Dimensional stabile Spiegelsubstrate für kryogene Anwendungen

Auf einer athermalen Werkstoffkombination basierende optische Spiegelsysteme für wissenschaftliche Instrumentierungen der Astronomie ermöglichen eine Steigerung der optischen Performance bei verschiedenen thermischen Umgebungsbedingungen. Bei der Verwendung eines thermisch angepassten Siliziumpartikel verstärkten Aluminiumwerkstoffs sind definierte Thermalbehandlungen notwendig, um die geforderten dimensionalen Stabilitäten bei der jeweiligen Anwendungstemperatur zu erreichen. Beschichtet mit einer röntgenamorphen Nickel-Phosphor-Legierung werden Anwendungen für den visuellen bzw. ultravioletten Spektralbereich ermöglicht. Die vorliegende Arbeit liefert werkstoffwissenschaftliche Grundlagen zur Auswahl geeigneter metallischer Substratwerkstoffe, welche über Rascherstarrungstechniken erzeugt wurden, sowie Richtlinien zu thermischen Behandlungen zur Realisierung athermaler optischer Spiegelsysteme für kryogene Anwendungen. Einflüsse der Temperatur auf die dimensionale Instabilität, wie längenausdehnungsbedingte und zyklothermische Instabilität, sowie die Langzeitinstabilität der untersuchten Werkstoffe werden theoretisch und experimentell erforscht und ausführlich diskutiert

Dimensional Stability of Mirror Substrates Made of Silicon Particle Reinforced Aluminum

In the present study, the thermal cycling stability of mirrors made of silicon particle reinforced aluminum compounds, containing an amount of 42 ± 2 wt.% silicon particles, is investigated with respect to thermal loading. The compound is processed by single-point diamond turning to optical mirrors that were subsequently thermally cycled in a temperature range between 40 °C to −60 °C and between 20 °C and −196 °C, respectively. The residual shape change of the optical surface was analyzed using Fizeau interferometry at room temperature. The change of shape deviation of the mirrors is compared with dilatometric studies of cylinders using the same temperature regime. Due to different coefficients of thermal expansion of the two constituents of the compound, thermal mismatch stresses in the ductile aluminum matrix and the brittle silicon particles are induced by the investigated thermal loads. The plasticity that occurs causes the formation of dislocations and stacking faults as substantiated by Transmission Electron Microscopy. It could be shown that the silicon particles lead to the cold working process of the reinforced aluminum matrix upon thermal cycling. By using interferometry, a higher dimensional stability of mirrors made of silicon particle reinforced aluminum due to thermal loads is demonstrated

A novel athermal approach for high-performance cryogenic metal optics

This paper describes a new athermal approach for high performance metal optics, particularly with regard to extreme environmental conditions as they usually may occur in terrestrial as well as in space applications. Whereas for mid infrared applications diamond turned aluminium is the preferred mirror substrate, it is insufficient for the visual range. For applications at near infrared wavelengths (0.8 μm - 2.4 μm) as well as at on cryogenic temperatures (-200°C) requirements exist, which are only partially met for diamond turned substrates. In this context athermal concepts such as optical surfaces with high shape accuracy and small surface micro-roughness without diffraction effect and marginal loss of stray light, are of enormous interest. The novel, patented material combination matches the Coefficient of Thermal Expansion (CTE) of an aluminium alloy with high silicon content (AlSi, Si >= 40 %) as mirror substrate with the CTE of the electroless nickel plating (NiP). Besides the harmonization of the CTE (~ 13 * 10-6 K-1), considerable advantages are achieved due to the high specific stiffness of these materials. Hence, this alloy also fulfils an additional requirement: it is ideal for the manufacturing of very stable light weight metal mirrors. To achieve minimal form deviations occurring due to the bimetallic effect, a detailed knowledge of the thermal expansion behavior of both, the substrate and the NiP layer is essential. The paper describes the reduction of the bimetallic bending by the use of expansion controlled aluminium-silicon alloys and NiP as a polishing layer. The acquisition of CTE-measurement data, the finite elements simulations of light weight mirrors as well as planned interferometrical experiments under cryogenic conditions are pointed out. The use of the new athermal approach is described exemplary

Ultraprecise flat mirrors for the pointing unit of the DESIS instrument on board of the ISS

Mirrors with excellent mechanical, thermal and optical properties are suitable for a broad spectrum of modern optical application. A growing number of multi- and hyperspectral imaging devices such as telescopes and spectrometers are based on all-reflective metal optics. Optics with higher mechanical or dynamic loads are often made of ceramics; at higher thermal loads, they are made of glass-ceramics. The DLR Earth Sensing Imaging Spectrometer (DESIS) is a space-based hyperspectral instrument developed by German Aerospace Center (DLR). The optical system of the spectrometer was designed, fabricated and pre-aligned by the Fraunhofer Institute of Applied Optics and Precision Engineering (IOF). The instrument was realized as an all-reflective system using metal-based mirrors using a modular, so-called snap-together approach. Parts of the system are flat mirrors for the pointing unit of the instrument. Two flat mirrors based on a metallic substrate material (Al 42Si) and one flat mirror based on a ceramic (HB Cesic®) were realized. The cost-efficient manufacturing technology of metal mirrors has an important advantage over glass, glass-ceramic and ceramic mirrors. For the pointing mirror, a more rigid and stiff material like HB-Cesic® was used. Different and tailored process chains were applied for both kinds of mirrors. The paper summarizes the fabrication of optical mirrors by i) grinding and polishing of ceramic matrix composite substrates; and ii) diamond machining combined with post-polishing techniques, like magnetorheological finishing (MRF) and chemical mechanical polishing (CMP) for metallic substrates. The process chains are described including testing setup and results with regard to different materials and manufacturing technologies. The mirrors show an excellent quality regarding flatness (lower 15 nm rms) and roughness (lower 1 nm rms, WLI magnification 50x)

Intraoperative transfusion practices in Europe

© 2016 The Author. Published by Oxford University Press on behalf of the British Journal of Anaesthesia.Background: Transfusion of allogeneic blood influences outcome after surgery. Despite widespread availability of transfusion guidelines, transfusion practices might vary among physicians, departments, hospitals and countries. Our aim was to determine the amount of packed red blood cells (pRBC) and blood products transfused intraoperatively, and to describe factors determining transfusion throughout Europe. Methods: We did a prospective observational cohort study enrolling 5803 patients in 126 European centres that received at least one pRBC unit intraoperatively, during a continuous three month period in 2013. Results: The overall intraoperative transfusion rate was 1.8%; 59% of transfusions were at least partially initiated as a result of a physiological transfusion trigger- mostly because of hypotension (55.4%) and/or tachycardia (30.7%). Haemoglobin (Hb)- based transfusion trigger alone initiated only 8.5% of transfusions. The Hb concentration [mean (sd)] just before transfusion was 8.1 (1.7) g dl-1 and increased to 9.8 (1.8) g dl-1 after transfusion. The mean number of intraoperatively transfused pRBC units was 2.5 (2.7) units (median 2). Conclusions: Although European Society of Anaesthesiology transfusion guidelines are moderately implemented in Europe with respect to Hb threshold for transfusion (7-9 g dl-1), there is still an urgent need for further educational efforts that focus on the number of pRBC units to be transfused at this threshold

Intraoperative transfusion practices and perioperative outcome in the European elderly: A secondary analysis of the observational ETPOS study

The demographic development suggests a dramatic growth in the number of elderly patients undergoing surgery in Europe. Most red blood cell transfusions (RBCT) are administered to older people, but little is known about perioperative transfusion practices in this population. In this secondary analysis of the prospective observational multicentre European Transfusion Practice and Outcome Study (ETPOS), we specifically evaluated intraoperative transfusion practices and the related outcomes of 3149 patients aged 65 years and older. Enrolled patients underwent elective surgery in 123 European hospitals, received at least one RBCT intraoperatively and were followed up for 30 days maximum. The mean haemoglobin value at the beginning of surgery was 108 (21) g/l, 84 (15) g/l before transfusion and 101 (16) g/l at the end of surgery. A median of 2 [1–2] units of RBCT were administered. Mostly, more than one transfusion trigger was present, with physiological triggers being preeminent. We revealed a descriptive association between each intraoperatively administered RBCT and mortality and discharge respectively, within the first 10 postoperative days but not thereafter. In our unadjusted model the hazard ratio (HR) for mortality was 1.11 (95% CI: 1.08–1.15) and the HR for discharge was 0.78 (95% CI: 0.74–0.83). After adjustment for several variables, such as age, preoperative haemoglobin and blood loss, the HR for mortality was 1.10 (95% CI: 1.05–1.15) and HR for discharge was 0.82 (95% CI: 0.78–0.87). Preoperative anaemia in European elderly surgical patients is undertreated. Various triggers seem to support the decision for RBCT. A closer monitoring of elderly patients receiving intraoperative RBCT for the first 10 postoperative days might be justifiable. Further research on the causal relationship between RBCT and outcomes and on optimal transfusion strategies in the elderly population is warranted. A thorough analysis of different time periods within the first 30 postoperative days is recommended