Influence of the position and size of various deterministic defects on the high cycle fatigue resistance of a 316L steel manufactured by laser powder bed fusion

Optimized 316L steel samples were manufactured using laser powder bed fusion and tested in high cycle fatigue at R = 0.1. They showed microstructural crack initiation and outstanding fatigue properties. Additional fatigue testings were then carried out on samples containing deterministic defects of various sizes and positions. All results summarized in a Kitagawa-Takahashi diagram show that the critical defect size is around 20 µm for surface defects and reach 380 µm for internal pores. Fracture surface analysis revealed that the large size gap between surface and internal fatigue crack initiation could be linked to the local gaseous environment in the pores.This work was financially supported by the CEA List, the PIMM laboratory, the I2M laboratory and the LAMPA laboratory in France

Simplified numerical model for the laser metal deposition additive manufacturing process

The laser metal deposition (LMD) laser technique is a free-form metal deposition process, which allows generating near net-shape structures through the interaction of a powder stream and a laser beam. A simplified numerical model was carried out to predict layer heights together with temperature distributions induced by the (LMD) process on a titanium alloy, and a metal matrix composite. Compared with previously developed models, this simplified approach uses an arbitrary Lagrangian Eulerian free surface motion directly dependent on the powder mass feed rate Dm. Considering thin wall builds of Ti-6Al-4V titanium alloy, numerical results obtained with comsol 4.3 Multiphysics software were successfully compared with the experimental data such as geometrical properties of manufactured walls, fast camera molten pools measurements, and thermocouple temperature recordings in the substrate during the manufacturing of up to 10 LMD. Even if the model did not consider coupled hydraulic-thermal aspects, it provides a more realistic local geometrical description of additive layer manufacturing walls than simpler thermal models, with much shorter calculation times than more sophisticated approaches considering thermocapillary fluid flow. In a second step, microstructures (equiaxed or columnar) were predicted on Ti-6Al-4V walls using microstructural map available in the literature, and local thermal gradients G (K/m) and solidification rate R (m/s) provided by the FE calculation near the solidification front. © 2017 Laser Institute of America

Influence of Anodized Titanium Surfaces on the Behavior of Gingival Cells in Contact with: A Systematic Review of In Vitro Studies

Electrochemically anodized (EA) surfaces promise enhanced biological properties and may be a solution to ensure a seal between peri-implant soft tissues and dental transmucosal components. However, the interaction between the modified nano-structured surface and the gingival cells needs further investigation. The aim of this systematic review is to analyze the biological response of gingival cells to EA titanium surfaces in in vitro studies with a score-based reliability assessment. A protocol aimed at answering the following focused question was developed: “How does the surface integrity (e.g., topography and chemistry) of EA titanium influence gingival cell response in in vitro studies?”. A search in three computer databases was performed using keywords. A quality assessment of the studies selected was performed using the SciRAP method. A total of 14 articles were selected from the 216 eligible papers. The mean reporting and the mean methodologic quality SciRAP scores were 87.7 ± 7.7/100 and 77.8 ± 7.8/100, respectively. Within the limitation of this review based on in vitro studies, it can be safely speculated that EA surfaces with optimal chemical and morphological characteristics enhance gingival fibroblast response compared to conventional titanium surfaces. When EA is combined with functionalization, it also positively influences gingival epithelial cell behavior

Analysis of As-Built Microstructures and Recrystallization Phenomena on Inconel 625 Alloy Obtained via Laser Powder Bed Fusion (L-PBF)

The microstructures induced by the laser-powder bed fusion (L-PBF) process have been widely investigated over the last decade, especially on austenitic stainless steels (AISI 316L) and nickel-based superalloys (Inconel 718, Inconel 625). However, the conditions required to initiate recrystallization of L-PBF samples at high temperatures require further investigation, especially regarding the physical origins of substructures (dislocation densities) induced by the L-PBF process. Indeed, the recrystallization widely depends on the specimen substructure, and in the case of the L-PBF process, the substructure is obtained during rapid solidification. In this paper, a comparison is presented between Inconel 625 specimens obtained with different laser-powder bed fusion (L-PBF) conditions. The effects of the energy density (VED) values on as-built and heat-under microstructures are also investigated. It is first shown that L-PBF specimens created with high-energy conditions recrystallize earlier due to a larger density of geometrically necessary dislocations. Moreover, it is shown that lower energy densities offers better tensile properties for as-built specimens. However, an appropriate heat treatment makes it possible to homogenize the tensile properties

Optimization and comparison of porosity rate measurement methods of Selective Laser Melted metallic parts

The systematic occurrence of porosities inside selective laser melted (SLM) parts is a well-known phenomenon. In order to improve the density of SLM parts, it is important not only to assess the physical origin of the different types of porosities, but also to be able to measure as precisely as possible the porosity rate so that one may select the optimum manufacturing parameters. Considering 316 L steel parts built with different input energies, the current paper aims to (1) present the different types of porosities generated by SLM and their origins, (2) compare different methods for measuring parts density and (3) propose optimal procedures. After a preliminary optimization step, three methods were used for quantifying porosity rate: the Archimedes method, the helium pycnometry and micrographic observations. The Archimedes method shows that results depend on the nature and temperature of the fluid, but also on the sample volume and its surface roughness. During the micrographic observations, it has been shown that the results depend on the magnification used and the number of micrographs considered. A comparison of the three methods showed that the optimized Archimedes method and the helium pycnometry technique gave similar results, whereas optimized micrographic observations systematically underestimated the porosity rate. In a second step, samples were analyzed to illustrate the physical phenomena involved in the generation of porosities. It was confirmed that: (1) low Volume Energy Density (VED) causes non-spherical porosities due to insufficient fusion, (2) in intermediary VED the small amount of remaining blowhole porosities come from gas occlusion in the melt-pool and (3) in excessive VED, cavities are formed due to the key-hole welding mode

Additive layer manufacturing of titanium matrix composites using the direct metal deposition laser process

Titanium Matrix Composites (TMC's) containing various volume fractions of (TiB+TiC) particles have been deposited from powder feedstocks consisting of a blend of pre-alloyed (Ti-6Al-4V+B4C) powders, using the direct metal deposition (DMD) laser process and the in-situ chemical reaction 5Ti+B4C→4TiB+TiC. Process optimization has allowed to obtain a homogeneous distribution of tiny TiB whiskers within the Ti-6Al-4V α/β matrix, with a full solubilization of C for low B4C contents (0.5 wt% and 1.5 wt%), and the formation of a small amount of globular TiC particles at higher B4C content (3%). Comparisons with Ti-6Al-4V DMD walls revealed a substantial grain refinement on TMC's due to enhanced grain nucleation on TiB whiskers, even for low B4C contents. Last, mechanical investigations indicated an increase of 10–15% of Vickers hardness, and a constant 10% increase of Young modulus on a large temperature range (20–600 °C) for all B4C conten

Phase II study of mTORC1 inhibition by everolimus in neurofibromatosis type 2 patients with growing vestibular schwannomas

Neurofibromatosis type 2 (NF2) is a genetic disorder with bilateral vestibular schwannomas (VS) as the most frequent manifestation. Merlin, the NF2 tumor suppressor, was identified as a negative regulator of mammalian target of rapamycin complex 1. Pre-clinical data in mice showed that mTORC1 inhibition delayed growth of NF2-schwannomas. We conducted a prospective single-institution open-label phase II study to evaluate the effects of everolimus in ten NF2 patients with progressive VS. Drug activity was monitored every 3 months. Everolimus was administered orally for 12 months and, if the decrease in tumor volume was >20 % from baseline, treatment was continued for 12 additional months. Other patients stopped when completed 12 months of everolimus but were allowed to resume treatment when VS volume was >20 % during 1 year follow-up. Nine patients were evaluable. Safety was evaluated using CTCAE 3.0 criteria. After 12 months of everolimus, no reduction in volume ≥20 % was observed. Four patients had progressive disease, and five patients had stable disease with a median annual growth rate decreasing from 67 %/year before treatment to 0.5 %/year during treatment. In these patients, tumor growth resumed within 3-6 months after treatment discontinuation. Everolimus was then reintroduced and VS decreased by a median 6.8 % at 24 months. Time to tumor progression increased threefold from 4.2 months before treatment to > 12 months. Hearing was stable under treatment. The safety of everolimus was manageable. Although the primary endpoint was not reached, further studies are required to confirm the potential for stabilization of everolimus

PROPOSAL OF A HANDY SETUP FOR DISCRIMINATING PARASITIC EFFECTS FOR THE MEASUREMENT OF IMPULSIVE THRUST FROM A MICROWAVE CAVITY

International audienceThis paper details the work of the LAPLACE Electromagnetism Research Group to develop an original measuring setup dedicated to the detection of an EMDrive like force. Recent peer-reviewed experimental results [1, 2] were obtained using similar setups based on a torsion pendulum combined with an optical sensor. These very accurate measurement setups are appropriate for measuring such an extremely weak force. They also appear costly, which may discourage other research teams from working on this topic. Our main goal is then to provide an alternative configuration, based on a commercial precision balance, in order to build a measuring setup more affordable, handy, and accurate enough to measure an EMDrive like force. Our experimental system is capable of feeding a truncated cone shaped 2.45 GHz resonant cavity with power up to 140 W. To calibrate the EMDrive force and avoid false positive thrusts, an original setup has been proposed and evaluated. It allows us to really consider that the parasitic effects do not alter the hypothetical force measurement by the use of force direction switching during the measurement

STRAIGHTFORWARD EMDRIVE SETUP USING A MICROWAVE CONTACTLESS TRANSITION: FIRST RESULTS ON FRUSTUM CAVITIES

International audienc