4,823 research outputs found

    Spectral studies of some hydroxy-derivatives of anthraquinones

    Get PDF
    The u.v., visible, and i.r. spectra of several hydroxy-anthraquinones are discussed and the bands are assigned. These bands are compared with those of anthracene and anthraquinone. The band at 207 nm. is assigned to a n-sigma* transition; the bands at 252, 272, and 326 nm. are assigned by measuring spectra in solvents of various polarities. The stability constant for the 12-dihydroxyanthraquinone-ethanol complex is obtained

    Značajke građe i optička svojstava otpuštenih tankih slojeva cdin2se4

    Get PDF
    CdIn2Se4 chalcogenides thin films were prepared by thermal evaporation process. The effect of thermal annealing in vacuum on the growth characteristics of the deposited films was studied using X-ray and transmission electron microscopy techniques. It was observed that the as deposited films (300 K) were poorly crystalline. The degree of crystallinity increases with increasing the annealing temperature from 300 to 500 K. The compositional elemental analysis of CdIn2Se4 thin films annealed at 500 K was found to be nearly stoichiometric, however, films annealed in vacuum at 575 K partially dissociated into two binary phases with CdIn2Se4 as the major phase. The effect of the annealing temperature on the dispersion of the refractive index of the deposited films was investigated and analyzed within the single effective-oscillator approach. Changes of the dispersion parameters were also investigated as a function of the annealing temperature. Analysis of the optical absorption data revealed the existence of allowed direct and indirect optical transitions, and both values of energy gaps decrease with increasing annealing temperature.Isparavanjem u vakuumu pripremali smo tanke slojeve halkogenida CdIn2Se4. Proučavali smo učinke toplinskog otpuštanja u vakuumu na strukturne značajke naparenih slojeva primjenom difrakcije X-zračenja i prolazne elektronske mikroskopije. Opaža se da su svježe (na 300 K) napareni slojevi slabo kristalinični. Stupanj kristaliničnosti povećava se s povišenjem temperature otpuštanja između 300 i 500 K. Analize elementalnog sastava tankih slojeva CdIn2Se4 otpuštenih do 500 K pokazale su gotovo točan stoihiometrijski sastav, međutim, slojevi otpušteni na 575 K djelomično se razlažu u dvije binarne faze, dok CdIn2Se4 ostaje glavna faza. Mjerili smo učinke otpuštanja na disperzivnost indeksa loma naparenih slojeva i analizirali ishode jedno-oscilatornim modelom. Promjene parametara disperzije također smo istraživali u ovisnosti o temperaturi otpuštanja. Analize podataka za optičku apsorpciju ukazuju na postojanje dozvoljenih izravnih i neizravnih optičkih prijelaza s padom širina procijepa za povećne temperature otpuštanja

    Značajke građe i optička svojstava otpuštenih tankih slojeva cdin2se4

    Get PDF
    CdIn2Se4 chalcogenides thin films were prepared by thermal evaporation process. The effect of thermal annealing in vacuum on the growth characteristics of the deposited films was studied using X-ray and transmission electron microscopy techniques. It was observed that the as deposited films (300 K) were poorly crystalline. The degree of crystallinity increases with increasing the annealing temperature from 300 to 500 K. The compositional elemental analysis of CdIn2Se4 thin films annealed at 500 K was found to be nearly stoichiometric, however, films annealed in vacuum at 575 K partially dissociated into two binary phases with CdIn2Se4 as the major phase. The effect of the annealing temperature on the dispersion of the refractive index of the deposited films was investigated and analyzed within the single effective-oscillator approach. Changes of the dispersion parameters were also investigated as a function of the annealing temperature. Analysis of the optical absorption data revealed the existence of allowed direct and indirect optical transitions, and both values of energy gaps decrease with increasing annealing temperature.Isparavanjem u vakuumu pripremali smo tanke slojeve halkogenida CdIn2Se4. Proučavali smo učinke toplinskog otpuštanja u vakuumu na strukturne značajke naparenih slojeva primjenom difrakcije X-zračenja i prolazne elektronske mikroskopije. Opaža se da su svježe (na 300 K) napareni slojevi slabo kristalinični. Stupanj kristaliničnosti povećava se s povišenjem temperature otpuštanja između 300 i 500 K. Analize elementalnog sastava tankih slojeva CdIn2Se4 otpuštenih do 500 K pokazale su gotovo točan stoihiometrijski sastav, međutim, slojevi otpušteni na 575 K djelomično se razlažu u dvije binarne faze, dok CdIn2Se4 ostaje glavna faza. Mjerili smo učinke otpuštanja na disperzivnost indeksa loma naparenih slojeva i analizirali ishode jedno-oscilatornim modelom. Promjene parametara disperzije također smo istraživali u ovisnosti o temperaturi otpuštanja. Analize podataka za optičku apsorpciju ukazuju na postojanje dozvoljenih izravnih i neizravnih optičkih prijelaza s padom širina procijepa za povećne temperature otpuštanja

    Observation of anisotropic diamagnetism above the superconducting transition in iron-pnictide Ba_(1-x)K_xFe2As2 single crystals due to thermodynamic fluctuations

    Full text link
    High resolution magnetization measurements performed in a high quality Ba_(1-x)K_xFe2As2 single crystal allowed to determine the diamagnetism induced above the superconducting transition by thermally activated Cooper pairs. These data, obtained with magnetic fields applied along and transverse to the crystal ab layers, demonstrate experimentally that the superconducting transition of iron pnictides may be explained at a phenomenological level in terms of the Gaussian Ginzburg-Landau approach for three-dimensional anisotropic superconductors.Comment: Final version with minor corrections. 6 pages, 4 figure

    Numeralia Bahasa Melayu Dialek Kapuas Hulu

    Get PDF
    : This study aims to examine and analyze numeralia Malay language used in the village Nibung Selimbau District of Kapuas Hulu. Aspects studied and analyzed from the numerali is the form, function and meaning numeralia Malay. The method used in this research is descriptive qualitative research methods. Data collection techniques used are fishing techniques and techniques semuka face. From the data obtained it can be concluded form BMDKH numeralia consists of numeralia monomorfemis and polimorfemis. BMDKH numeralia function in units of syntax can fill some syntactic function, among others, the subjective function, serves predicate, object function, and function information. Numeralia meaning BMDKH consists of a prefix meaning numeralia to-stated meaning or collective collection and express the meaning of the order, meaning numeralia with all prefixes declared collective or group, with a prefix meaning BE- numeralia states collectively or collection
    corecore