Optimization of Selective Laser Sintering Process for Fabrication of Zirconium Diboride Parts

Selective Laser Sintering (SLS) was investigated to fabricate Zirconium Diboride (ZrB2) parts for ultra-high temperature applications. Experiments were conducted to determine values of SLS process parameters (laser power, scan speed, line spacing, and layer thickness) that can be used to build ZrB2 parts with high integrity and sharp geometrical features. A sacrificial plate with a proper number of layers (determined from experimentation) separated from the main part was built in order to reduce thermal gradients when building the main part. The sacrificial plate was found to assist in eliminating cracks in the bottom of the main part. The fabricated green parts then went through post processing steps including binder burnout and sintering at proper temperature schedules, to remove the binder and sinter the ZrB2 particles. The test bars after sintering had an average relative density of 87% and an average flexural strength of 250 MPa.Mechanical Engineerin

Investigation of selective laser sintering of zirconium diboride parts

This research investigates the fabrication of three-dimensional parts from ZrB₂, an ultra high temperature ceramic (UHTC), using the selective laser sintering (SLS) process. Based on an experimental investigation, optimum values for the SLS parameters (scan speed, laser power, energy density, scan spacing and layer thickness), used on a DTM Sinterstation 2000, were determined to build green ZrB₂ parts with high integrity and sharp geometrical features. This was done by melting the polymer binder used to bond the ceramic particles layer-by-layer according to the cross-section of a CAD model. The use of a sacrificial plate to eliminate cracks in the bottom of the part was demonstrated and the proper number of separation layers between the sacrificial plate and the main part was determined experimentally. The fabricated green parts went through post processing steps including binder burnout and sintering in furnaces at appropriate temperature schedules to remove the binder and sinter the ZrB₂ particles. Several test bars were fabricated and determined to have good properties with an average relative density of 87% and an average flexural strength of 250 MPa --Abstract, page iv

To entrepreneur or not to entrepreneur? How identity discrepancies influence enthusiasm for academic entrepreneurship

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Investigation of Laser Sintering for Freeform Fabrication of Zirconium Diboride Parts

This paper presents a study wherein the Laser Sintering (LS) process is used to perform additive manufacturing of zirconium diboride (ZrB2) parts. Experiments were conducted to determine values of LS process parameters (laser power, scan speed, energy density, line spacing, and layer thickness) that can be used to improve building of ZrB2 parts. A sacrificial plate with a proper number of layers was first constructed in order to reduce thermal gradients in building the main part. The sacrificial plate was found to eliminate cracks that would otherwise occur in the bottom of the main part. The fabricated green parts went through post-processing steps, including binder burnout and sintering at appropriate heat treatment schedules, to remove the binder and sinter the ZrB2 particles. The test bars after sintering had an average relative density of 87% and an average flexural strength of 250 MPa