Microgravity nucleation and particle coagulation experiments support

A preliminary model for diffusion between concentric hemispheres was adapted to the cylindrical geometry of a microgravity nucleation apparatus, and extended to include the effects of radiation and conduction through the containment walls. Computer programs were developed to calculate first the temperature distribution and then the evolving concentration field using a finite difference formulation of the transient diffusion and radiation processes. The following estimations are made: (1) it takes approximately 35 minutes to establish a steady temperature field; (2) magnesium vapors released into the argon environment at the steady temperature distribution will reach a maximum supersaturation ratio of approximately 10,000 in the 20-second period at a distance of 15 cm from the source of vapors; and (3) approximately 750W electrical power will be required to maintain steady operating temperatures within the chamber

Microgravity nucleation and particle coagulation experiments support

A hollow sphere model is developed to predict the range of supersaturation ratio values for refractory metal vapors in a proposed experimental nucleation apparatus. Since the experiments are to be carried out in a microgravity environment, the model neglects the effects of convection and assumes that the only transfer of vapors through an inert gas atmosphere is by conduction and molecular diffusion. A consistent set of physical properties data is assembled for the various candidate metals and inert ambient gases expected to be used in the nucleation experiments. Transient partial pressure profiles are computed for the diffusing refractory species for two possible temperature distributions. The supersaturation ratio values from both candidate temperature profiles are compared with previously obtained experimetnal data on a silver-hydrogen system. The model is used to simulate the diffusion of magnesium vapor through argon and other inert gas atmospheres over ranges of initial and boundary conditions. These results identify different combinations of design and operating parameters which are liekly to produce supersaturation ratio values high enough to induce homogeneous nucleation in the apparatus being designed for the microgravity nucleation experiments

Microgravity nucleation and particle coagulation experiments support

Researchers at NASA Goddard Space Flight Center have embarked on a program to study the formation and growth of cosmic grains. This includes experiments on the homogeneous nucleation of refractory vapors of materials such as magnesium, lead, tin, and silicon oxides. As part of this program, the Chemical Engineering Department of the University of Virginia has undertaken to develop a math model for these experiments, to assist in the design and construction of the apparatus, and to analyze the data once the experiments have begun. Status Reports 1 and 2 addressed the design of the apparatus and the development of math models for temperature and concentration fields. The bulk of this report discusses the continued refinement of these models, and the assembly and testing of the nucleation chamber along with its ancillary equipment, which began in the spring of 1988

Microgravity nucleation and particle coagulation experiments support

Modifications to the nucleation apparatus suggested by our first microgravity flight campaign are complete. These included a complete 'repackaging' of the equipment into three racks along with an improved vapor spout shutter mechanism and additional thermocouples for gas temperature measurements. The 'repackaged' apparatus was used in two KC-135 campaigns: one during the week of June 3, 1991 consisting of two flights with Mg and two with Zn, and another series consisting of three flights with Zn during the week of September 23, 1991. Our effort then was focused on the analysis of these data, including further development of the mathematical models to generate the values of temperature and supersaturation at the observed points of nucleation. The efforts to apply Hale's Scaled Nucleation Theory to our experimental data have met with only limited success, most likely due to still inadequate temperature field determination. Work on the development of a preliminary particle collector system designed to capture particles from the region of nucleation and condensation, as well as from other parts of the chamber, are discussed

Microgravity nucleation and particle coagulation experiments support

This project is a part of a program at GSFC to study to formation and growth of cosmic dust grain analogs under terrestrial as well as microgravity conditions. Its primary scientific objective is to study the homogeneous nucleation of refractory metal vapors and a variety of their oxides among others, while the engineering, and perhaps a more immediate objective is to develop a system capable of producing mono-dispersed, homogeneous suspensions of well-characterized refractory particles for various particle interaction experiments aboard the Space Shuttle and Space Station Freedom. Both of these objectives are to be met by a judicious combination of laboratory experiments on the ground and aboard NASA's KC-135 experimental research aircraft. Major effort during the current reporting period was devoted to the evaluation of our very successful first series of microgravity test runs in Feb. 1990. Although the apparatus performed well, it was decided to 'repackage' the equipment for easier installation on the KC-135 and access to various components. It will now consist of three separate racks: one each for the nucleation chamber, the power subsystem, and the electronic packages. The racks were fabricated at the University of Virginia and the assembly of the repackaged units is proceeding well. Preliminary analysis of the video data from the first microgravity flight series was performed and the results appear to display some trends expected from Hale's Scaled Nucleation Theory of 1986. The data acquisition system is currently being refined

Annual collection and storage of solar energy for the heating of buildings. Report No. 2. Annual progress report, May 1976--July 1977

A new system for year-round collection and storage of solar heated water for heating of buildings has been designed and constructed at the University of Virginia. The system is composed of an energy storage sub-system which stores hot water in an underground pool and of a solar collector sub-system which acts not only to collect solar energy throughout the year but also to limit the evaporative and convective heat losses from the storage system. The annual collection and storage system began operation in late February 1977. Data are presented which illustrates the transient heat transfer which occurs during the start-up phase of operation. Thermal performance results are presented illustrating the efficiency of the solar collector and the variation of solar energy input to storage during a typical day's operation in May. Data are also presented which show the transient build-up of energy storage in the earth which surrounds the storage pool. An analog model has been developed to analyze the transient energy phenomena which occur within the earth surrounding the pool. These include transient heat losses from the pool to the earth and energy storage within the earth. Results of the analog model for idealized conditions are confirmed by exact mathematical solutions and by numerical analysis using a digital computer

Zinc Nucleation and Growth in Microgravity

We report our experiences with zinc nucleation in a microgravity environment aboard NASA's Reduced Gravity Research Facility. Zinc vapor is produced by a heater in a vacuum chamber containing argon gas. Nucleation is induced by cooling and its onset is easily detected visually by the appearance of a cloud of solid, at least partially crystalline zinc particles. Size distribution of these particles is monitored in situ by photon correlation spectroscopy. Samples of particles are also extracted for later analysis by SEM. The initially rapid increase in particle size is followed by a slower period of growth. We apply Scaled Nucleation Theory to our data and find that the derived critical temperature of zinc, the critical cluster size at nucleation, and the surface tension values are all in reasonably good agreement with their accepted literature values