1,172 research outputs found

    Hysteresis and relaxation of hard–soft nanocomposite samples

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    We present experimental results on the hysteresis and relaxation of Fe/Ba hexaferrite composite samples prepared by ball milling starting from precursor Fe and Ba hexaferrite particles. Our results show that, for maximum applied fields of up to 8 kOe, the measured loops show a shift of up to 85 Oe. The compositional dependence of that loop displacement presents two maxima (at approximately x=0.3 and =0.7) and a minimum at =0.5. These results are discussed in terms of the dipolar coupling between both phases

    Precise Thermal NDE for Quantifying Structural Damage

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    We have developed precise thermal NDE as a wide-area inspection tool to quantify structural damage within airframes and bridge decks. We used infrared cameras and image processing to produce precise temperature, thermal inertia, and cooling-rate maps of flash-heated aircraft skins. These maps allowed us to distinguish major structural defects from minor flaws which do not warrant costly repairs. We quantified aircraft skin corrosion defects with metal losses as low as 5% with 3% overall uncertainty [1–6]. We proved the feasibility of precise thermal NDE to inspect naturally-heated asphalt-concrete bridge decks. To this end, we quantified structural damage within asphalt-concrete slabs by locating the sites, and determining the relative volumes, of concrete displacements from 2-inch deep and 4-inch deep synthetic delaminations in asphalt-concrete slabs [4–8]

    Ligand exchange in gold-coated FePt nanoparticles

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    In this work, we present the magnetic properties of gold-coated FePt nanoparticles and the study of stable aqueous dispersions of FePt@Au and FePt synthesized after ligand exchange with mercaptoundecanoic acid. The particle size determined from transmission electron microscopy (TEM) micrographs goes from 4 nm for the uncoated nanoparticles to a maximum of 10 nm for the gold-coated ones indicating that the thickness of the shell ranges from 1 to 3 nm. The magnetic characterization consists in hysteresis cycles at 10 and 300 K. The results show that, at low field and room temperature, the magnetic behavior of uncoated and coated nanoparticles are surprisingly quite similar. Because the gold-coated nanoparticles keep the magnetic properties of FePt and the presence of gold improves the functionalization of nanoparticles, the system is suitable for biological application. Mercaptoundecanoic ligand transfer was used to render water stable nanoparticles in a wide pH range. Transmission electron microscopy and dynamic light scattering (DLS) results show the nanoparticles slightly agglomerate after ligand exchange. Fourier transform infrared spectroscopy results suggest that thiol binds to the gold atoms of the surface

    First measurement of the K−n →Λπ−non-resonant transition amplitude below threshold

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    We present the analysis of K−absorption processes on He4 leading to Λπ−final states, measured with the KLOE spectrometer at the DAΦNE e+e−collider and extract, for the first time, the modulus of the non-resonant K−n →Λπ−direct production amplitude about 33 MeV below the K‾N threshold. This analysis also allows to disentangle the K−nuclear absorption at-rest from the in-flight capture, for K−momenta of about 120 MeV. The data are interpreted with the help of a phenomenological model, and the modulus of the non-resonant K−n →Λπ−amplitude for K−absorption at-rest is found to be |AK−n→Λπ−|=(0.334±0.018stat−0.058+0.034syst)fm

    Risk mapping for the sustainable protection of cultural heritage in extreme changing environments

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    Cultural heritage is widely recognized to be at risk due to the impact of climate change and associated hazards, such as events of heavy rain, flooding, and drought. User-driven solutions are urgently required for sustainable management and protection of monumental complexes and related collections exposed to changes of extreme climate. With this purpose, maps of risk-prone areas in Europe and in the Mediterranean Basin have been produced by an accurate selection and analysis of climate variables (daily minimum and maximum temperature-Tn and Tx, daily cumulated precipitation-RR) and climate-extreme indices (R20mm, R95pTOT, Rx5 day, CCD, Tx90p) defined by Expert Team on Climate Change Detection Indices (ETCCDI). Maps are available to users via an interactive Web GIS (Geographic Information System) tool, which provides evaluations based on historical observations (high-resolution gridded data set of daily climate over Europe-E-OBS, 25 km) and climate projections (regional climate models-RCM, ~12 km) for the near and far future, under Representative Concentration Pathways (RCP) 4.5 and 8.5 scenarios. The tool aims to support public authorities and private organizations in the decision making process to safeguard at-risk cultural heritage. In this paper, maps of risk-prone areas of heavy rain in Central Europe (by using R20mm index) are presented and discussed as example of the outputs achievable by using the Web GIS tool. The results show that major future variations are always foreseen for the 30-year period 2071-2100 under the pessimistic scenario (RCP 8.5). In general, the coastal area of the Adriatic Sea, the Northern Italy, and the Alps are foreseen to experience the highest variations in Central Europe

    Search for Deeply Bound Kaonic Nuclear States with AMADEUS

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    We briefly report on the search for Deeply Bound Kaonic Nuclear States with AMADEUS in the Sigma0 p channel following K- absorption on 12C and outline future perspectives for this work

    Synthesis and characterization of FePt/Au core-shell nanoparticles

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    In this work, the structural and magnetic properties of the gold- coated FePt nanoparticles synthesized from high- temperature solution phase are presented. The amount of gold was optimized to obtain most of the FePt particles coated. The particle diameter increases from 4 to 10 nm as observed by TEM. The magnetic properties are largely affected by the coating. At low temperature, the coercive. field Hc of the coated nanoparticles decreases about three times respect to the uncoated and the blocking temperature reduces to the half. The changes of the magnetic behavior are discussed in terms of the effect of the gold atoms at the FePt core surface
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