Studies on the mechanical and thermal stability of Calotropis gigantea fibre-reinforced bran nano particulates epoxy composite

Abstract In recent trends, the usage of synthetic materials has been reduced by introducing natural fibres for lightweight applications. In this study, Madar (Calotropis gigantea) fibre is selected for the reinforcement phase (40%), and the epoxy polymer is blended with bran filler selected as a matrix material. To calculate hybrid composite mechanical characteristics, five composite laminates with different fibre/filler weight ratios were made. The results show that when the weight ratio of madar fibre increased, the superior mechanical properties were observed in the composite laminate sample (A), such as tensile strength (20.85 MPa), flexural strength (24.14 MPa), impact energy absorption (23 J) compared with an increasing the weight ratio of bran nanofiller to this composite material. At the same time, increasing bran nanofillers can improve thermal stability up to 445 °C of degrading temperature. To analyse the surface interaction between the madar fibres, bran nanofillers, and epoxy matrix by conducting the scanning electron microscope (SEM) analysis before subjecting to the mechanical test and also to identify the failure mode by conducting the SEM test after the laminates are broken during the mechanical tests of the hybrid composite

Effectiveness of Nanosilica on Enhancing the Mechanical and Microstructure Properties of Kenaf/Carbon Fiber-Reinforced Epoxy-Based Nanocomposites

With an ultrasonic frequency of 15 kHz and an 850 W power capacity, the effects of nanosilica particle inclusion on the tensile, flexural, and impact properties of woven fiber-reinforced kenaf/carbon fiber/epoxy hybrid composites were explored experimentally. The nanoparticles were dispersed uniformly in the epoxy using an ultrasonic probe. Test samples were made according to ASTM requirements for three distinct weight compositions of nanosilica particles (1, 1.5, and 2 wt%). The composites were made utilizing the compression moulding process with the following parameters: (i) weight ratio of nanosilica, (ii) length of kenaf fibers, and (iii) number of carbon fiber layers to achieve the objectives above. According to unmodified samples, with a nanosilica concentration of 1.5 wt%, tensile strength improved by 31%, flexural strength increased by 42.36%, and impact strength increased by 22.65%. It was established that the interaction of micro silica particles with epoxy and fiber, which improved interfacial tension, had a substantial impact on mechanical and water retention capabilities. The 1.5 wt% nanosilica inclusion absorbs less moisture than the 1 and 2 wt% silica composites. A scanning electron microscope was used to examine the fractured surface of the tested nanocomposites

Multiresponse Optimization of Mechanical Behaviour of Calotropis gigantea/Nano-Silicon-Based Hybrid Nanocomposites under Cryogenic Environment

The utilization of natural fibre-based biodegradable polymers has expanded in the present circumstances since natural fibres are relatively inexpensive, recyclable, lighter, nonflammable, and harmless. However, hydrophilic nature is the most serious issue. To address this issue, the current study was applied to enhance the material characteristics of hybrid composites strengthened by CGF and nanosilica powder. To accomplish the mentioned goal, RSM calculated and optimized the following processing parameters using the BBD arrangement at various CGF fibre thickness (gsm), weight percent of nanosilica powder (wt. percent), and cryogenic treatment period (min). To prevent hydrophilic nature, the fibres were pretreated for four hours with a 5% alkaline solution. Deterioration models were created to analyze the material characteristics, and the optimal progression variables were determined. Based on the multiresponse surface methodology, the governable process variables for nano-silica- and CGF-based hybrid nanocomposites should be set at 3% silica, 300 gsm of CGF, and 30 minutes of cryogenic treatment. The tension, bending, and impact property correlation coefficient values (R2) are 0.95, 0.94, and 0.95, respectively. The above-mentioned combinations provide better water absorption and mechanical strength

Processing and Characterization of Novel Bio-Waste Hybrid Brick Composites for Pollution Control

The main focus of this research is to enhance the use of eco-friendly materials these days. The current materials used in building construction are chemical-based and are harmful to humans and the environment. This research work has developed a new type of hybrid brick by using natural fibres and waste materials. This research focuses on fabricating novel bricks reinforced with different percentages of coconut waste fibre, wheat straw fibre, waste wood animal dung ash, gypsum, sand, and cement. The fabricated novel brick’s physical, mechanical, chemical, acoustic, and heat-absorbing properties were evaluated

Effect of Nano TiO2 Filler Addition on Mechanical Properties of Bamboo/Polyester Hybrid Composites and Parameters Optimized Using Grey Taguchi Method

Exploration has shifted from traditional materials and alloys to composite materials in recent years to develop lightweight, high-effective materials for specific purposes. Natural fibres are less costly, biodegradable, and nonflammable than glass fibres. This study explores how titanium oxide affects woven polyester reinforced composite’s mechanical and physical characteristics. Nanocomposites were created by hand utilizing the following terms: (i) TiO2 nanoparticle filler weight ratio, (ii) fibre content, and (iii) fibre diameter, all at three unique levels. Using the L9 (33) orthogonal design, nine composite samples are generated and tested according to the ASTM standard. According to the research, hybrid composites containing 4% titanium oxide powder and 15 mm length of bamboo fibre with 0.24 mm of bamboo fibre diameter have high mechanical strength. Adding fibre to pristine polyester increased its mechanical properties. As the fibre and filler percentages grew, more effort was required to break the fragments between the matrix and its resin. The verification test, which uses the optimal processing value and grey relational analysis, outperforms the real test results by a wide margin. Tensile strength increased by 14.76%, flexural strength increased by 14.07%, and hardness increased by 25.55%

Experimental Testing on Mechanical, Durability, and Adsorption Dispersion Properties of Concrete with Multiwalled Carbon Nanotubes and Silica Fumes

The major goal of this research is to see how carbon nanotubes and silica fume affect the durability and mechanical qualities of high-performance concrete (HPC). Mechanical properties, such as split tensile strength, compressive strength, elasticity modulus, and flexural strength, and durability properties like water absorption, abrasion, chloride penetration, acid, and sea water resistance, impact resistance of HPC consisting silica fume (SF), and carbon nanotubes (CNT) were examined in this study. Varied trail combinations with different proportions of CNT and SF admixtures were created for this reason. Portland cement was partially replaced with 1 percent, 1.5 percent, 2 percent, and 3 percent CNT, while SF was substituted with 5 percent, 7.5 percent, and 10 percent. Both CNT and SF outperform conventional concrete in terms of mechanical and durability attributes, according to the findings. CNT produces superior results than SF due to its smaller size

Multiresponse Optimization of Mechanical and Physical Adsorption Properties of Activated Natural Fibers Hybrid Composites

In the current scenario, natural fiber-based biodegradable composites have increased because natural composite fibers are very cheap, biodegradable, lightweight, fireproof, and nontoxic. The present research work was carried out to optimize the mechanical properties of hybrid composites reinforced by Calotropis gigantea and hemp. To achieve these objectives, the following process parameters were determined, and RSM carried out optimization with the Box-Behnken experimental setup at three different levels: compression molding temperature (°C), pressure (bar), and time (min). The fibers were pretreated for 4 hours with a 5% NaOH solution to prevent moisture absorption. Regression equations were constructed to evaluate the mechanical properties, and the best process parameters were established. The results reveal that a pressure of 35 bar, a time duration of 7 minutes, and a temperature of 176°C are the best conditions for compression molding. The second aim was to compare CGF and hemp fiber-derived activated carbon adsorbents by determining physical adsorption properties, chemical compositions, and scanning electron microscope. Natural fibers were shown to be ideal candidates for manufacturing mesoporous activated carbon adsorbents with high surface area (1389–1433 m2/g), high mesopore percentage (63–68%), and high carbon content (80–87%). Even though hemp activated carbon had a greater mesoporous structure (69%) than CGF-derived activated carbons, the CGF-derived activated carbons had larger surface areas and higher C content

Water Retention Behaviour and Fracture Toughness of Coir/Pineapple Leaf Fibre with Addition of Al2O3 Hybrid Composites under Ambient Conditions

Due to their high mechanical and physical properties, natural fibre-based composite materials have been important in many fields of application for four to five years. The chief intention of the current study is to determine the mechanical and water retention features of composite materials under ambient conditions. Coir and pineapple leaf fibre were used as a reinforcement, aluminium oxide as additives, and polyester as a matrix. The hybrid resources were laminated by the manual hand lay-up method. The mechanical characteristics like tensile, flexural, and fracture toughness properties were tested as per the ASTM standard. Nanoparticle weight ratio and its size variation significantly impact mechanical qualities. The hybrid composite’s water retention behaviour was tested for two types of water levels: ordinary tab water and nanofluid. The moisture uptake of the composites rose as the fibre volume increased, and after 640 hours, all of the composites had reached equilibrium. According to the results, the following combinations have the maximum mechanical strength: 15% wt.% coir, 15% wt.% pineapple, 10% wt.% nanofiller, and 60% wt.% polyester resin. The combinations mentioned above withstand the most load during the tests. Compared to 20% filler, 10% Al2O3 filler produces good interfacial adhesion in the current study. The fractured specimens were analyzed using scanning electron microscopic (SEM) pictures to recognize better the failure process of composites during mechanical testing

Investigation on Efficient Removal of Fluoride from Ground Water Using Activated Carbon Adsorbents

Groundwater seems to be the most significant natural source of potable water for millions of individuals. Fluoride pollution in groundwater is a big problem in Tamil Nadu’s Dharmapuri area. According to a survey done in a school in the Dharmapuri area, dental and skeletal fluoroses afflict almost 75% of school kids. There is no proven or recommended cost-effective strategy for lowering fluoride levels in the home. This study proposes cost-effective and efficient natural treatment approaches for lowering fluoride levels. In this experiment, fluorides in groundwater are eliminated to a suitable extent utilizing natural adsorbents. Neem stem charcoal (activated carbon), neem leaves powder, dry coconut husk, coconut shell charcoal (activated carbon), and rice husk powder are natural adsorbents. The adsorbents were utilized at different concentrations until the best concentration was found. The ideal concentration removes the bulk of fluoride from groundwater and delivers adequate treatment. People could adopt this cost-effective procedure because just a few components are enough. As per the Bureau of Indian Standards, the concentration should not exceed 1.5 ppm, and it should not be lesser than 1 ppm; keeping this in mind, the neem stem charcoal which has higher efficiency in removing fluoride can be used in extensive environments, but in this selected place, it reduces the concentration even below 1 ppm, which relays below the standard level. As a result, adopting these procedures helps prevent dental and skeletal fluoroses, which is common among young people