22 research outputs found
Additional file 4 of Sedentary behaviour in hospitalised older people: a scoping review protocol
Additional file 4. Data presentation table for SB and SBBR2
Electrochemical, Regioselective, and Stereoselective Synthesis of Allylic Thioethers and Selenoethers under Transition-Metal-Free and Oxidant-Free Conditions
We
disclose a mild, scalable, electricity-promoted cross coupling
protocol between allylic iodides and disulfides/diselenides for the
formation of C–S/Se bonds in the absence of transition metals,
bases, and oxidants. The stereochemically different densely functionalized
allylic iodides gave regio- and stereoselective diverse thioethers
in good yields. This strategy demonstrates a sustainable promising
approach for the synthesis of allylic thioethers in 38–80%
yields. This protocol also provides a synthetic platform for the synthesis
of allylic selenoethers. A single-electron transfer radical pathway
was also validated with radical scavenger experiments and cyclic voltammetry
data
Electrochemical, Regioselective, and Stereoselective Synthesis of Allylic Thioethers and Selenoethers under Transition-Metal-Free and Oxidant-Free Conditions
We
disclose a mild, scalable, electricity-promoted cross coupling
protocol between allylic iodides and disulfides/diselenides for the
formation of C–S/Se bonds in the absence of transition metals,
bases, and oxidants. The stereochemically different densely functionalized
allylic iodides gave regio- and stereoselective diverse thioethers
in good yields. This strategy demonstrates a sustainable promising
approach for the synthesis of allylic thioethers in 38–80%
yields. This protocol also provides a synthetic platform for the synthesis
of allylic selenoethers. A single-electron transfer radical pathway
was also validated with radical scavenger experiments and cyclic voltammetry
data
Additional file 2 of Sedentary behaviour in hospitalised older people: a scoping review protocol
Additional file 2. CINAHL search
Electrochemical Bisarylation of Carbonyls: A Direct Synthetic Strategy for Bis(indolyl)methane
An interesting electrochemical direct bisarylation of
carbonyls
with indole derivatives to afford the corresponding bis(indolyl)methane
(BIM) derivatives is described. The developed protocol is suitable
for aliphatic, aromatic, and heteroaromatic aldehydes, which react
with various electron-rich and electron-poor indoles to afford the
corresponding BIMs in good to excellent yields. Isatin derivatives
also underwent bisarylation with various indole derivatives under
the influence of current to afford the corresponding BIMs in excellent
yields
Additional file 1 of Sedentary behaviour in hospitalised older people: a scoping review protocol
Additional file 1. PRISMA-P 2015 Checklist
Electrochemical Bisarylation of Carbonyls: A Direct Synthetic Strategy for Bis(indolyl)methane
An interesting electrochemical direct bisarylation of
carbonyls
with indole derivatives to afford the corresponding bis(indolyl)methane
(BIM) derivatives is described. The developed protocol is suitable
for aliphatic, aromatic, and heteroaromatic aldehydes, which react
with various electron-rich and electron-poor indoles to afford the
corresponding BIMs in good to excellent yields. Isatin derivatives
also underwent bisarylation with various indole derivatives under
the influence of current to afford the corresponding BIMs in excellent
yields
Additional file 3 of Sedentary behaviour in hospitalised older people: a scoping review protocol
Additional file 3. Data extraction form
Additional file 1: of Protocol-based management of older adults with hip fractures in Delhi, India: a feasibility study
Focus group discussion for healthcare providers. (DOCX 781 kb
Additional file 2: of Protocol-based management of older adults with hip fractures in Delhi, India: a feasibility study
Patient and carer focus group discussion. (DOCX 780 kb
