1,250 research outputs found

    Application of Nanoindentation Technique in Martensitic Structures

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    Superconductivity under pressure in the Dirac semimetal PdTe2

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    The Dirac semimetal PdTe2_2 was recently reported to be a type-I superconductor (Tc=T_c = 1.64 K, μ0Hc(0)=13.6\mu_0 H_c (0) = 13.6 mT) with unusual superconductivity of the surface sheath. We here report a high-pressure study, p≤2.5p \leq 2.5 GPa, of the superconducting phase diagram extracted from ac-susceptibility and transport measurements on single crystalline samples. Tc(p)T_c (p) shows a pronounced non-monotonous variation with a maximum Tc=T_c = 1.91 K around 0.91 GPa, followed by a gradual decrease to 1.27 K at 2.5 GPa. The critical field of bulk superconductivity in the limit T→0T \rightarrow 0, Hc(0,p)H_c(0,p), follows a similar trend and consequently the Hc(T,p)H_c(T,p)-curves under pressure collapse on a single curve: Hc(T,p)=Hc(0,p)[1−(T/Tc(p))2]H_c(T,p)=H_c(0,p)[1-(T/T_c(p))^2]. Surface superconductivity is robust under pressure as demonstrated by the large superconducting screening signal that persists for applied dc-fields Ha>HcH_a > H_c. Surprisingly, for p≥1.41p \geq 1.41 GPa the superconducting transition temperature at the surface TcST_c^S is larger than TcT_c of the bulk. Therefore surface superconductivity may possibly have a non-trivial nature and is connected to the topological surface states detected by ARPES. We compare the measured pressure variation of TcT_c with recent results from band structure calculations and discuss the importance of a Van Hove singularity.Comment: manuscript 9 pages with 8 figures + supplemental material 3 pages with 6 figure

    Nano-indentation properties of tungsten carbide-cobalt composites as a function of tungsten carbide crystal orientation

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    Tungsten carbide-cobalt (WC-Co) composites are a class of advanced materials that have unique properties, such as wear resistance, hardness, strength, fracture-toughness and both high temperature and chemical stability. It is well known that the local indentation properties (i.e., nano- and micro-hardness) of the single crystal WC particles dispersed in such composite materials are highly anisotropic. In this paper, the nanoindentation response of the WC grains of a compact, full-density, sintered WC-10Co composite material has been investigated as a function of the crystal orientation. Our nanoindentation survey has shown that the nanohardness was distributed according to a bimodal function. This function was post-processed using the unique features of the finite mixture modelling theory. The combination of electron backscattered difiraction (EBSD) and statistical analysis has made it possible to identify the orientation of the WC crystal and the distinct association of the inherent nanoindentation properties, even for a small set (67) of nanoindentations. The proposed approach has proved to be faster than the already existing ones and just as reliable, and it has confirmed the previous findings concerning the relationship between crystal orientation and indentation properties, but with a significant reduction of the experimental data

    Correlation between the indentation properties and microstructure of dissimilar capacitor discharge welded WC-Co/high-speed steel joints

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    The welding of cemented carbide to tool steel is a challenging task, of scientific and industrial relevance, as it combines the high level of hardness of cemented carbide with the high level of fracture toughness of steel, while reducing the shaping cost and extending the application versatility, as its tribological, toughness, thermal and chemical properties can be optimally harmonised. The already existing joining technologies often impart either insufficient toughness or poor high-temperature strength to a joint to withstand the ever-increasing severe service condition demands. In this paper, a novel capacitor discharge welding (CDW) process is investigated for the case of a butt-joint between a tungsten carbide-cobalt (WC-Co) composite rod and an AISI M35 high-speed steel (HSS) rod. The latter was shaped with a conical-ended projection to promote a high current concentration and heat at the welding zone. CDW functions by combining a direct current (DC) electric current pulse and external uniaxial pressure after a preloading step, in which only uniaxial pressure is applied. The relatively high heating and cooling rates promote a thin layer of a characteristic ultrafine microstructure that combines high strength and toughness. Morphological analysis showed that the CDW process: (a) forms a sound and net shaped joint, (b) preserves the sub-micrometric grain structure of the original WC-Co composite base materials, via a transitional layer, (c) refines the microstructure of the original martensite of the HSS base material, and (d) results in an improved corrosion resistance across a 1-mm thick layer near the weld interface on the steel side. A nano-indentation test survey determined: (e) no hardness deterioration on the HSS side of the weld zone, although (f) a slight decrease in hardness was observed across the transitional layer on the composite side. Furthermore, (g) an indication of toughness of the joint was perceived as the size of the crack induced by processing the residual stress after sample preparation was unaltered

    Rate- and State-Dependent Friction Law and Statistical Properties of Earthquakes

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    In order to clarify how the statistical properties of earthquakes depend on the constitutive law characterizing the stick-slip dynamics, we make an extensive numerical simulation of the one-dimensional spring-block model with the rate- and state-dependent friction law. Both the magnitude distribution and the recurrence-time distribution are studied with varying the constitutive parameters characterizing the model. While a continuous spectrum of seismic events from smaller to larger magnitudes is obtained, earthquakes described by this model turn out to possess pronounced ``characteristic'' features.Comment: Minor revisions are made in the text and in the figures. Accepted for publication in Europhys. Letter

    ROOTING OF DATE PALM (PHOENIX DACTYLIFERA L.) OFFSHOOTS BY ISOPROTHIOLANE (IPT)

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    The experiment was conducted at Alhassa Oasis (25° 22′ N' latitude; 49°34′ E longitude) and altitude is 179 m a.s.l , Kingdom of Saudi Arabia. Treatments included the following Isoprothiolane (IPT) concentrations incorporated at the bottom of offshoot hole: control (without IPT), 25g, 50g, 75g, 100g, 200g and 500g / offshoot hole. The offshoots weight ranged between 25 – 30 kg. The IPT concentrations of 75 and 100 g/ offshoot hole seemed to be quite optimal for improving rooting of date palm offshoots. The best rooting percentage, length of root, root fresh and dry weights were obtained under 75 and 100 g/ offshoot whole IPT concentrations. Offshoots under the control and the lowest and highest IPT treatments reflected poor rooting ability. The chlorophyll content data although looked relatively similar between treatments, a slight edge of 75 and 100 g/ offshoot hole was noticeable. This relative edge might have played a significant role in the photosynthetic ability of offshoots. The efficiency of rooting of offshoots under both concentrations might have resulted from their edged photosynthetic ability
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