Physico-chemical quality and homogeneity of folic acid and iron in enriched flour using principal component analysis

The aim of the present work was to determine parameters of the corn and wheat flour matrix, such as protein, lipid, moisture, ash and carbohydrates, folic acid and iron contents. Three principal components explained 91% of the total variance. Wheat flours were characterized by high protein and moisture content. On the other hand, the corn flours had the greater carbohydrates, lipids and folic acid levels. The concentrations of folic acid were lower than the issued value for wheat flours. Nevertheless, corn flours presented extremely high values. The iron concentration was higher than that recommended in Brazilian legislation. Poor homogenization of folic acid and iron was observed in enriched flours. This study could be useful to help the governmental authorities in the enriched food programs evaluation.6016417

Metabolic fingerprinting of royal jelly: characterization and proof of authenticity

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)Introduction Metabolic fingerprint is a high-throughput screening to provide a sample classification. Objectives Herein, we describe a metabolic fingerpint strategy for proof of authenticity and possible adulteration of natural products. This strategy provides useful and complementary information to food science for content analysis. Methods Twelve samples of commercial royal jelly were analysed by electrospray ionization mass spectrometry (ESI-MS) in the negative mode. ESI-MS/MS was performed for characteristic negatively charged ions. Results Thermostability studies were also performed to royal jelly samples in order to evaluate the change on chemical composition with different times of exposure to heating and storage at room temperature. Conclusion The methodology developed in this work is useful to proof of authenticity and degradation of royal jelly samples using minimum sample preparation and direct injection of extracts.34185190Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES