Using the simple peel test to measure the adhesive fracture energy, Ga

The adhesive fracture energy of structural adhesive joints may be readily ascertained from linear-elastic fracture-mechanics (LEFM) methods, and indeed an ISO Test Method (ISO 25217: 2009) now exists for the LEFM Mode I value, Gc, as a result of the efforts of the European Structural Integrity Society (ESIS) ‘TC4 Committee’ [1,2]. These LEFM test methods involve the preparation and testing of adhesively-bonded double-cantilever beam (DCB) and tapered double-cantilever beam (TDCB) specimens [3,4]. Notwithstanding the sound and reproducible results that may be obtained from such methods, the LEFM test specimens are relatively complex and expensive to make and test, and many industries would far prefer to deduce the value of the adhesive fracture energy from the very common and widely-used ‘peel test’. (In the present paper, for clarity, the adhesive fracture energy is termed GA when deduced from a peel test.) Indeed, the peel test is an attractive test method to assess the fracture performance of a wide range of structural adhesive joints and flexible laminates. However, although it is a relatively simple test to undertake, it is often a complex test to analyse and thus obtain a characteristic measure of the toughness of the adhesive joint, or laminate

Modelling and predicting fatigue crack growth in structural adhesive joints

The present paper examines crack growth in a range of structural adhesive joints under cyclic-fatigue loadings. It is shown that cyclic-fatigue crack-growth in such materials can be modelled by a form of the Hartman and Schijve crack-growth equation which aims to give a unique and linear ‘master’ representation for the fatigue data points that have been experimentally obtained. This relationship is shown to capture the experimental data representing the effects of test conditions, such as the R-ratio (=σmin /σmax) present in the fatigue cycle and test temperature. It also captures the typical scatter often seen in such tests, especially at low values of the fatigue crack-growth rate. Furthermore, the methodology is shown to be applicable to, and to unify, the results from Mode I (opening tensile), Mode II (in-plane shear) and Mixed-Mode I/II fatigue tests. Finally, it is used to predict successfully the rate of fatigue crack-growth in two bonded-repair type joints where naturally-occurring disbonds have initiated and grown

A systematic approach to the formulation of anti-onychomycotic nail patches

Nail patches have a potential role as drug carriers for the topical treatment of nail diseases such as onychomycosis, a common condition. O ur aim was therefore to develop a systematic and novel appr oach to the formulat ion of a simple drug -in-adhesive ungual patch. Twelve pressure -sensitive adhesives (PSAs), four backing membranes, two release liners and three drugs were screened for pharmaceutical and mechanical properties . From this initial screeni ng, two PSAs, two drugs, one backing membrane and one release liner were selected for further investigation. Patches were prepared by solvent -casting and characterised. The patches had good uniformity of thickness and of drug content, and showed minimal drug crystallisation during six month s of storage. Meanwhile, the d rug stability in the patch upon storage and patch adhesion to the nail was influenced by the nature of the drug, the PSA and the backing membrane . The reported methodology paves the way for a systematic formulation of ungual nail patches to add to the armamentarium of nail medicines . Further , from this work, the best patch formulation has been identified