512 research outputs found
DEVELOPING THE METHODS OF FOOD PRESERVATIVES EXTRACTION FROM COMPLEX MATRICES FOR BIOASSAY PURPOSE
The presence of food additives in food products may be associated with the risk of their toxic effects on human body. Therefore, the study of approaches to testing their safety seems to be a particularly urgent task. The aim of this study was to determine the conditions for extracting food preservatives from the samples of preserved pureed vegetables for further bioassay of the extract obtained in the Allium test. Onion roots were used as a test object in this method. Two extraction methods of benzoic and sorbic acids added to pureed vegetables have been developed. Distilled water and acetone were used as extracting solutions. The extraction efficiency was evaluated on Shimadzu Prominence LC-20 liquid chromatograph (Japan) in the ultraviolet range, wavelength 235 nm (benzoic acid), 285 nm (sorbic acid). According to the results of studies using both water and acetone as extractants, the degree of preservatives extraction was approximately the same and quite high. In the quantitative calculation of the preservatives content in pureed vegetables, the value of the correction factor was 0.8. However, due to certain production characteristics of this product, i. e. the stage of cauliflower homogenization, obtaining an extract with acetone seems to be more acceptable for the Allium test conditions.The presence of food additives in food products may be associated with the risk of their toxic effects on human body. Therefore, the study of approaches to testing their safety seems to be a particularly urgent task. The aim of this study was to determine the conditions for extracting food preservatives from the samples of preserved pureed vegetables for further bioassay of the extract obtained in the Allium test. Onion roots were used as a test object in this method. Two extraction methods of benzoic and sorbic acids added to pureed vegetables have been developed. Distilled water and acetone were used as extracting solutions. The extraction efficiency was evaluated on Shimadzu Prominence LC-20 liquid chromatograph (Japan) in the ultraviolet range, wavelength 235 nm (benzoic acid), 285 nm (sorbic acid). According to the results of studies using both water and acetone as extractants, the degree of preservatives extraction was approximately the same and quite high. In the quantitative calculation of the preservatives content in pureed vegetables, the value of the correction factor was 0.8. However, due to certain production characteristics of this product, i. e. the stage of cauliflower homogenization, obtaining an extract with acetone seems to be more acceptable for the Allium test conditions
Sterile neutrino and dark matter
We consider the equation that describes the dynamics of the sterile neutrino
density in primeval plasma. The analysis of this equation results in the 5%
contribution of the sterile neutrino with mixing parameters and to the energy density of the
Universe. The considered parameters of the sterile neutrino correspond to the
warm dark matter.Comment: 7 pages, 11 figure
Infrared studies of a La_(0.67)Ca_(0.33)MnO_3 single crystal: Optical magnetoconductivity in a half-metallic ferromagnet
The infrared reflectivity of a La_(0.67)Ca_(0.33)MnO_3 single crystal is studied over a broad range of temperatures (78–340 K), magnetic fields (0–16 T), and wave numbers (20–9000cm^(-1)). The optical conductivity gradually changes from a Drude-like behavior to a broad peak feature near 5000cm-1 in the ferromagnetic state below the Curie temperature T_C=307K. Various features of the optical conductivity bear striking resemblance to recent theoretical predictions based on the interplay between the double exchange interaction and the Jahn-Teller electron-phonon coupling. A large optical magnetoconductivity is observed near T_C
Infrared Studies of a La_{0.67}Ca_{0.33}MnO_3 Single Crystal: Optical Magnetoconductivity in a Half-Metallic Ferromagnet
The infrared reflectivity of a single crystal
is studied over a broad range of temperatures (78-340 K), magnetic fields (0-16
T), and wavenumbers (20-9000 cm). The optical conductivity gradually
changes from a Drude-like behavior to a broad peak feature near 5000 cm
in the ferromagnetic state below the Curie temperature . Various
features of the optical conductivity bear striking resemblance to recent
theoretical predictions based on the interplay between the double exchange
interaction and the Jahn-Teller electron-phonon coupling. A large optical
magnetoconductivity is observed near .Comment: 4 pages, 4 figures, Latex, PostScript; The 7th Joint MMM-Intermag
Conference,San Francisco, January 6-9, 1998; The Int. Conf. on Strongly
Correlated Electron Systems, Paris, July 15-18,199
Steps in the Negative-Differential-Conductivity Regime of a Superconductor
Current-voltage characteristics were measured in the mixed state of
Y1Ba2Cu3O(7-delta) superconducting films in the regime where flux flow becomes
unstable and the differential conductivity dj/dE becomes negative. Under
conditions where its negative slope is steep, the j(E) curve develops a
pronounced staircase like pattern. We attribute the steps in j(E) to the
formation of a dynamical phase consisting of the succesive nucleation of
quantized distortions in the local vortex velocity and flux distribution within
the moving flux matter.Comment: 5 pages, 3 figure
Defect-unbinding and the Bose-glass transition in layered superconductors
The low-field Bose-glass transition temperature in heavy-ion irradiated
Bi_2Sr_2CaCu_2O_8+d increases progressively with increasing density of
irradiation-induced columnar defects, but saturates for densities in excess of
1.5 x10^9 cm^-2. The maximum Bose-glass temperature corresponds to that above
which diffusion of two-dimensional pancake vortices between different vortex
lines becomes possible, and above which the ``line-like'' character of vortices
is lost. We develop a description of the Bose-glass line that is in excellent
quantitative agreement with the experimental line obtained for widely different
values of track density and material parameters.Comment: 4 pages, 4 figures, submitted to Phys. Rev. Let
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