Influence of adhesive systems on the bonding of dental amalgam to glass ionomer cement

Statement of problem. Dental amalgam restorations have traditionally been retained in cavity preparations by surgical procedures called retention form. In this procedure healthy dental structure is usually removed to create adequate retention. The increasing use of bonding systems for restorative procedures may result in more conservative cavity preparations. Purpose. The purpose of this study was to evaluate the tensile bond strength of the amalgam to glass ionomer cement under the influence of three adhesive systems (Panavia-EX, Vidrion F fresh mix, and Alpha Seal). Material and methods. The bonded assemblies were stored in an environment of 100% relative humidity and 37 degrees C for 24-hour and 30-day storage periods. The test specimen was loaded in tension to failure on a universal testing machine with a crosshead speed of 6 mm/min. Results. The results revealed that in the 24-hour period without acid etch fresh Vidrion F and Panavia Ex adhesives were stronger than autopolymerizing sealant. Panavia Ex adhesive was stronger in the 24-hour period with acid etch. Conclusions. The 30-day period with acid etch revealed no statistical difference among the adhesives. In the 30-day period without acid etch, the fresh Vidrion F adhesive recorded the greatest tensile bond strength.77212713

Evaluation of varying amounts of thermal cycling on bond strength and permanent deformation of two resilient denture liners

Statement of problem. Two problems found in prostheses with resilient liners are bond failure to the acrylic resin base and increased permanent deformation due to material aging. Purpose. This in vitro study evaluated the effect of varying amounts of thermal cycling on bond strength and permanent deformation of 2 resilient denture liners bonded to an acrylic resin base. Material and methods. Plasticized acrylic resin (PermaSoft) or silicone (Softliner) resilient lining materials were processed to a heat-polymerized acrylic resin (QC-20). One hundred rectangular specimens (10 X 10-mm(2) cross-sectional area) and 100 cylindrically-shaped specimens (12.7-mm diameter X 19.0-mm height) for each liner/resin combination were used for the tensile and deformation tests, respectively. Specimen shape and liner thickness were standardized. Specimens were divided into 9 test groups (n=10) and were thermal cycled for 200, 500, 1000, 1500, 2000, 2500, 3000, 3500, and 4000 cycles. Control specimens (n=10) were stored for 24 hours in water at 37degreesC. Mean bond strength, expressed as stress at failure (MPa), was determined with a tensile test using a universal testing machine at a crosshead speed of 5 mm/min. Analysis of failure mode, expressed as a percent (%), was recorded as either cohesive, adhesive, or both, after observation. Permanent deformation, expressed as a percent (%), was determined using ADA specification no. 18. Data from both tests were examined with a 2-way analysis of variance and a Tukey test (alpha=.05). Results. For the tensile test, Softliner specimens submitted to different thermal cycling regimens demonstrated no significantly different bond strength values from the control; however, there was a significant difference between the PermaSoft control group (0.47 +/- 0.09 MPa [mean +/- SD]) and the 500 cycle group (0.46 +/- 0.07 MPa) compared to the 4000 cycle group (0.70 +/- 0.20 MPa) (P<.05). With regard to failure type, the Softliner groups presented adhesive failure (100%) regardless of specimen treatment. PermaSoft groups presented adhesive (53%), cohesive (12%), or a combined mode of failure (35%). For the deformation test, there was no significant difference among the Softliner specimens. However, a significant difference was observed between control and PermaSoft specimens after 1500 or more cycles (1.88% +/- 0.24%) (P<.05). Conclusions. This in vitro study indicated that bond strength and permanent deformation of the 2 resilient denture liners tested varied according to their chemical composition.92328829

Effect of thermocycling on bond strength and elasticity of 4 long-term soft denture liners

Statement of problem. Two problems found in prostheses with soft liners are bond failure to the acrylic resin base and loss of elasticity due to material aging. Purpose. This in vitro study evaluated the effect of thermocycling on the bond strength and elasticity of 4 long-term soft denture liners to acrylic resin bases. Material and methods. Four soft lining materials (Molloplast-B, Flexor, Permasoft, and Pro Tech) and 2 acrylic resins (Classico, and Lucitone 199) were processed for testing according to manufacturers' instructions. Twenty rectangular specimens (10 X 10-mm(2) cross-sectional area) and twenty cylinder specimens (12.7-mm diameter X 19.0-mm height) for each liner/resin combination were used for the tensile and deformation tests, respectively. Specimen shape and liner thickness were standardized. Samples were divided into a test group that was thermocycled 3000 times and a control group that was stored for 24 hours in water at 37degreesC. Mean bond strength, expressed in megapascals (Wa), was determined in the tensile test with the use of a universal testing machine at a crosshead speed of 5 mm/min. Elasticity, expressed as percent of permanent deformation, was calculated with an instrument for measuring permanent deformation described in ADA/ANSI specification 18. Data from both tests were examined with 1-way analysis of variance and a Tukey test, with calculation of a Scheffe interval at a 95% confidence level. Results. In the tensile test under control conditions, Molloplast-B (1.51 +/- 0.28 MPa [mean SD]) and Pro Tech (1.44 +/- 0.27 MPa) liners had higher bond strength values than the others (P < .05). With regard to the permanent deformation test, the lowest values were observed for Molloplast-B (0.48% +/- 0.19%) and Flexor (0.44% +/- 0.14%) (P < .05). Under thermocycling conditions, the highest bond strength occurred with Molloplast-B (1.37 +/- 0.24 MPa) (P < .05) With regard to the deformation test, Flexor (0.46% +/- 0.13%) and Molloplast-B (0.44% +/- 0.17%) liners had lower deformation values than the others (P < .05). Conclusion. The results of this in vitro study indicated that bond strength and permanent deformity values of the 4 soft denture liners tested varied according to their chemical composition. These tests are not completely valid for application to dental restorations because the forces they encounter are more closely related to shear and tear. However, the above protocol serves as a good method of investigation to evaluate differences between thermocycled and control groups.88551652

Fatigue performance of joints executed in pure titanium structures with several diameters

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)This study evaluated fatigue strength of CP-Ti laser-welded joints. Sixty (20/diameter) CP-Ti casted dumbbell rods with diameters of 1.5, 2.0, and 3.5 mm were sectioned and welded using two joint openings (0.0 (00) and 0.6 mm (06)). Six groups were formed, amounting to a total of 9 (n=10) with inclusion of intact groups. Welding was executed using 360 V/8 ms (1.5 and 2.0 mm) and 380 V/9 ins (3.5 mm). Joints were finished, polished, and submitted to radiographic examination to visually analyze presence of porosity (PP). Specimens were submitted to cyclic tests, and the number of cycles until failure (NC) was recorded. Fractured surfaces were examined by SEM. Kruskal-Wallis and Dunn (alpha=0.05) tests demonstrated that NC was lower for all diameters with 06, and for 3.5 mm/00. NC and PP were found to have a negative correlation (Spearman Coefficient). For CP-Ti frameworks with thin diameters, laser welding is better when structures are juxtaposed.306887893Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)FAPESP [06/58816-2

Photoelastic Analysis of the Distribution of Stress in Different Systems of Overdentures on Osseous-Integrated Implants

Objective: The aim of this study was to evaluate the distribution of generated stress around implants and adjacent bone tissue using different implant-retained overdenture designs through photoelastic analysis. Methods: Over an edentulous human mandible, achieved from a human model, 2 or 4 microunit analog abutments were embedded (Master; Conexao Systems Prosthodontics, Sao Paulo, Brazil), settled in the interforaminal region. Three models of photoelastic resin (Araltec Chemicals Ltda, Hunstman, Guarulhos, Sao Paulo, Brazil), with 2 or 4 incorporated implants and microunit abutments, were obtained from molds using silicone for duplication. Inclusion, finishing, and polishing procedures were applied on the frameworks. This study was based on 3 different mechanisms of implant-retained mandibular overdentures: O'ring (GI), bar-clip (GII) (both with 2 implants), and their association (GIII) (with 4 implants). After the adaptation of each overdenture system on the photoelastic models, 100-N alternate occlusal loads were applied on back-side and frontside regions. The photoelastic analysis was made with the aid of a plain polariscope linked to a digital camera, Sony Cybershot > 100, which allowed visualization of the fringes and registration of images on digital photographs. Results: The results demonstrated higher tension concentrated over the GIII, with a flat distribution of stress to the posterior ridge and overload on the posterior implants. GI showed the smaller stress level, and GII, intermediate level; there was distribution of stress to the posterior ridge in these 2 groups. Conclusion: The use of bar attachment proved to be a better alternative, because it showed a moderate level of tension with a more uniform stress distribution and possessed higher retention than did the ball system.22623322336State of Sao Paulo, Brazil [2005/03595-9]State of Sao Paulo, Brazil [2005/03595-9

Radiographic inspection of porosity in Ti-6Al-4V laser-welded joints

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)Widely used in dentistry, Ti-6Al-4V alloy is difficult to cast and solder, as it frequently exhibits pores inside the structure. This study was conducted to evaluate the effect of joint openings and diameters of laser-welded joints executed in Ti-6Al-4V structures on the presence of pores as checked by radiographic procedures. Sixty dumbbell rods with central diameters of 1.5, 2.0 and 3.5 mm were created from Ti-6Al-4V-wrought bars. Specimens were sectioned and welded using two joint openings (0.0 and 0.6 mm). The combination of variables created six groups (n = 10). Laser welding was executed using 360V/8ms (1.5 and 2.0 mm) and 380V/9ms (3.5 mm), with the focus and frequency set to zero. The joints were finished, polished and submitted to radiographic examination. The radiographs were visually examined for the presence of pores in the joints, qualitatively. The percentage of radiographic presence of pores was calculated without counting pores per joint. Data were analyzed using a chi-square test (alpha = 0.05). For the 1.5-mm specimens, the incidence of pore presence was significantly higher (p = 0.0001) when using 0.6-mm joint openings (40%) compared to 0.0-mm openings (0%). For the 2.0-mm specimens, there was no significant difference between groups (p = 0.2008). However, for the 3.5-mm specimens, the incidence of pore presence was lower (p = 0.0061) for 0.6-mm openings (50%) compared to 0.0-mm openings (70%). Therefore, laser welding of Ti-6Al-4V structures with thin diameters provides the best condition for the juxtaposition of the parts.252103108Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)NEODENT Industria e Comercio de Materiais Dentarios LtdaFundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)FAPESP [06/58816-2, 07/51306-1

Corrosion-fatigue of laser-repaired commercially pure titanium and Ti-6Al-4V alloy under different test environments

This study evaluated the corrosion-fatigue life of laser-repaired specimens fabricated from commercially pure titanium (CP Ti) and Ti-6Al-4V alloy, tested under different storage conditions. For each metal, 30 dumbbell rods with a central 2.3 mm diameter were prepared by lost-wax casting with the Rematitan System. Simulating the failure after service, corrosion-fatigue life in different media at room temperature (air, synthetic saliva and fluoride synthetic saliva) was determined at a testing frequency of 10 Hz for intact specimens and after laser repairing, using a square waveform with equal maximum tensile and compressive stress that was 30% lower than the 0.2% offset yield strength. For laser welding, the fractured specimens were rejoined using a jig to align the sections invested in type-IV dental stone. The adjacent areas of the gap was air-abraded with 100 mum aluminum oxide, laser welded and retested under the same conditions as the initial intact specimens. The number of cycles at failure was recorded, and the fracture surface was examined with a scanning electron microscope (SEM). The number of cycles for failure of the welded and intact specimens was compared by ANOVA and the Tukey test at a 5% probability level. Within the limitations of this study, the number of cycles required for fracture decreased in wet environments and the laser repairing process adversely affected the life of both metals under the corrosion-fatigue conditions.31101029103

Radiographic inspection of porosity in pure titanium dumbbell castings

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)Radiographic inspection of porosity in pure titanium dumbbell castings Background: Titanium frameworks are frequently indicated for implant supported prostheses; however, voids are usually encountered inside cast titanium. Objective: This study aimed to confirm the efficacy of a radiographic technique for inspection of porosity in commercially pure titanium castings with different diameter. Materials and methods: Sixty dumbbell rods (n = 20) with a central 1.5, 2.0 and 3.5 mm diameter were prepared by lost-wax casting. Cast specimens were finished and polished and submitted to radiographic examination (90 kV, 15 mA, 0.6 s and 10-13 mm of distance) using periapical film. The radiographs were visually analysed for the presence of porosity in the extension of the dumbbell or in the central portion of the rods. Data were submitted to Pearson Chi-square test (5%). Results: The tested radiographic method proved to be suitable for the evaluation of cast frameworks. Internal porosities were observed in most of the specimens (91.7%) (p = 0.0005); however, only 20% occurred on the central portion of the rods (p = 0.612). Conclusion: Internal porosities can be visualised through radiographs and occur mostly in small diameter structures. The radiographic evaluation of metal structures can improve the quality of frameworks and thereby potentially increase the longevity of the rehabilitation.283233237Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)FAPESP [2006/58816-2, 2007/51306-1

Influence of Methodologic Aspects on the Results of Implant-Abutment Interface Microleakage Tests: A Critical Review of In Vitro Studies

Purpose: This study sought to evaluate the influence of methodologic aspects on variations in the findings of in vitro microleakage studies of the implant-abutment interface. Materials and Methods: The MEDLINE, EMBASE, and Cochrane Library databases were consulted for in vitro studies published between 1990 and August 2011. Date from the studies that met the inclusion and exclusion criteria were arranged in tables and subjected to descriptive analysis. Results: Twenty-one studies were found to be eligible for the analysis after application of the inclusion/exclusion criteria. Sixteen studies used bacteria (76.2%), one used a bacterial toxin (4.76%), one used saliva (4.76%), two employed dyes (9.52%), and one used a combination of dyes and bacteria (4.76%). Eight studies evaluated microleakage from the inner portion of the implant to the external portion (38.1%) and nine examined the reverse (42.85%), while four studies investigated the relationship between them (19.05%). The volume inoculated inside the implants ranged from 0.1 to 5.0 mL. The bacterial concentrations used in the tests ranged from 2.41 x 10(6) to 8 x 10(8) colony-forming units/mL. Oral bacterial flora; mixtures of bacteria, toluidine blue, and gentian violet; and lipopolysaccharide of Salmonella enterica bacterial toxins were used. The monitoring period of test results ranged from 24 hours to 11 weeks for bacteria, 5 minutes to 7 days for dye, and 7 days for bacterial toxins. In four studies, microleakage was correlated with the size of the implant-abutment microgap. The external-hexagon implant configuration showed the greatest microleakage, followed by internal-trilobe, internal-hexagon, and internal-taper configurations. Conclusion: The lack of standardization hinderd comparisons of the studies and could explain the divergent results. It is suggested for future studies that special emphasis be placed upon inoculation and analysis of the specific volume for each system, lower concentrations of inoculated bacterial suspensions, and shorter follow-up time when using bacteria. INT J ORAL MAXILLOFAC IMPLANTS 2012;27:793-800.27479380