Development of EM-CCD-based X-ray detector for synchrotron applications

A high speed, low noise camera system for crystallography and X-ray imaging applications is developed and successfully demonstrated. By coupling an electron-multiplying (EM)-CCD to a 3:1 fibre-optic taper and a CsI(Tl) scintillator, it was possible to detect hard X-rays. This novel approach to hard X-ray imaging takes advantage of sub-electron equivalent readout noise performance at high pixel readout frequencies of EM-CCD detectors with the increase in the imaging area that is offered through the use of a fibre-optic taper. Compared with the industry state of the art, based on CCD camera systems, a high frame rate for a full-frame readout (50 ms) and a lower readout noise (<1 electron root mean square) across a range of X-ray energies (6–18 keV) were achieved

Grain Sorghum Performance

Twenty-five grain sorghum hybrids and one variety planted May 22 were evaluated at the Western Kentucky Substation at Princeton for yield, plant height, date headed, head type and moisture. They were also evaluated at Lexington for bird damage and at the Robinson Substation for MDM

1974 Preliminary Report of Kentucky Small Grain Variety Trials at Bowling Green and Lexington

Each year the small grain variety trials are conducted at Princeton, Murray, Bowling Green and Lexington. In 1974, the plots at Princeton and Murray were severely infected with a complex of diseases including Barley Yellow Dwarf, Septoria glume blotch, wheat scab and an unidentified disease in the wheat. As a result of the intensity of these diseases, the data obtained from these plots was very erratic and the results were not considered to be experimentally valid. The data obtained at Bowling Green and Lexington were quite valid and representative of the general situation in Kentucky

The meshing of timing belt teeth in pulley grooves

The work described here has been carried out to obtain a better understanding of the tooth root cracking failure mode of timing belts. Previous work has demonstrated the close dependence of this on the tooth deflections of fully meshed teeth, generated by torque transmission, but has not considered the additional distortions generated in the partially meshed conditions at entry to and exit from a pulley groove. Approximate compatibility and constitutive equations are combined with a rigorous consideration of tooth equilibrium in partial meshing to show how bending moments are generated at both exit from a driven pulley and entry to a driving pulley. Experimentally determined belt lives correlate very well with a combined measure of fully meshed tooth strain and strain due to bending at entry or exit. The analysis also shows that this strain measure reduces with increasing belt tooth stiffness, confirming the importance of a high tooth stiffness for a long belt life. Tooth force variations through the partial meshing cycle have also been predicted and compared with measurements obtained from a special strain gauge instrumented pulley. A greater pulley rotation than is predicted is required for a belt tooth to seat in a pulley groove. There is room for improvement in the modellin

Improving the resolution in soft X-ray emission spectrometers through photon-counting using an Electron Multiplying CCD

In 2007, a study of back-illuminated Charge-Coupled Devices (CCDs) for soft X-ray photon detection demonstrated the improvements that could be brought over more traditional micro-channel plate detectors for X-ray spectrometers based on diffraction gratings and position sensitive detectors. Whilst the spatial resolution was reported to be improved dramatically, an intrinsic limit of approximately 25 micrometers was found due to the spreading of the charge cloud generated in the CCD across several pixels. To overcome this resolution limit, it is necessary to move away from the current integrated imaging methods and consider a photon-counting approach, recording the photon interaction locations to the sub-pixel level. To make use of photon-counting techniques it is important that the individual events are separable. To maintain the throughput of the spectrometer for high intensity lines, higher frame rates and therefore higher readout speeds are required. With CCD based systems, the increased noise at high readout speeds can limit the photon-counting performance. The Electron-Multiplying CCD shares a similar architecture with the standard CCD but incorporates a "gain register". This novel addition allows controllable gain to be applied to the signal before the read noise is introduced, therefore allowing individual events to be resolved above the noise even at much higher readout rates. In the past, the EM-CCD has only been available with imaging areas too small to be practical in soft X-ray emission spectrometers. The current drive for large area Electron-Multiplying CCDs is opening this technology to new photon-counting applications, requiring in-depth analysis of the processes and techniques involved. Early results indicate that through the introduction of photon-counting techniques the resolution in such systems can be dramatically improved

Developing a high-resolution x-ray imager using electron-multiplying (EM) CCDs

Applications at synchrotron facilities such as macromolecular crystallography and high energy X-ray diffraction require high resolution imaging detectors with high dynamic range and large surface area. Current systems can be split into two main categories: hybrid pixel detectors and scintillator-coupled Charge-Coupled Devices (CCDs). Whilst both have limitations, CCD-based systems (coupled to fibre-optics to increase imaging area) are often used in these applications due to their small pixels and the high resolution. Electron-Multiplication CCDs (EM-CCDs) are able to suppress the readout noise associated with increased readout speed offering a low noise, high speed detector solution. A previous pilot study using a small-area (8 mm × 8 mm) scintillator-coupled EM-CCD found that through high frame-rates, low noise and novel uses of photon-counting, resolution could be improved from over 80 μm to 25 μm at 2 fps. To further improve this detector system, high speed readout electronics can be used alongside a fibre-optic taper and EM-CCD to create a “best of both worlds” solution consisting of the high resolution of a CCD, along with the low noise, high speed (high dynamic range) and large effective area of pixel detectors. This paper details the developments in the study and discusses the latest results and their implication on the system design

The noise performance of electron-multiplying charge-coupled devices at X-ray energies

Electron-multiplying charge-coupled devices (EMCCDs) are used in low-light-level (L3) applications for detecting optical, ultraviolet, and near-infrared photons (10–1100 nm). The on-chip gain process is able to increase the detectability of any signal collected by the device through the multiplication of the signal before the output node. Thus, the effective readout noise can be reduced to subelectron levels, allowing the detection of single photons. However, this gain process introduces an additional noise component due to the stochastic nature of the multiplication. In optical applications, this additional noise has been characterized. The broadening of the detected peak is described by the excess noise factor. This factor tends to a value of √2 at high gain (>100x). In X-ray applications, the situation is improved by the effect that Fano factor f has on the shot noise associated with X-ray photon detection (f ≈ 0.12 at X-ray energies). In this paper, the effect of the detection of X-ray photons in silicon is assessed both analytically and through a Monte Carlo model of the gain amplification process. The excess noise on the signal is predicted (termed the modified Fano factor) for photon detection in an EM-CCD at X-ray energies. A hypothesis is made that the modified Fano factor should tend to 1.115 at high levels of gain (>10x). In order to validate the predictions made, measurements were taken using an 55 Fe source with Mn k-alpha X-ray energy of 5898 eV. These measurements allowed the hypothesis to be verified

Mitigating radiation-induced charge transfer inefficiency in full-frame CCD applications by ‘pumping’ traps

The charge transfer efficiency of a CCD is based on the average level of signal lost per pixel over a number of transfers. This value can be used to directly compare the relative performances of different structures, increases in radiation damage or to quantify improvements in operating parameters. This number does not however give sufficient detail to mitigate for the actual signal loss/deference in either of the transfer directions that may be critical to measuring shapes to high accuracy, such as those required in astronomy applications (e.g. for Gaia’s astrometry or the galaxy distortion measurements for Euclid) based in the radiation environment of space. Pocket-pumping is an established technique for finding the location and activation levels of traps; however, a number of parameters in the process can also be explored to identify the trap species and location to sub-pixel accuracy. This information can be used in two ways to increase the sensitivity of a camera. Firstly, the clocking process can be optimised for the time constant of the majority of traps in each of the transfer directions, reducing deferred charge during read out. Secondly, a correction algorithm can be developed and employed during the post-processing of individual frames to move most of any deferred signal back into the charge packet it originated from. Here we present the trap-pumping techniques used to optimise the charge transfer efficiency of p- and n-channel e2v CCD204s and describe the use of trap-pumped images for on-orbit calibration and ground based image correction algorithms