Effect of Internal Pressure on Microstructural and Mechanical Properties of X10CrNiCuNb18-9-3 (SUPER 304H) Austenitic Stainless Steel

Despite the current tendencies towards decarbonization of the energy sector, it is still necessary to maintain the lifetime of existing coal-fired power plants. Austenitic stainless steels belong among materials used in energetics, in this case, SUPER 304H (X10CrNiCuNb18-9-3). This steel is used for the experiment that simulates real operating conditions, specifically high temperature (700°C) and constant inner pressure (25 MPa), which is induced by inserting a distilled water medium before sealing. This work deals with the evaluation of the microstructure and mechanical properties of the SUPER 304H specimens, both with and without inner pressure. All the specimens underwent the same long-term exposure in a form of laboratory annealing. The mechanical properties were evaluated by performing the tensile, impact and hardness tests and microstructure was characterized by light optical microscopy and scanning electron microscopy

Analysis of behavior of composite material during loading tests

Abstract Composites are widely used as a material suitable for construction applications, but the operating conditions can lead to reduction of materials properties, damage initiation and collapse of the structure, so it is necessary to monitor condition of components and thus prevent its catastrophic failure. The unidirectional glass fiber reinforced polymer matrix composite (GFRP) was inspected with usage of non-destructive (NDT) acoustic emission during the static loading tests. The 0° test specimens were manufactured and tested under tensile and three-point flexural load for which the custom-made apparatus was used. Failure mechanisms were inspected by detailed analysis using scanning electron microscopy (SEM) to deduce the damage sequence. Tensile stress-initiated matrix cracking which induces formation of scarps, ribbons and riverlines followed by delamination and fiber failure with formation of radials. Flexural load showed cracks in matrix, delamination and typical compression regions in form of fiber microbuckling. Based on the speed of wave propagation and linear localization, damage processes were detected in form of lateral cracking, delamination and integrity loss during the tensile and flexural tests. The data obtained from mechanical testing were correlated with selected acoustic emission parameters (counts, events, amplitude and duration). Behavior of GFRP material during the tensile test can be described very well with usage of counts while the flexural test provides much less information. The evaluation of damage processes using event parameter based on the amplitude and duration proved to be problematic due to the noise interference. The Short-time Fourier transform (ST-FFT) and peak frequency was used for identification of failure modes. In case of tensile and flexural load the matrix cracking has lower frequencies while delamination and fiber failure have higher values.</jats:p