Playing with fire: Exploring ceramic pyrotechnology in the Late Neolithic Balkans through an archaeometric and experimental approach

Addressing ceramic pyrotechnology plays a key role in understanding a wide range of cultural and social behaviours associated to pottery production. Firing is the process which transforms clay into ceramic, which is one of the most frequently preserved materials in the majority of Neolithic and later archaeological sites. Though firing temperatures and the functions of various pyrotechnological installations have been extensively investigated in archaeology, both have often been addressed separately. Most of our knowledge on firing structures and procedures in the Neolithic are still largely based on ethnoarchaeological evidence. To move forward, we need to consider all aspects involved in ancient pyrotechnology, together with use of additional investigative tools. This study aims to address Neolithic pottery firing from a diverse perspective that merges archaeometric analyses and experimental archaeology. To demonstrate the potential of this approach, we combined an archaeometric case study of pottery from the late Neolithic (5200–4800 BCE) from the site of Gradište-Iđjoš (Serbia) with experimental pit firings, likely one of the mostly frequently employed firing techniques used in prehistoric periods. Scientific analyses include X-ray powder diffraction (XRPD), scanning electron microscopy (SEM), and ceramic petrography. These methods were run on both archaeological materials and experimental reproductions. Additionally, a detailed program of firing temperature monitoring, integrated observations on atmospheric conditions, soaking time, and duration were recorded to contribute to the study. The experiments enabled us to collect results useful for our understanding of the pyrotechnological knowledge of Neolithic potters from a technological and social point of view. In addition, they demonstrated the potential of a dedicated methodological framework for studying pottery firing that can be applied to other chronological and cultural contexts

An interdisciplinary approach to the study of kiln firing: a case study from the Campus Galli open-air museum (southern Germany)

Pottery kilns are a common feature in the archaeological record of different periods. However, these pyrotechnological installations are still seldom the target of interdisciplinary investigations. To fill this gap in our knowledge, an updraft kiln firing experiment was run at the Campus Galli open-air museum (southern Germany) by a team consisting of experimental archaeologists, material scientists, geoarchaeologists, and palaeobotanists. The entire process from the preparation of the raw materials to the firing and opening of the kiln was carefully recorded with a particular focus on the study of the raw materials used for pottery making, as well as on fuel usage. The temperatures were monitored by thermocouples placed at different positions in the combustion and firing chambers. In addition, thermocouples were installed within the kiln wall to measure the temperature distribution inside the structure itself. Unfired raw materials as well as controlled and experimentally thermally altered ceramic samples were then characterised with an integrated analysis including ceramic petrography, X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), and portable X-ray fluorescence (pXRF). Our work provides data about mineralogical and microstructural developments in both pottery kiln structures and the ceramics produced in this type of installations. This is helpful to discuss the limits and potential of various scientific analyses commonly used in ancient ceramic pyrotechnological studies. Overall, our work contributes to a better understanding of updraft kiln technology and offers guidelines on how to address the study of this type of pyrotechnological installations using interdisciplinary research strategies

Study of two-dimensional photonic crystals cavity using organic gain materials

International audienc

Study of two-dimensional photonic crystals cavity using organic gain materials

International audienc