10 research outputs found

    Improving XMM-Newton EPIC pn data at low energies: method and application to the Vela SNR

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    High quantum efficiency over a broad spectral range is one of the main properties of the EPIC pn camera on-board XMM-Newton. The quantum efficiency rises from ~75% at 0.2 keV to ~100% at 1 keV, stays close to 100% until 8 keV, and is still ~90% at 10 keV. The EPIC pn camera is attached to an X-ray telescope which has the highest collecting area currently available, in particular at low energies (more than 1400 cm2 between 0.1 and 2.0 keV). Thus, this instrument is very sensitive to the low-energy X-ray emission. However, X-ray data at energies below ~0.2 keV are considerably affected by detector effects, which become more and more important towards the lowest transmitted energies. In addition to that, pixels which have received incorrect offsets during the calculation of the offset map at the beginning of each observation, show up as bright patches in low-energy images. Here we describe a method which is not only capable of suppressing the contaminations found at low energies, but which also improves the data quality throughout the whole EPIC pn spectral range. This method is then applied to data from the Vela supernova remnant.Comment: Proc. SPIE Vol. 5488: Astronomical Telescopes and Instrumentation, UV - Gamma-Ray Space Telescope Systems, Eds. Guenther Hasinger and Martin J. Turner, 22-24 June 2004, Glasgow, Scotland United Kingdo

    Energy-dispersive Laue diffraction by means of a frame-store pnCCD

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    A frame-store pn-junction CCD detector was applied to the energy-dispersive X-ray Laue diffraction study of a gamma-LiAlO2 crystal with white synchrotron radiation. Exploiting the simultaneous spatial and energy resolution of the detector the crystallographic unit cell of gamma-LiAlO2 could be determined without any a priori information about the sample. The potential for application in X-ray structure analysis is tested by comparing experimental structure factors taken under a single exposure with those calculated from the known crystal structure. After correcting the measured spot intensities by angular and energy-dependent parameters, the agreement between experimental and theoretical kinematical structure factors is better than 10%

    A 64k pixel CMOS-DEPFET module for the soft X-rays DSSC imager operating at MHz-frame rates

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    The 64k pixel DEPFET module is the key sensitive component of the DEPFET Sensor with Signal Compression (DSSC), a large area 2D hybrid detector for capturing and measuring soft X-rays at the European XFEL. The final 1-megapixel camera has to detect photons with energies between 250eV and 6keV, and must provide a peak frame rate of 4.5MHz to cope with the unique bunch structure of the European XFEL. This work summarizes the functionalities and properties of the first modules assembled with full-format CMOS-DEPFET arrays, featuring 512×128 hexagonally-shaped pixels with a side length of 136 μm. The pixel sensors utilize the DEPFET technology to realize an extremely low input capacitance for excellent energy resolution and, at the same time, an intrinsic capability of signal compression without any gain switching. Each pixel of the readout ASIC includes a DEPFET-bias current cancellation circuitry, a trapezoidal-shaping filter, a 9-bit ADC and a 800-word long digital memory. The trimming, calibration and final characterization were performed in a laboratory test-bench at DESY. All detector features are assessed at 18°C. An outstanding equivalent noise charge of 9.8 e⁻rms is achieved at 1.1-MHz frame rate and gain of 26.8 Analog-to-Digital Unit per keV (ADU/keV). At 4.5MHz and 3.1 ADU/keV, a noise of 25.5 e⁻rms and a dynamic range of 26 ke⁻ are obtained. The highest dynamic range of 1.345 Me⁻ is reached at 2.25 MHz and 1.6 ADU/keV. These values can fulfill the specification of the DSSC project

    The High Time Resolution Spectrometer (HTRS) aboard the International X-ray Observatory (IXO)

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    The High Time Resolution Spectrometer (HTRS) is one of the five focal plane instruments of the International X-ray Observatory (IXO). The HTRS is the only instrument matching the top level mission requirement of handling a one Crab X-ray source with an efficiency greater than 10%. It will provide IXO with the capability of observing the brightest X-ray sources of the sky, with sub-millisecond time resolution, low deadtime, low pile-up (less than 2% at 1 Crab), and CCD type energy resolution (goal of 150 eV FWHM at 6 keV). The HTRS is a non-imaging instrument, based on a monolithic array of Silicon Drift Detectors (SDDs) with 31 cells in a circular envelope and a X-ray sensitive volume of 4.5 cm2 x 450 μm. As part of the assessment study carried out by ESA on IXO, the HTRS is currently undergoing a phase A study, led by CNES and CESR. In this paper, we present the current mechanical, thermal and electrical design of the HTRS, and describe the expected performance assessed through Monte Carlo simulations

    Anomalous signal from S atoms in protein crystallographic data from an X-ray free-electron laser

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    X-ray free-electron lasers (FELs) enable crystallographic data collection using extremely bright femtosecond pulses from microscopic crystals beyond the limitations of conventional radiation damage. This diffraction-before-destruction approach requires a new crystal for each FEL shot and, since the crystals cannot be rotated during the X-ray pulse, data collection requires averaging over many different crystals and a Monte Carlo integration of the diffraction intensities, making the accurate determination of structure factors challenging. To investigate whether sufficient accuracy can be attained for the measurement of anomalous signal, a large data set was collected from lysozyme microcrystals at the newly established `multi-purpose spectroscopy/imaging instrument' of the SPring-8 Ångstrom Compact Free-Electron Laser (SACLA) at RIKEN Harima. Anomalous difference density maps calculated from these data demonstrate that serial femtosecond crystallography using a free-electron laser is sufficiently accurate to measure even the very weak anomalous signal of naturally occurring S atoms in a protein at a photon energy of 7.3 keV

    Toward unsupervised single-shot diffractive imaging of heterogeneous particles using X-ray free-electron lasers

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    Single shot diffraction imaging experiments via X-ray free- electron lasers can generate as many as hundreds of thousands of diffraction patterns of scattering objects. Recovering the real space contrast of a scat- tering object from these patterns currently requires a reconstruction process with user guidance in a number of steps, introducing severe bottlenecks in data processing. We present a series of measures that replace user guidance with algorithms that reconstruct contrasts in an unsupervised fashion. We demonstrate the feasibility of automating the reconstruction process by generating hundreds of contrasts obtained from soot particle diffraction experiments

    Sensing the wavefront of x-ray free-electron lasers using aerosol spheres

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    Characterizing intense, focused x-ray free electron laser (FEL) pulses is crucial for their use in diffractive imaging. We describe how the distribution of average phase tilts and intensities on hard x-ray pulses with peak intensities of 10^21 W/cm^2 can be retrieved from an ensemble of diffraction patterns produced by 70 nm-radius polystyrene spheres, in a manner that mimics wavefront sensors. Besides showing that an adaptive geometric correction may be necessary for diffraction data from randomly injected sample sources, our paper demonstrates the possibility of collecting statistics on structured pulses using only the diffraction patterns they generate and highlights the imperative to study its impact on single-particle diffractive imaging
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