as being primarily due to the subjective difficulty of the task) were more likely to view effort and ability as inversely related than participants who were induced to perceive effort as self-initiated (i.e., as being due to students’ motivation to go beyond the basic demands of the task). The current studies expanded on this research by demonstrating that, in the absence of an effort source manipulation, college students spontaneously invoked beliefs about the source of effort when evaluating their own (Study 2) and other students’ (Studies 1–3) abilities. The three studies also showed that our novel measure of individual differences in effort source beliefs was a better predictor of participants’ judgments of math ability (Studies 1 and 2) and verbal ability (Study 3) than a standard measure of their ability mindsets (i.e., beliefs about the extent to which intelligence is malleable). Specifically, participants who naturally tended to perceive effort as task-elicited generally rated students who expended relatively little effort as having more ability than did participants who tended to perceive effort as self-initiated. Implications for research on student motivation and for education practice are discussed

    Synthesis and characterization of SiO

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    SiO2/Bi2WO6 photocatalyst with Si/Bi/W=1:2:1 molar ratio was obtained by the sol-gel method from bismuth nitrate, sodium tungstate and biogenic silica from rice husk biomass followed by calcination. Bi2WO6 was used as a control sample. FT-IR, SEM, XRD, EDXRF, UV-Vis methods were used to systematically characterize the as-obtained materials. Photodegradation of Indigo Carmine in exposure to UV, sunlight and xenon light was studied to evaluate their photocatalytic activities in the presence of SiO2/Bi2WO6 and Bi2WO6. It was shown that the degradation degree of Indigo Carmine in the presence of SiO2/Bi2WO6 under the action of UV irradiation and sunlight reaches 36% and 14%, respectively. The SiO2/Bi2WO6 sample is stable during photocatalytic studies

    Synthesis and characterization of SiO

    No full text
    SiO2/Bi2WO6 photocatalyst with Si/Bi/W=1:2:1 molar ratio was obtained by the sol-gel method from bismuth nitrate, sodium tungstate and biogenic silica from rice husk biomass followed by calcination. Bi2WO6 was used as a control sample. FT-IR, SEM, XRD, EDXRF, UV-Vis methods were used to systematically characterize the as-obtained materials. Photodegradation of Indigo Carmine in exposure to UV, sunlight and xenon light was studied to evaluate their photocatalytic activities in the presence of SiO2/Bi2WO6 and Bi2WO6. It was shown that the degradation degree of Indigo Carmine in the presence of SiO2/Bi2WO6 under the action of UV irradiation and sunlight reaches 36% and 14%, respectively. The SiO2/Bi2WO6 sample is stable during photocatalytic studies

    Electrochemical Properties of Bismuth Oxide Films on Titanium Formed by Plasma Electrolytic Oxidation

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    На повСрхности Ρ‚ΠΈΡ‚Π°Π½Π° ΠΌΠ΅Ρ‚ΠΎΠ΄ΠΎΠΌ ΠΏΠ»Π°Π·ΠΌΠ΅Π½Π½ΠΎ-элСктролитичСского оксидирования (ПЭО) сформированы Π²ΠΈΡΠΌΡƒΡ‚ΠΎΡΠΎΠ΄Π΅Ρ€ΠΆΠ°ΡˆΠΈΠ΅ оксидныС покрытия ΠΈΠ· элСктролитов, содСрТащих комплСксныС ΠΈΠΎΠ½Ρ‹ ЭДВА-Bi3+. ΠžΠΏΡ€Π΅Π΄Π΅Π»Π΅Π½Ρ‹ элСктрохимичСскиС характСристики – Ρ‚ΠΎΠΊΠΈ ΠΎΠ±ΠΌΠ΅Π½Π°, коэффициСнты пСрСноса Ξ± ΠΈ Ξ², коэффициСнты a ΠΈ b Π² ΡƒΡ€Π°Π²Π½Π΅Π½ΠΈΠΈ ВафСля. Для ΠΏΠΎΠ»ΡƒΡ‡Π΅Π½Π½Ρ‹Ρ… систСм установлСно Π²ΠΎΠ·Π½ΠΈΠΊΠ½ΠΎΠ²Π΅Π½ΠΈΠ΅ аналитичСского сигнала ΠΏΡ€ΠΈ комплСксономСтричСском Ρ‚ΠΈΡ‚Ρ€ΠΎΠ²Π°Π½ΠΈΠΈ солСй ΠΆΠ΅Π»Π΅Π·Π° (III). Рядом физичСских ΠΌΠ΅Ρ‚ΠΎΠ΄ΠΎΠ² (ΡΠΊΠ°Π½ΠΈΡ€ΡƒΡŽΡ‰Π°Ρ элСктронная микроскопия с энСргодиспСрсным Π°Π½Π°Π»ΠΈΠ·ΠΎΠΌ ΠΈ рСнтгСновская фотоэлСктронная спСктроскопия) ΠΈΠ·ΡƒΡ‡Π΅Π½Ρ‹ морфология ΠΈ состав повСрхности оксидных ΠΏΠΎΠΊΡ€Ρ‹Ρ‚ΠΈΠΉ. НайдСна коррСляция ΠΌΠ΅ΠΆΠ΄Ρƒ ΠΌΠΎΡ€Ρ„ΠΎΠ»ΠΎΠ³ΠΈΠ΅ΠΉ, составом повСрхности ΠΈ элСктрохимичСскими свойствами ΠΎΠ±Ρ€Π°Π·Ρ†ΠΎΠ²Bismuth oxide layers on a titanium are formed by a plasma electrolytic oxidation (PEO) method from electrolytes containing complex ions EDTA-Bi3+. Electrochemical characteristics – exchange currents, transport coefficients Ξ± and Ξ², a and b coefficients in Tafel’s equation are defined. For the obtained systems occurrence of an analytical signal at complexometric titration of salts of Fe (III) is established. The structural features of surface electrodes have been investigated by scanning electron microscopy (SEM) and X-ray photoelectron spectroscopy (XPS) techniques. Correlation between morphology, structure of a surface and electrochemical properties of samples is foun

    Electrochemical Properties of Bismuth Oxide Films on Titanium Formed by Plasma Electrolytic Oxidation

    No full text
    На повСрхности Ρ‚ΠΈΡ‚Π°Π½Π° ΠΌΠ΅Ρ‚ΠΎΠ΄ΠΎΠΌ ΠΏΠ»Π°Π·ΠΌΠ΅Π½Π½ΠΎ-элСктролитичСского оксидирования (ПЭО) сформированы Π²ΠΈΡΠΌΡƒΡ‚ΠΎΡΠΎΠ΄Π΅Ρ€ΠΆΠ°ΡˆΠΈΠ΅ оксидныС покрытия ΠΈΠ· элСктролитов, содСрТащих комплСксныС ΠΈΠΎΠ½Ρ‹ ЭДВА-Bi3+. ΠžΠΏΡ€Π΅Π΄Π΅Π»Π΅Π½Ρ‹ элСктрохимичСскиС характСристики – Ρ‚ΠΎΠΊΠΈ ΠΎΠ±ΠΌΠ΅Π½Π°, коэффициСнты пСрСноса Ξ± ΠΈ Ξ², коэффициСнты a ΠΈ b Π² ΡƒΡ€Π°Π²Π½Π΅Π½ΠΈΠΈ ВафСля. Для ΠΏΠΎΠ»ΡƒΡ‡Π΅Π½Π½Ρ‹Ρ… систСм установлСно Π²ΠΎΠ·Π½ΠΈΠΊΠ½ΠΎΠ²Π΅Π½ΠΈΠ΅ аналитичСского сигнала ΠΏΡ€ΠΈ комплСксономСтричСском Ρ‚ΠΈΡ‚Ρ€ΠΎΠ²Π°Π½ΠΈΠΈ солСй ΠΆΠ΅Π»Π΅Π·Π° (III). Рядом физичСских ΠΌΠ΅Ρ‚ΠΎΠ΄ΠΎΠ² (ΡΠΊΠ°Π½ΠΈΡ€ΡƒΡŽΡ‰Π°Ρ элСктронная микроскопия с энСргодиспСрсным Π°Π½Π°Π»ΠΈΠ·ΠΎΠΌ ΠΈ рСнтгСновская фотоэлСктронная спСктроскопия) ΠΈΠ·ΡƒΡ‡Π΅Π½Ρ‹ морфология ΠΈ состав повСрхности оксидных ΠΏΠΎΠΊΡ€Ρ‹Ρ‚ΠΈΠΉ. НайдСна коррСляция ΠΌΠ΅ΠΆΠ΄Ρƒ ΠΌΠΎΡ€Ρ„ΠΎΠ»ΠΎΠ³ΠΈΠ΅ΠΉ, составом повСрхности ΠΈ элСктрохимичСскими свойствами ΠΎΠ±Ρ€Π°Π·Ρ†ΠΎΠ²Bismuth oxide layers on a titanium are formed by a plasma electrolytic oxidation (PEO) method from electrolytes containing complex ions EDTA-Bi3+. Electrochemical characteristics – exchange currents, transport coefficients Ξ± and Ξ², a and b coefficients in Tafel’s equation are defined. For the obtained systems occurrence of an analytical signal at complexometric titration of salts of Fe (III) is established. The structural features of surface electrodes have been investigated by scanning electron microscopy (SEM) and X-ray photoelectron spectroscopy (XPS) techniques. Correlation between morphology, structure of a surface and electrochemical properties of samples is foun
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