25 research outputs found

    Behaviour of metals at ultra-high strain rate by using femtosecond laser shockwaves

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    The mechanical behavior of materials under extreme conditions can be investigated by using laser driven shocks. Actually, femtosecond (fs) technologies allow to reach strong pressures over a very fast duration. This work is dedicated to characterize metals behavior in this ultra-short mode, (aluminum, tantalum), leading to an extreme dynamic solicitation in the target (>107s−1). The study includes the validation of experimental results obtained on the LULI 100TW facility by comparison with numerical model. Three modeling steps are considered. First, we characterize the pressure loading resulting from the fs laser-matter interaction, different from what happens in the classical nanosecond regime. Then, the shock wave propagation is observed through the target and particularly its pressure decay, strong in this regime. The elastic-plastic influence on the shock attenuation is discussed, particularly for tantalum which has a high elastic limit. Dynamic damage appears with spallation. Experimentally, spallation is characterized by VISAR measurements and post-test observations. Shots with different thicknesses have been carried out to determine the damage properties in function of strain rate. We show in this work that a simple instantaneous rupture criterion is not sufficient to reproduce the damage induced in the sample. Only the Kanel model, which includes damage kinetics, is able to reproduce experimental data (VISAR measurements, spall thickness). A generalization of this model to any strain rate can be performed by confronting these results to other shock generators data (ns laser driven shocks, plate impacts). One remarkable result is that every Kanel parameters follows a power law with strain rate in dynamic regime (105 to 108s−1) for both aluminum and tantalum

    Red Xylem and Higher Lignin Extractability by Down-Regulating a Cinnamyl Alcohol Dehydrogenase in Poplar.

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    Cinnamyl alcohol dehydrogenase (CAD) catalyzes the last step in the biosynthesis of the lignin precursors, the monolignols. We have down-regulated CAD in transgenic poplar (Populus tremula X Populus alba) by both antisense and co-suppression strategies. Several antisense and sense CAD transgenic poplars had an approximately 70% reduced CAD activity that was associated with a red coloration of the xylem tissue. Neither the lignin amount nor the lignin monomeric composition (syringyl/guaiacyl) were significantly modified. However, phloroglucinol-HCl staining was different in the down-regulated CAD plants, suggesting changes in the number of aldehyde units in the lignin. Furthermore, the reactivity of the cell wall toward alkali treatment was altered: a lower amount of lignin was found in the insoluble, saponified residue and more lignin could be precipitated from the soluble alkali fraction. Moreover, large amounts of phenolic compounds, vanillin and especially syringaldehyde, were detected in the soluble alkali fraction of the CAD down-regulated poplars. Alkaline pulping experiments on 3-month-old trees showed a reduction of the kappa number without affecting the degree of cellulose degradation. These results indicate that reducing the CAD activity in trees might be a valuable strategy to optimize certain processes of the wood industry, especially those of the pulp and paper industry

    A comparative study of three adhesion tests (EN 582, similar to ASTM C633, LASAT (LASer Adhesion Test), and bulge and blister test) performed on plasma sprayed copper deposited on aluminium 2017 substrates

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    International audienceThe aim of this study was to compare three adhesion tests carried out on plasma-sprayed copper coatings on aluminium substrates. The first test, the bond pull test, designated EN 582 or ASTM C633, involves a uniaxial static stress and is commonly used in the coating industry. The second test, the LASAT (LASer Adhesion Test), is a recently developed technique based on spallation phenomenon due to laser induced shock waves. In this test, the coating delamination results from spallation at the coating/substrate interface due to uniaxial tensile stress. The last test, the bulge and blister test, involves a quasi-static measurement of the crack propagation energy at the coating/substrate interface. These three techniques have been used to evaluate the influences of different process parameters involved in the coating adhesion such as aluminium surface roughness, substrate pre-heating and plasma spray conditions
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