284 research outputs found
Agriculture Study Abroad program to Poland
The Technology Travel Course (TSM 496) is an elective course that meets the university-wide international perspectives requirement. The course has a curricular home in the department of Agricultural and Biosystems Engineering (ABE), Iowa State University (ISU). It enables instructors to develop and offer a study abroad program structured as a faculty-led trip abroad. This course is also an excellent opportunity for students to learn/compare technology concepts and applications in an international context that is encouraged by the ABE External Advisory Board. The objectives of this paper are to (1) Review the application of TSM 496 to Ag Study Abroad trip to Poland (with cultural trips to Czech Republic, Denmark, Germany, Lithuania, and Ukraine, and to (2) summarize curricular enhancement of student learning objectives (SLOs) and competencies. The course has been offered yearly since 2011, and served 48 students from several majors in Agriculture & Life Sciences and Engineering colleges. The pre-departure course is focused on teaming up ISU students with students at two agricultural universities in Poland. Teams develop comparative projects focused on agriculture with specific emphasis on animal systems production, technology, environment, sustainability, and regulations. Projects are finalized and presented jointly at special Polish-American Student Workshops. The joint project format creates an opportunity to make friends with students in Poland while working on international projects. The scientific part of the program is a mix of field trips to farms, plants, co-ops, lab tours, cultural sites and activities. Students have many opportunities to socialize, get inspired by rich culture, history, science, agro business attitudes and the spirit of change. SLOs are measured with the program surveys. Currently 65 SLOs/competencies are enhanced with 17 provided by this program (26%). In addition, 25 new competencies are gained, a 38% increase to the new total of 90. Students highly rate this learning and often list it as a highlight of their college career thus far. Data analysis of the Program Evaluation Surveys shows high degree of developing student skills, meeting and enhancement of class goals, departmental and college SLOs
2017 update - Air Quality Laboratory & Olfactometry Laboratory Equipment - Koziel\u27s Lab
EQUIPMENT
Major equipment in Dr. Koziel’s laboratory ([email protected]) see reference list below for complete descriptions of equipment used in previous research.
For odorous VOC gas quantification: VOCs: Agilent 6890 GC-MS-FID-PID (5975C) VOCs: multidimensional GC-MS-Olfactometry (based on Agilent GC-MS platform) equipped with thermal desorption for sorbent tubes. NH3 and H2S (Drager electrochemical portable meter). INNOVA (NH3, CO2) Greenhouse gas GC-FID-ECD (for CO2, CH4, and N2O
Characterizing the Smell of Marijuana by Odor Impact of Volatile Compounds: An Application of Simultaneous Chemical and Sensory Analysis
Recent US legislation permitting recreational use of marijuana in certain states brings the use of marijuana odor as probable cause for search and seizure to the forefront of forensic science, once again. This study showed the use of solid-phase microextraction with multidimensional gas chromatography—mass spectrometry and simultaneous human olfaction to characterize the total aroma of marijuana. The application of odor activity analysis offers an explanation as to why high volatile chemical concentration does not equate to most potent odor impact of a certain compound. This suggests that more attention should be focused on highly odorous compounds typically present in low concentrations, such as nonanal, decanol, o-cymene, benzaldehyde, which have more potent odor impact than previously reported marijuana headspace volatiles
The relationship between chemical concentration and odor activity value explains the inconsistency in making a comprehensive surrogate scent training tool representative of illicit drugs
This report highlights the importance of an individual chemical\u27s odor impact in the olfactory identification of marijuana, cocaine, and heroin. There are small amounts of highly odorous compounds present in headspace of these drugs, with very low odor detection thresholds, that are more likely responsible for contributing to the overall odor of these drugs. Previous reports of the most abundant compounds in headspace can mislead researchers when dealing with whole odor of these drugs. Surrogate scent formulations, therefore, must match the odor impact of key compounds and not just the chemical abundance of compounds. The objective of this study was to compare odorous volatile organic compounds (VOCs) emitted from illicit drug samples of marijuana, cocaine, and heroin to surrogate smell formulations using simultaneous sensory (via human olfaction) and chemical analyses. Use of solid phase microextraction (SPME) allowed VOCs in drug headspace to be extracted and pre-concentrated on site, and analyzed by multidimensional gas chromatography–mass spectrometry–olfactometry (MDGC–MS-O). Use of MDGC–MS-O allowed for further separation of odorous compounds and simultaneous detection by the human nose of the separate odor parts that make up the total aroma of these drugs. The compounds most abundant in headspace were not the most odor impactful when ranked by odor activity values (OAVs) (defined as ratio of concentration to odor detection threshold, ODT). There were no apparent correlations between concentrations and OAVs. A 1 g marijuana surrogate lacked in odor active acids, aldehydes, ethers, hydrocarbons, N-containing, and S-containing VOCs and was overabundant in odor active alcohols and aromatics compared with real marijuana. A 1 g cocaine surrogate was overabundant in odor active alcohols, aldehydes, aromatics, esters, ethers, halogenates, hydrocarbons, ketones and N-containing compounds compared with real. A 1 g heroin surrogate should contain less odor active acids, alcohols, aromatics, esters, ketones, and N-containing compounds. Drug quantity, age and adulterants can affect VOC emissions and their odor impact. The concept of odor activity value, then, is useful to researchers without access to more sophisticated instrumentation. Odor activity values can be calculated from published odor detection thresholds. More research is warranted to expand the database, and determine odor detection thresholds for compounds of interest. Additional information could be obtained from establishing ODTs of key odorants for canines
Odor impact of volatiles emitted from marijuana, cocaine, heroin and their surrogate scents
Volatile compounds emitted into headspace from illicit street drugs have been identified, but until now odor impact of these compounds have not been reported. Data in support of identification of these compounds and their odor impact to human nose are presented. In addition, data is reported on odor detection thresholds for canines highlighting differences with human ODTs and needs to address gaps in knowledge. New data presented here include: (1) compound identification, (2) gas chromatography (GC) column retention times, (3) mass spectral data, (4) odor descriptors from 2 databases, (5) human odor detection thresholds from 2 databases, (6) calculated odor activity values, and (7) subsequent ranking of compounds by concentration and ranking of compounds by odor impact (reported as calculated odor activity values)
Analysis of Odorants in Marking Fluid of Siberian Tiger (Panthera tigris altaica) Using Simultaneous Sensory and Chemical Analysis with Headspace Solid-Phase Microextraction and Multidimensional Gas Chromatography-Mass Spectrometry-Olfactometry
Scent-marking is the most effective method of communication in the presence or absence of a signaler. These complex mixtures result in a multifaceted interaction triggered by the sense of smell. The objective was to identify volatile organic compound (VOC) composition and odors emitted by total marking fluid (MF) associated with Siberian tigers (Panthera tigris altaica). Siberian tiger, an endangered species, was chosen because its MF had never been analyzed. Solid phase microextraction (SPME) for headspace volatile collection combined with multidimensional gas chromatography-mass spectrometry-olfactometry for simultaneous chemical and sensory analyses were used. Thirty-two VOCs emitted from MF were identified. 2-acetyl-1-pyrroline, the sole previously identified compound responsible for the “characteristic” odor of P. tigris MF, was identified along with two additional compounds confirmed with standards (urea, furfural) and four tentatively identified compounds (3-methylbutanamine, (R)-3-methylcyclopentanone, propanedioic acid, and 3-hydroxybutanal) as being responsible for the characteristic aroma of Siberian tiger MF. Simultaneous chemical and sensory analyses improved characterization of scent-markings and identified compounds not previously reported in MF of other tiger species. This research will assist animal ecologists, behaviorists, and zookeepers in understanding how scents from specific MF compounds impact tiger and wildlife communication and improve management practices related to animal behavior. Simultaneous chemical and sensory analyses is applicable to unlocking scent-marking information for other species
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