8 research outputs found

    Characterization of volatile and odor-active compounds of the essential oil from Bidens graveolens Mart. (Asteraceae).

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    Made available in DSpace on 2020-01-10T18:12:16Z (GMT). No. of bitstreams: 1 Silvaetal2020FlavourandFragranceJournal.pdf: 416234 bytes, checksum: c787e768127dd577e2342e218c9a257c (MD5) Previous issue date: 2020bitstream/item/208517/1/Silva-et-al-2020-Flavour-and-Fragrance-Journal.pd

    Development and validation of a method for the analysis of Ochratoxin A in roasted coffee by liquid chromatography/electrospray-mass spectrometry in Tandem (LC/ESI-MS/MS).

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    A method using LC/ESI-MS/MS for the quantitative analysis of Ochratoxin A in roasted coffee was described. Linearity was demonstrated (r = 0.9175). The limits of detection and quantification were 1.0 and 3.0 ng g-1, respectively. Trueness, repeatability and intermediate precision values were 89.0-108.8%; 2.4-13.7%; 12.5-17.8%, respectively. To the best of our knowledge, this is the first report in which Ochratoxin A in roasted coffee is analysed by LC/ESI-MS/MS, contributing to the field of mycotoxin analysis, and it will be used for future production of Certified Reference Material
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