188 research outputs found
A small sealed Ta crucible for thermal analysis of volatile metallic samples
Differential thermal analysis on metallic alloys containing volatile elements
can be highly problematic. Here we show how measurements can be performed in
commercial, small-sample, equipment without modification. This is achieved by
using a sealed Ta crucible, easily fabricated from Ta tubing and sealed in a
standard arc furnace. The crucible performance is demonstrated by measurements
on a mixture of Mg and MgB, after heating up to 1470. We
also show data, measured on an alloy with composition GdMg, that
clearly shows both the liquidus and a peritectic, and is consistent with
published phase diagram data
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