Humidity effects on tip-induced polarization switching in lithium niobate

Interest to ferroelectric materials has been increased significantly in last decades due to development of new generation of nonlinear optical and data storage devices. Scanning probe microscopy (SPM) can be used both for study of domain structures with nanoscale spatial resolution and for writing the isolated nanodomains by local application of the electric field. Tip-induced switching in the ambient still needs experimental investigations and theoretical explorations. Here we studied influence of the value of relative humidity in the SPM chamber on the process of tip-induced polarization switching. This phenomenon was attributed to existing of the water meniscus between tip and the sample surface in humid atmosphere. Presented results are important for further complex investigations of the ferroelectric materials and their applications.Comment: 15 pages, 5 figures, Submitted to Applied Physics Letter

Electromechanical Probing of Ionic Currents in Energy Storage Materials

The electrochemical processes in energy storage materials are generally linked with changes of molar volume of the host compound. Here, the frequency dependent strain response of 1D electrochemically active systems to periodic electric bias is analyzed. The sensitivity and resolution of these electrochemical strain measurements are compared to the current-based electrochemical impedance spectroscopy. The resolution and detection limits of interferometric and atomic force microscopy based systems for probing electrochemical reactions on the nanoscale are analyzed.Comment: 12 pages, 4 figures, 2 tables, 2 appendices, submitted to Appl. Phys. Let

Experimental Study of the Effect of External Signal on Microwave Oscillations in a Nonrelativistic Electron Beam with Virtual Cathode

The effect of an external harmonic signal on the characteristics of microwave generation in a nonrelativistic electron beam with virtual cathode (VC) formed in a static retarding electric field (low-voltage vircator system) has been experimentally studied. A significant increase in the vircator generation power is observed when the frequency of the external signal is close to the frequency of VC oscillations. At large detunings, a broadband chaotic generation is observed.Comment: 3 pages, 2 figure