Transit Time Effect on Voltage Contrast in the Stroboscopic Scanning Electron Microscope

Voltage contrast varies if the specimen voltage changes within the secondary electron transit time through the specimen electric field. This effect would affect the time resolution in stroboscopic scanning electron microscopy. The method to calculate the transit time effect that was described in a previous paper is reviewed. The calculated results agreed well with the experiment in which a specially designed specimen is used to estimate the applied voltage as exactly as possible

Intrinsic Low Temperature Paramagnetism in B-DNA

We present experimental study of magnetization in $\lambda$-DNA in conjunction with structural measurements. The results show the surprising interplay between the molecular structures and their magnetic property. In the B-DNA state, $\lambda$-DNA exhibits paramagnetic behaviour below 20 K that is non-linear in applied magnetic field whereas in the A-DNA state, remains diamagnetic down to 2 K. We propose orbital paramagnetism as the origin of the observed phenomena and discuss its relation to the existence of long range coherent transport in B-DNA at low temperature.Comment: 5 pages, 4 figures, submitted to Physical Review Letters October 200

New Analytical Methods for the Surface/ Interface and the Micro-Structures in Advanced Nanocomposite Materials by Synchrotron Radiation

Analytical methods of surface/interface structure and micro-structure in advanced nanocomposite materials by using the synchrotron radiation are introduced. Recent results obtained by the energy-tunable and highly collimated brilliant X-rays, in-situ wide angle/small angle X-ray diffraction with high accuracy are reviewed. It is shown that small angle X-ray scattering is one of the best methods to characterize nanoparticle dispersibility, filler aggregate/agglomerate structures and in-situ observation of hierarchical structure deformation in filled rubber under cyclic stretch. Grazing Incidence(small and wide angle) X-ray Scattering are powerful to analyze the sintering process of metal nanoparticle by in-situ observation as well as the orientation of polymer molecules and crystalline orientation at very thin surface layer (ca 7nm) of polymer film. While the interaction and conformation of adsorbed molecule at interface can be investigated by using high energy X-ray XPS with Enough deep position (ca 9 micron m).Received: 11 October 2010; Revised: 13 December 2010; Accepted: 23 December 201

Noise Measurement of Interacting Ferromagnetic Particles with High Resolution Hall Microprobes

We present our first experimental determination of the magnetic noise of a superspinglass made of < 1 pico-liter frozen ferrofluid. The measurements were performed with a local magnetic field sensor based on Hall microprobes operated with the spinning current technique. The results obtained, though preliminary, qualitatively agree with the theoretical predictions of Fluctuation-Dissipation theorem (FDT) violation [1].Comment: 4pages, 2 figure

Non-generality of the Kadowaki-Woods ratio in correlated oxides

An explicit expression for the Kadowaki-Woods ratio in correlated metals is derived by invoking saturation of the (high-frequency) Fermi-liquid scattering rate at the Mott-Ioffe-Regel limit. Significant deviations observed in a number of oxides are quantitatively explained due to variations in carrier density, dimensionality, unit cell volume and the number of individual sheets in the Brillouin zone. A generic re-scaling of the original Kadowaki-Woods plot is also presented.Comment: 9 pages of text, 1 table, 2 figure

Growth of a dynamical correlation length in an aging superspin glass

We report on zero field cooled magnetization relaxation experiments on a concen- trated frozen ferrofluid exhibiting a low temperature superspin glass transition. With a method initially developed for spin glasses, we investigate the field dependence of the relaxations that take place after different aging times. We extract the typical number of correlated spins involved in the aging dynamics. This brings important insights into the dynamical correlation length and its time growth. Our results, consistent with expressions obtained for spin glasses, extend the generality of these behaviours to the class of superspin glasses. Since the typical flipping time is much larger for superspins than for atomic spins, our experiments probe a time regime much closer to that of numerical simulations

Superspin glass aging behavior in textured and nontextured frozen ferrofluid

The effect of magnetic anisotropy-axis alignment of individual nanoparticles on the collective aging behavior in the superspin glass state of a frozen ferrofluid has been investigated. The ferrofluid studied here consists of maghemite nanoparticles (\gamma-Fe2O3, mean diameter = 8.6 nm) dispersed in glycerin at a volume fraction of ~15%. The low temperature aging behavior has been explored through 'zero-field cooled magnetization' (ZFCM) relaxation measurements using SQUID magnetometry. The ZFCM response functions were found to scale with effective age of the system in both textured and non-textured superspin glass states, but with markedly different scaling exponents, \mu. The value of {\mu} was found to shift from ~0.9 in non-textured case to ~ 0.6 in the textured case, despite the identical cooling protocol used in both experiments

Effect of controlled disorder on quasiparticle thermal transport in Bi2_2Sr2_2CaCu2_2O8_8

Low temperature thermal conductivity, $\kappa$, of optimally-doped Bi2212 was studied before and after the introduction of point defects by electron irradiation. The amplitude of the linear component of $\kappa$ remains unchanged, confirming the universal nature of heat transport by zero-energy quasiparticles. The induced decrease in the absolute value of $\kappa$ at finite temperatures allows us to resolve a nonuniversal term in $\kappa$ due to conduction by finite-energy quasiparticles. The magnitude of this term provides an estimate of the quasiparticle lifetime at subkelvin temperatures.Comment: 5 pages including 2 .eps figuer

Small-polaron hopping conductivity in bilayer manganite La1.2_{1.2}Sr1.8_{1.8}Mn2_{2}O7_{7}

We report anisotropic resistivity measurements on a La$_{1.2}$Sr$_{1.8}$Mn$_{2}$O$_{7}$ single crystal over a temperature $T$ range from 2 to 400 K and in magnetic fields $H$ up to 14 T. For $T\geq 218$ K, the temperature dependence of the zero-field in-plane $\rho_{ab}(T)$ resistivity obeys the adiabatic small polaron hopping mechanism, while the out-of-plane $\rho_{c}(T)$ resistivity can be ascribed by an Arrhenius law with the same activation energy. Considering the magnetic character of the polarons and the close correlation between the resistivity and magnetization, we developed a model which allows the determination of $\rho_{ab,c}(H,T)$. The excellent agreement of the calculations with the measurements indicates that small polarons play an essential role in the electrical transport properties in the paramagnetic phase of bilayer manganites.Comment: 4 pages, 3 figures, to appear in Physical Review