Optimization of a Green Dyeing Process Using Natural Dyes Extracted from Corchorus Olitorius Leaves

The main purpose of this study is to develop a green dyeing process using Corchorus olitorius dye extract. Corchorus olitorius leaves were used as a new dyestuff source that has never been used for cotton fabric dyeing. Dye extraction was performed using a non-conventional clean process containing ethanol in an ultrasound bath. The extracted dye was applied to cotton fabric in a bath exhaustion process. The effect of dyeing parameters on the color strength of dyed fabric was studied. A response surface methodology design was used to optimize the dyeing process. The results showed that pH, dyeing temperature, and dyeing time significantly affect the dyed fabric. The optimum dyeing parameters were found at 90°C in a bath pH of 9 for 90 min. Finally, to improve the color strength, and the color-fastness, three mordanting processes, and three different mordants were used. Results show that pre-mordanted dyed cotton fabric using aluminum potassium sulfate produces the best fastness properties

Sustainable Dyeing of Cotton Fibers Using Aqueous Extract of Citrullus Colocynthis Leaves: Chemical Characterization, and Dyeing Optimization Process Using Response Surface Methodology

Owing to their advantageous characteristics, natural dyes are highly needed to replace hazardous synthetic colored molecules. In this work, an aqueous extract of Citrullus colocynthis leaves was prepared, analyzed using Fourier Transform Infrared (FT-IR) spectroscopy and High-Pressure Liquid Chromatography/Mass Spectrometry (LC-MS/MS), and further used to dye cotton fibers. FT-IR results suggested that the studied Citrullus colocynthis leaf is possibly rich in phenolic and flavonoid constituents. The dyeing experiments were carried out at various experimental conditions: dyeing duration (30–60 min), temperature (60–100°C), and pH (5–9). Response surface methodology (RSM), with the help of Minitab 17.1.0, was used to optimize the dyeing process. The optimum obtained dyeing conditions were time = 30 min, temperature = 91°C, and pH = 7. The cationization of cotton fabric with polyethyleneimine and a co-polymer of dimethyl diallyl ammonium chloride and diallylamin, and the pre-biomordanting with pomegranate peel and date palm pits significantly improved the color strength (K/S) results. Overall, the dyed cotton samples exhibited good fastness characteristics

Sustainable Dyeing of Cotton Fibers Using Aqueous Extract of <i>Citrullus Colocynthis</i> Leaves: Chemical Characterization, and Dyeing Optimization Process Using Response Surface Methodology

Owing to their advantageous characteristics, natural dyes are highly needed to replace hazardous synthetic colored molecules. In this work, an aqueous extract of Citrullus colocynthis leaves was prepared, analyzed using Fourier Transform Infrared (FT-IR) spectroscopy and High-Pressure Liquid Chromatography/Mass Spectrometry (LC-MS/MS), and further used to dye cotton fibers. FT-IR results suggested that the studied Citrullus colocynthis leaf is possibly rich in phenolic and flavonoid constituents. The dyeing experiments were carried out at various experimental conditions: dyeing duration (30–60 min), temperature (60–100°C), and pH (5–9). Response surface methodology (RSM), with the help of Minitab 17.1.0, was used to optimize the dyeing process. The optimum obtained dyeing conditions were time = 30 min, temperature = 91°C, and pH = 7. The cationization of cotton fabric with polyethyleneimine and a co-polymer of dimethyl diallyl ammonium chloride and diallylamin, and the pre-biomordanting with pomegranate peel and date palm pits significantly improved the color strength (K/S) results. Overall, the dyed cotton samples exhibited good fastness characteristics.</p