1,680 research outputs found
AC VS. DC flash sintering: Influence of field frequency on flash processes
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A comparative study of magnetic and electrical properties of BiFeO3 mutiferroic ceramics sintered by electric field assisted-methods: Spark plasma sintering and flash sintering
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Multi-Phase Flash Sintering: The Next Natural Step in Flash Sintering Evolution
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Effect of reactive flash sintering on the magnetic and hyperfine parameters of SrFe12O19 ceramic permanent magnets
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Electrical properties of stoichiometric BiFeO3 prepared by mechanosynthesis with either conventional or spark plasma sintering
Phase-pure powders of stoichiometric BiFeO3 have been prepared by mechanosynthesis. Ceramics sintered by either conventional heating in air or spark plasma sintering (SPS) followed by oxidative anneal in air are highly insulating with conductivity e.g. ~10–6 Scm–1 at 300 °C and activation energy 1.15(2) eV, which are comparable to those of a good-quality BiFeO3 single crystal. By contrast, the as-prepared SPS sample without the post-sinter anneal shows higher conductivity e.g. ~10–6 Scm–1 at 225 °C and lower activation energy 0.67(3) eV, indicating some reduction of the sample by the SPS process. The reason for the high conductivity observed in some ceramic samples reported in the literature appears to be unclear at presentGobierno de España CTQ 2011-27626 MAT 2008-06619Junta de Andalucia TEP-0300
Reactive Flash Sintering of High Entropy (Mn0.2Co0.2Ni0.2Cu 0.2X 0.2)Fe2O4 (X=Fe, Mg) Spinel Oxides
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Quantitative characterization of multicomponent polymers by sample-controlled thermal analysis
This paper explores the potential of sample-controlled thermal analysis (SCTA) in order to perform compositional analysis of multicomponent polymeric materials by means of thermogravimetric experiments. In SCTA experiments, the response of the sample to the temperature determines the evolution of the temperature by means of a feedback system; thus, what is controlled is not the temperature-time profile, as in conventional analysis, but rather the evolution of the reaction rate with time. The higher resolving power provided by the technique has been used for determining the composition of polymer blends composed of polyvinyl chloride (PVC) and different commercial plasticizers, a system where the individual components have very similar thermal stabilities, thereby rendering useless thermogravimetric experiments run under conventional conditions. Different SCTA procedures, such as constant rate thermal analysis (CRTA), which has received special attention, and high-resolution and stepwise isothermal analysis have been tested, and the results obtained have been compared with linear heating rate technique. It has been proven that CRTA can be used to effectively determine the exact composition of the blend.Junta de Andalucía TEP-03002Ministerio de Ciencia e Innovación MAT 2008- 06619/MA
Reactive Flash Sintering
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Detection of dengue virus serotype 2 in aedes aegypti in Quintana Roo, Mexico, 2011
Abstract. In October 2011, the State Health Department announced that several laboratory-confirmed cases of dengue had occurred among residents in two neighborhoods of Benito Juarez, Quintana Roo State, Mexico. To identify the dengue virus serotype(s) temporally and spatially associated with the cases, entomologic-based virus surveillance was initiated in October 2011 in both
neighborhoods. Adult mosquitoes were collected from 88 houses by CDCbackpack aspirator, and all female Aedes aegypti L. (n = 419) were individually homogenized and assayed in pools of as many as 10 by reverse transcriptionpolymerase chain reaction (RT-PCR) using dengue virus-specific primers. Five (12%) of 41 pools were positive for dengue virus RNA. The individual mosquitoes that comprised the pools were analyzed separately by RT-PCR using dengue virus serotype-specific primers. Six mosquitoes were positive for dengue virus serotype-2 (DENV-2) RNA, three of which were collected in the same house. The mean number of female Ae. aegypti collected in each house was 4.76 ± 6.19. The overall
dengue virus-infection rate in female Ae. aegypti was 1.4%. Interestingly, most (60%) of mosquito females were collected only from 15 (17%) houses. In summary,
we provide evidence of recent DENV-2 transmission in Quintana Roo State
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