Grain boundary character distribution derived from three-dimensional microstructure reconstruction

Manual serial sectioning which includes consecutive steps of sample preparation and Electron Back Scattering Diffraction (EBSD) measurement was employed to extract the twodimensional (2D) sections of a pure nickel sample and to reconstruct the three-dimensional (3D) microstructure. A general alignment algorithm based on the minimization of misorientation between two adjacent sections has been developed to accurately align the sections. By employing this alignment algorithm, any in-plane (translational) and rotational misalignment as well as the planparallelity can be corrected. Surface triangulation technique was used to reconstruct the grain boundary surfaces. The Grain Boundary Character Distribution (GBCD) was derived from reconstructed grain boundaries. The results show that a smoother grain boundary plane can be obtained after precise translational and rotational alignment and correction of planparallelity. The relative grain boundary energy was computed as a function of the five grain boundary parameters based on equilibrium at triple lines. The results show that the grain boundary planes carrying a ?3 type misorientation are dominantly parallel to the {111} crystal plane, which indicates the presence of coherent twin boundaries. It was observed that coherent ?3 type boundaries exhibit the minimum relative grain boundary energy, which is approximately 57% smaller than the average of all ?3 boundaries, including also incoherent twin boundaries.Materials Science and EngineeringMechanical, Maritime and Materials Engineerin

Quantitative correlation between slip patterning and microstructure during tensile elongation in 6xxx series aluminum alloy

To the purpose of evaluating the effect of deformation on the microstructure, aluminum structures were analyzed on tensile strained samples extended to 25% elongation. In the substructure of these deformed samples linear slip patterns were observed, generally confined to the bulk of the grain. In order to study the crystallographic aspect of these slip patterns, two methods were applied based on orientation contrast microscopy (EBSD). The first method is the statistical analysis of stereological nature, which allows us to determine the incidence of certain crystallographic planes with the slip patterns. In other to corroborate the statistical method, also a 3D analysis was carried out on two perpendicular planes of observation (TD and ND sections). The results of both methods were in a very good agreement. It was found that the linear features are predominantly parallel to the {111} crystal planes, although the frequency of {111} planes was not exclusive; also other crystal planes such as {112} and {110} are involved. These observations give a stronger statistical basis for similar observations earlier made by TEM on much smaller fields of observation.Materials Science and EngineeringMechanical, Maritime and Materials Engineerin

Three-dimensional characterization of grain boundaries in pure nickel by serial sectioning via mechanical polishing

Five macroscopic boundary parameters can be extracted from three-dimensional orientation maps. Serial sectioning, which includes consecutive steps of material removal, and electron backscatter diffraction (EBSD) measurement were employed to extract a stack of two-dimensional sections of a pure nickel sample. The EBSD patterns were collected from large millimetre scale areas and mechanical polishing was applied to prepare the sections. The three-dimensional microstructure was then reconstructed from these sections. A new alignment algorithm based on the minimization of misorientation between two adjacent sections has been developed to accurately align the sections. Differently from the conventional alignment methods, the new algorithm corrects not only the translational misalignment but also rotational and plane parallelity misalignments. The aligned three-dimensional microstructure exhibits smooth grain boundary planes and continuous orientation gradients inside the grains as experimental scatter induced by misalignment was largely removed. Grain boundaries were reconstructed from the aligned three-dimensional map, and the distribution of boundaries in the domain of five acroscopic boundary parameters was computed using kernel density estimation. Methods for estimating the reliability of the distributions are demonstrated. This distribution is compared with the distributions obtained previously for other face-centered cubic materials, including a different pure nickel sample.Materials Science and EngineeringMechanical, Maritime and Materials Engineerin

On the bending of MS1-P20 hybrid steels additively manufactured using laser powder bed fusion

Maraging steel (MS1)-tool steel (P20) bimetals additively manufactured using the laser powder bed fusion technique were studied under different heat treatment cycles and loading conditions. The hardening of P20 and aging of MS1 were performed sequentially on the hybrid samples. The interfacial characteristics and microstructural evolution of the bulk materials were studied using various advanced electron microscopy techniques. The post-processing procedures successfully produced a uniform martensitic structure throughout the MS1-P20 hybrid steels, leading to a less detectable interface under electron backscatter diffraction (EBSD) imaging. The mechanical performance of heat-treated hybrid steels was evaluated using complex loading conditions. 3-point and 4-point bending tests were performed to assess the impact of heat treatments on the mechanical performance of the hybrid steels. The heat-treated samples exhibited higher strength with relatively homogeneous hardness variations and deformed more uniformly in bending conditions.Green Open Access added to TU Delft Institutional Repository 'You share, we take care!' - Taverne project https://www.openaccess.nl/en/you-share-we-take-care Otherwise as indicated in the copyright section: the publisher is the copyright holder of this work and the author uses the Dutch legislation to make this work public.Team Jilt Sietsm

Additive manufactured versus cast AlSi10Mg alloy: Microstructure and micromechanics

This study aims at assessing the effect of solution heat treatment (at a temperature just below the eutectic temperature) followed by various cooling rates on the microstructure and mechanical properties of additively manufactured AlSi10Mg and the cast counterpart. The mechanical properties were evaluated using a depth-sensing nanoindentation platform. The cast and additively manufactured parts were solutionized at 540 ​°C for 2 ​h followed by water quenching, air cooling, and furnace cooling. Results show extensive microstructural changes (e.g. size and morphology of eutectic-silicon phase) and evolutions in the mechanical properties of the heat-treated materials relative to the as-printed and as-cast ones. Besides, the microstructure and micromechanical properties of the materials broadly alter the cast and additive manufacturing conditions. Depending on the cooling condition, the mentioned cooling cycles directly affect the morphology of eutectic-silicon in both cast and additive manufactured materials starting with silicon fragmentation, then followed by silicon spheroidization, and silicon coarsening. The microstructural evolution affects the local micromechanical properties of the studied materials. The results of this study provide insights into the control of microstructure and hence mechanical properties of AlSi10Mg alloy by addressing suitable heat treatment cycles. This study, for the first time, assesses and compares the effect of various post-fabrication cooling rates in the cast and additive manufacturing conditions in an AlSi10Mg alloy.Team Jilt Sietsm

High strain rate torsional response of maraging steel parts produced by laser powder bed fusion techniques: Deformation behavior and constitutive model

The deformation performance of maraging steel samples fabricated using the laser powder bed fusion technique was evaluated using the split Hopkinson torsion bar (SHTB) test. Thin-walled tubular maraging steel samples were deformed under dynamic torsional loading at strain rates of 260 s−1 to 720 s−1 using twist angles varying from 3 to 12°. Microstructural and textural investigations were carried out on deformed samples using the electron backscatter diffraction technique and scanning electron microscopy. Results showed that maraging steel samples fractured when deformed using an angle of twist of 12° and strain rate of 650 s−1. As a result of deformation localization at high strain rates, adiabatic shear bands are developed in some thin-walled tubular torsion specimens deformed using the 12-degree angle of twist, leading to fracture. Textural studies showed that texture weakening occurred with an increment in strain rate ascribable to grain fragmentation. In this study, two models (empirically and semi-empirically) were employed for describing maraging steel performance during high strain-rate torsional loading. Simulation results based on Kobayashi-Odd and Nemat-Nasser models agreed well with the experimental data.Green Open Access added to TU Delft Institutional Repository 'You share, we take care!' - Taverne project https://www.openaccess.nl/en/you-share-we-take-care Otherwise as indicated in the copyright section: the publisher is the copyright holder of this work and the author uses the Dutch legislation to make this work public.Team Jilt Sietsm

Microstructural Evolution in Additively Manufactured Fe-Cr-Ni Maraging Stainless Steel

In this work, the effect of heating rate on the phase transformation temperatures was investigated using dilatometry analysis. Continuous heating and isothermal holding above Ac3 temperature on microstructural evolutions in additively manufactured (AM) parts of Fe-Cr-Ni maraging stainless steel were studied. The microstructural features developed within the heating processes were characterized employing electron backscatter diffraction and transmission electron microscopy. Austenite reversion was found to take place in two steps for the AM parts by a diffusive mechanism as well as the precipitation reactions. Although grain refinement occurred during the austenite reversion of the continuously heated samples, the microstructure showed a coarser grain size after isothermal heating. The crystallographic orientations developed after the heating processes were different from those of the initial ones implying the absence of the austenite memory effect.Green Open Access added to TU Delft Institutional Repository 'You share, we take care!' - Taverne project https://www.openaccess.nl/en/you-share-we-take-care Otherwise as indicated in the copyright section: the publisher is the copyright holder of this work and the author uses the Dutch legislation to make this work public.Team Jilt Sietsm