Review on the possible tool materials for friction stir welding of steel plates

The friction stir welding (FSW) process is mainly used in industrial applications for joining low melting temperature materials such as aluminium and magnesium. FSW has many advantages in comparison with conventional fusion arc welding. Therefore the interest to use this technique for joining steel plates has grown. However such usage is still limited because of the lack of adequate tool materials. This review gives an overview of possible tool materials for FSW of steels focussing on tungsten, tungsten carbide, pcBN and a few ultra-high temperature ceramics

The Surface Characterization of Modified Chrysotile Asbestos

In this paper, results of a semi-quantitative and qualitative leaching study of chrysotile and Chrysophosphate® fibers in oxalic acid and succinate salt buffer solutions with laser microprobe mass analysis (LAMMA) and electron probe X-ray micro-analysis (EPXMA) are presented, which demonstrate clearly the potential of these sensitive surface analytical tools for the analysis of natural physico-chemically modified and depleted fibers. These results are verified with those obtained by atomic absorption spectroscopy (AAS) for the measurement of the leached magnesium and iron concentration in solution. In order to study differences in adsorption behaviour and reaction capability between natural and chemically modified chrysotile, LAMMA-analysis was performed on fibers treated with benzo[a]pyrene, N,N-dimethylaniline (DMA) and ortho-phenylene-diamine (OPDA). In correlation with biomedical investigations. this study could contribute to the elucidation of the potential sequences of fiber surface properties in relation to the biological activity and cytotoxicity

Applications of Laser Microprobe Mass Analysis for Characterization of Asbestos

Laser microprobe mass analysis with the commercial LAMMA-500 (transmission type) instrument when utilized in laser desorption conditions provides information which allows the identification of particular asbestos varieties, in various types of samples, including lung tissue. Also it has detection capability of adsorbed organic material and it is a valuable tool for the study of the surface of chemically modified asbestos fibers manufactured by silanation or through phosgene treatment (chrysophosphate). Recent progress within our laboratory is discussed, and shortcomings of the methodology are indicated

Multi-wire submerged arc welding: a study of secondary process parameters

The goal of this thesis is to investigate the effect of secondary process parameters on the geometry of the weld bead in multi-wire submerged arc welding. Bead-on-plate welding experiments will be conducted using 3, 4 and 5 wires. The parameters being varied will be the wire stick out, the angles of the torches and the spacing in between. Primary process parameters like voltage, current and welding speed will be kept constant. Penetration, bead width and height, percentage dilution, HAZ, weld penetration shape factor and weld reinforcement shape factor will be measured and evaluated. Fewer experiments will be needed because of the use of a design of experiments approach, namely a fractional factorial design. This will allow to determine the significance of each single parameter and their mutual interaction with respect to weld bead shape

Electron Probe Micro-Analysis and Laser Microprobe Mass Analysis of Material Leached from a Limestone Cathedral

Electron probe X-ray micro-analysis (EPXMA) and Laser microprobe mass analysis (LAMMA), were applied to characterize the leachate of sandy limestones of a Belgian cathedral. Individual suspended particles, found in water that was sprayed over the cathedral walls ( 1 each ate water ), were sized and analyzed by automated EPXMA-analysis, and classified with hierarchical cluster methods. LAMMA was used to gather more information about particles, present in the solution, as well as in suspension. It was found that the leachate from black walls, had a high sulphate concentration and a large variety of particles in suspension, with different morphology and composition, with silicates as most abundant group. The leachate from white walls is characterized by a predominant Ca-rich suspension, with both original and recrystallized calcite particles, and by a much lower sulphate-ion concentration in the solution. LAMMA-analysis revealed that the organic group of the EPXMA-analysis, consists mostly of carbon-containing fly-ash particles. Hence, in general, it could be concluded that walls which are not subject to direct rainfall are generally covered with a gypsum crust, that turns black due to adhesion of soil dust and fly-ash particles, while white walls become thinner due to rainwater erosion of weathering products and original stone components

Screening of Banana Hybrids for Resistance to Pratylenchus coffeae

The reaction of twenty-four new synthetic banana hybrids to Pratylenchus coffeae was studied under artificially inoculated pot conditions. Two banana hybrids, H-04-05 and H-04-06 were found to be resistant and ten hybrids, H-04-01, H-04-03, H-04-04, H-04-07, H-04-09, H-04-11, H-04-16, H-04-19, H-04-21 and H-04-24 were found to be tolerant to the lesion nematode, Pratylenchus coffeae and the remaining were rated as susceptible

The microbial diversity of the Su Bentu cave, Italy and the influence of human exploration.

Introduction: The microbial diversity in the Su Bentu Cave (Sardinia, Italy) was investigated by means of Illumina MiSeq analysis. The hypogean environment is of great interest for astrobiological research as cave conditions may resemble those in extra-terrestrial regions. Furthermore, they hold high potential to identify novel, extremely adapted organisms to severely oligo-trophic habitats. However, the influence of human is not neglectable and in-depth investigations are needed to determine the impact of exploration on an otherwise mostly pristine ecosystem. The cave investigated in this study develops for several kilometres into the mountain, two hundred metres below the topographic surface and is characterized by a strong air circulation. Its structure is composed of huge passages carved in limestone where an ephemeral underground stream creates some lakes, close to which seven samples of visible calcite rafts, manganese deposits and moonmilk (a hydrated calcium carbonate speleothem), were sampled during an expedition in 2014. Other samples were re-trieved from a frequently used campsite and from some dry cave passages leading deeper into the cave