Superconducting properties of MgB2 thin films prepared on flexible plastic substrates

Superconducting MgB2 thin films were prepared on 50-micrometer-thick, flexible polyamide Kapton-E foils by vacuum co-deposition of Mg and B precursors with nominal thickness of about 100 nm and a special ex-situ rapid annealing process in an Ar or vacuum atmosphere. In the optimal annealing process, the Mg-B films were heated to approximately 600 C, but at the same time, the backside of the structures was attached to a water-cooled radiator to avoid overheating of the plastic substrate. The resulting MgB2 films were amorphous with the onset of the superconducting transition at T_(c,on) about 33 K and the transition width of approximately 3 K. The critical current density was > 7x10^5 A/cm^2 at 4.2 K, and its temperature dependence indicated a granular film composition with a network of intergranular weak links. The films could be deposited on large-area foils (up to 400 cm^2) and, after processing, cut into any shapes (e.g., stripes) with scissors or bent multiple times, without any observed degradation of their superconducting properties.Comment: 3 figure

Phonons in MgB2 by Polarized Raman Scattering on Single Crystals

The paper presents detailed Raman scattering study of the unusually broad E2g phonon mode in MgB2 crystal. For the first time, it is shown by the polarized Raman scattering on few-micron-size crystallites with natural faces that the observed broad Raman feature really does obey the selection rules of an E2g mode. Raman spectra on high quality polycrystalline superconducting MgB2 wires reveal a very symmetric E2g phonon line near 615 1/cm with the room temperature linewidth of 260 1/cm only. Additional scattering of different polarization dependence, observed in certain crystallites is interpreted as weighted phonon density of states induced by lattice imperfections.Comment: 4 pages + 7 figure

Time-resolved dynamics of the superconducting two-gap state in MgB2 thin films

Femtosecond pump-probe studies show that carrier dynamics in MgB2 films is governed by the sub-ps electron-phonon (e-ph) relaxation present at all temperatures, the few-ps e-ph process well pronounced below 70 K, and the sub-ns superconducting relaxation below Tc. The amplitude of the superconducting component versus temperature follows the superposition of the isotropic dirty gap and the 3-dimensional gap dependences, closing at two different Tc values. The time constant of the few-ps relaxation exhibits a double-divergence at temperatures corresponding to the Tc's of the two gaps.Comment: Accepted for publication in Phys.Rev.Let

In situ annealing of superconducting MgB2 films prepared by pulsed laser deposition

The in situ annealing conditions of pulsed laser deposited MgB2 films were studied. The precursor films were deposited at 250 C from a stoichiometric MgB2 target in a 120mTorr Ar atmosphere. The films were then in situ annealed at a temperature from 450 C to 800 C and an annealing time from 1 minute to 10 minutes. We found that the superconducting properties depend in a crucial way on the annealing conditions: temperature, heating rate and time. The best film with a thickness of ~600nm was obtained under the following annealing conditions: Tanneal=680-690 C, tanneal=1 min, heating rate= 38 C/min. The Tc onset of the film is 28K with a transition width of ~10K. The hysteresis loop of magnetic moment of the film indicates weak field dependence in high fields. Magneto-optical imaging of the film showed quite homogeneous magnetic flux penetration, indicating structural homogeneity. The films without annealing showed no superconductivity.Comment: 12 pages, 6 figure

Transport Behavior of Commercially Available 100-Ω Standard Resistors

Several types of commercial 100-Ω resistors can be used with the cryogenic current comparator to maintain the resistance unit, derived from the quantized Hall effect (QHE), and to disseminate this unit to laboratory resistance standards. Up until now, the transport behavior of these resistors has not been investigated. Such an investigation is of importance for carrying out comparisons that are close to the level of a direct comparison of two QHE apparatuses. A set of five 100-Ω resistors from three different manufacturers has been sent to 11 participating national metrological institutes. All laboratories but one have measured the resistors based on their laboratory's quantized Hall resistance measurements. A constant drift model has been applied, and the results are evaluated in such a way that the transport properties of these resistors are treated independently for the different types of resistor. Under certain conditions, these resistors allow comparisons with uncertainties better than 1 part in 108