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    Tiny MoO<sub>3</sub> nanocrystals self-assembled on folded molybdenum disulfide nanosheets via a hydrothermal method for supercapacitor

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    <p>Coupling of two active semiconductors can easily lead to a deterioration of their intrinsic properties. In this work, tiny MoO<sub>3</sub> nanocrystals were deposited on 3D MoS<sub>2</sub> frameworks via a hydrothermal reaction, with heterostructures forming by oxygen-bonding interactions at their interface. When tested as a supercapacitor electrode, the MoS<sub>2</sub>/MoO<sub>3</sub> heterostructure exhibited a high specific capacitance of 287.7 F g<sup>−1</sup> at a current density of 1 A g<sup>−1</sup>, and a remarkable cycling stability after 1000 cycles at 1 A g<sup>−1</sup> in an aqueous solution compared to pristine MoS<sub>2</sub>. The results thus reveal the superior properties of the MoS<sub>2</sub>/MoO<sub>3</sub> heterostructure for supercapacitor electrode.</p> <p>We successfully synthesized tiny MoO<sub>3</sub> nanocrystals deposited on 3D MoS<sub>2</sub> frameworks via a self-assembly. The MoS<sub>2</sub>/MoO<sub>3</sub> heterostructure exhibited a high specific capacitance and cycling stability compared to pristine MoS<sub>2</sub>.</p
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