4 research outputs found
Microstructural Features in Multicore CuβNb Composites
none5siThe study is devoted to heavily drawn multicore Cuβ18Nb composites of cylindrical and rectangular shapes. The composites were fabricated by the melt-and-deform method, namely, 600 in situ rods of Cuβ18%Nb alloy were assembled in a copper shell and cold-drawn to a diameter of 15.4 mm (e = 10.2) and then rolled into a rectangular shape the size of 3 Γ 5.8 mm (e = 12.5). The specimens were analyzed from the viewpoints of their microstructure, microhardness, and thermal stability. The methods of SEM, TEM, X-ray analysis, and microhardness measurements were applied. It is demonstrated that, at higher strain, the fiber texture β¨110β©Nbβ₯ β¨111β©Cuβ₯ DD (drawing direction), characteristic of this material, becomes sharper. The distortions of niobium lattice can be observed, namely, the {110} Nb interplanar distance is broadened in longitudinal direction of specimens and compacted in transverse sections. The copper matrix lattice is distorted as well, though its distortions are much less pronounced due to its recrystallization. Evolution of microstructure under annealing consists mainly in the coagulation of ribbon-like Nb filaments and in the vanishing of lattice distortions. The structural changes in Nb filaments start at 300β400 Β°C, then develop actively at 600 Β°C and cause considerable decrease of strength at 700β800 Β°C.openElena N. Popova, Irina L. Deryagina,Evgeniya G. Valova-Zaharevskaya, Ruello Maria Letizia, Vladimir V. PopovElena N., Popova; Irina L., Deryagina; Evgeniya G., Valova-Zaharevskaya; Ruello, Maria Letizia; Vladimir V., Popo
Structure and Properties of High-Strength Cu-7.7Nb Composite Wires under Various Steps of Strain and Annealing Modes
Microstructure and mechanical properties of in situ Cu-7.7Nb microcomposite (MC) wires manufactured by cold drawing with intermediate heat treatment (HT) have been studied. The evolution of Nb filaments morphology under various steps of deformation and modes of intermediate HT have been studied by the SEM and TEM methods. According to X-ray analysis, internal microstresses accumulate in the niobium filaments of the drawn MC, leading to a decrease in ductility. After heat treatment, the ductility of the wire increases significantly, since the microstresses in the niobium decrease even at the lowest HT temperature. The strength of the composite decreases under the HT because of negative changes in morphology and interface density of Nb filaments. The Nb texture is stable under the HT up to 800 Β°C. The Nb filaments morphology and semi-coherent boundaries at Cu/Nb interfaces are restored under the post-HT cold drawing, leading to a sharp increase in the strength of the MC wire. Reducing the niobium concentration to 7.7%Nb relative to the traditional MC with 16β20%Nb and the recovery of the wire ductility under the HT makes it possible to obtain long-scale high-strength microwires with an extremely small diameter of 0.05 mm and high ultimate tensile strength of 1227 MPa
Effect of Doping Mode and Composite Geometry on the Structure of Nanocrystalline Nb<sub>3</sub>Sn Layers in Superconducting Nb/Cu-Sn Composites
ΠΠ΅ΡΠΎΠ΄Π°ΠΌΠΈ ΠΏΡΠΎΡΠ²Π΅ΡΠΈΠ²Π°ΡΡΠ΅ΠΉ ΠΈ ΡΠΊΠ°Π½ΠΈΡΡΡΡΠ΅ΠΉ ΡΠ»Π΅ΠΊΡΡΠΎΠ½Π½ΠΎΠΉ ΠΌΠΈΠΊΡΠΎΡΠΊΠΎΠΏΠΈΠΈ Ρ ΠΏΡΠΈΠ²Π»Π΅ΡΠ΅Π½ΠΈΠ΅ΠΌ ΠΊΠΎΠ»ΠΈΡΠ΅ΡΡΠ²Π΅Π½Π½ΠΎΠ³ΠΎ ΠΌΠΈΠΊΡΠΎΠ°Π½Π°Π»ΠΈΠ·Π° ΠΈΠ·ΡΡΠ΅Π½Ρ ΠΌΠ½ΠΎΠ³ΠΎΠ²ΠΎΠ»ΠΎΠΊΠΎΠ½Π½ΡΠ΅ ΡΠ²Π΅ΡΡ
ΠΏΡΠΎΠ²ΠΎΠ΄ΡΡΠΈΠ΅ ΠΊΠΎΠΌΠΏΠΎΠ·ΠΈΡΡ Nb/Cu-Sn, ΠΈΠ·Π³ΠΎΡΠΎΠ²Π»Π΅Π½Π½ΡΠ΅ "Π±ΡΠΎΠ½Π·ΠΎΠ²ΡΠΌ" ΠΌΠ΅ΡΠΎΠ΄ΠΎΠΌ ΠΈ Π»Π΅Π³ΠΈΡΠΎΠ²Π°Π½Π½ΡΠ΅ ΡΠΈΡΠ°Π½ΠΎΠΌ. Π£ΡΡΠ°Π½ΠΎΠ²Π»Π΅Π½ΠΎ Π²Π»ΠΈΡΠ½ΠΈΠ΅ ΡΠΏΠΎΡΠΎΠ±Π° Π»Π΅Π³ΠΈΡΠΎΠ²Π°Π½ΠΈΡ ("ΠΈΡΠΊΡΡΡΡΠ²Π΅Π½Π½ΠΎΠ΅" Π»Π΅Π³ΠΈΡΠΎΠ²Π°Π½ΠΈΠ΅ Nb-Π²ΠΎΠ»ΠΎΠΊΠΎΠ½ ΡΠΏΠ»Π°Π²ΠΎΠΌ ΠΠ’50 ΠΈΠ»ΠΈ Π»Π΅Π³ΠΈΡΠΎΠ²Π°Π½ΠΈΠ΅ ΡΠΈΡΠ°Π½ΠΎΠΌ Π±ΡΠΎΠ½Π·ΠΎΠ²ΠΎΠΉ ΠΌΠ°ΡΡΠΈΡΡ) ΠΈ Π²Π½Π΅ΡΠ½Π΅Π³ΠΎ Π΄ΠΈΠ°ΠΌΠ΅ΡΡΠ° ΠΊΠΎΠΌΠΏΠΎΠ·ΠΈΡΠ° Π½Π° ΠΌΠΎΡΡΠΎΠ»ΠΎΠ³ΠΈΡ Nb-Π²ΠΎΠ»ΠΎΠΊΠΎΠ½ ΠΈ Π΄ΠΈΡΡΡΠ·ΠΈΠΎΠ½Π½ΡΡ
ΡΠ»ΠΎΠ΅Π²
Nb3Sn ΠΈ Π½Π° ΡΡΠ΅Π΄Π½ΠΈΠΉ ΡΠ°Π·ΠΌΠ΅Ρ Π·Π΅ΡΠ΅Π½ ΡΠ²Π΅ΡΡ
ΠΏΡΠΎΠ²ΠΎΠ΄ΡΡΠ΅ΠΉ ΡΠ°Π·Ρ. ΠΡΡΠ²Π»Π΅Π½Π° ΠΊΠΎΡΡΠ΅Π»ΡΡΠΈΡ ΠΌΠ΅ΠΆΠ΄Ρ ΡΡΠ΅Π΄Π½ΠΈΠΌ
ΡΠ°Π·ΠΌΠ΅ΡΠΎΠΌ Π·Π΅ΡΠ΅Π½ ΡΠ°Π·Ρ Nb3Sn ΠΈ ΠΊΡΠΈΡΠΈΡΠ΅ΡΠΊΠΎΠΉ ΠΏΠ»ΠΎΡΠ½ΠΎΡΡΡΡ ΡΠΎΠΊΠ° ΡΠ²Π΅ΡΡ
ΠΏΡΠΎΠ²ΠΎΠ΄Π½ΠΈΠΊΠ°.Multifilamentary superconducting bronze-processed Nb/Cu-Sn composites doped with Ti have been studied
by transmission and scanning electron microscopy. The effect of doping mode (artificial doping of Nb
filaments by inserts of NbTi alloy or Ti doping of the bronze matrix) and external wire diameter on the
morphology of Nb filaments and Nb3Sn layers and on grain sizes of the superconducting phase has been
revealed. Correlation between the average grain size of Nb3Sn phase and critical current density of a
composite is demonstrated
Effect of Doping Mode and Composite Geometry on the Structure of Nanocrystalline Nb<sub>3</sub>Sn Layers in Superconducting Nb/Cu-Sn Composites
ΠΠ΅ΡΠΎΠ΄Π°ΠΌΠΈ ΠΏΡΠΎΡΠ²Π΅ΡΠΈΠ²Π°ΡΡΠ΅ΠΉ ΠΈ ΡΠΊΠ°Π½ΠΈΡΡΡΡΠ΅ΠΉ ΡΠ»Π΅ΠΊΡΡΠΎΠ½Π½ΠΎΠΉ ΠΌΠΈΠΊΡΠΎΡΠΊΠΎΠΏΠΈΠΈ Ρ ΠΏΡΠΈΠ²Π»Π΅ΡΠ΅Π½ΠΈΠ΅ΠΌ ΠΊΠΎΠ»ΠΈΡΠ΅ΡΡΠ²Π΅Π½Π½ΠΎΠ³ΠΎ ΠΌΠΈΠΊΡΠΎΠ°Π½Π°Π»ΠΈΠ·Π° ΠΈΠ·ΡΡΠ΅Π½Ρ ΠΌΠ½ΠΎΠ³ΠΎΠ²ΠΎΠ»ΠΎΠΊΠΎΠ½Π½ΡΠ΅ ΡΠ²Π΅ΡΡ
ΠΏΡΠΎΠ²ΠΎΠ΄ΡΡΠΈΠ΅ ΠΊΠΎΠΌΠΏΠΎΠ·ΠΈΡΡ Nb/Cu-Sn, ΠΈΠ·Π³ΠΎΡΠΎΠ²Π»Π΅Π½Π½ΡΠ΅ "Π±ΡΠΎΠ½Π·ΠΎΠ²ΡΠΌ" ΠΌΠ΅ΡΠΎΠ΄ΠΎΠΌ ΠΈ Π»Π΅Π³ΠΈΡΠΎΠ²Π°Π½Π½ΡΠ΅ ΡΠΈΡΠ°Π½ΠΎΠΌ. Π£ΡΡΠ°Π½ΠΎΠ²Π»Π΅Π½ΠΎ Π²Π»ΠΈΡΠ½ΠΈΠ΅ ΡΠΏΠΎΡΠΎΠ±Π° Π»Π΅Π³ΠΈΡΠΎΠ²Π°Π½ΠΈΡ ("ΠΈΡΠΊΡΡΡΡΠ²Π΅Π½Π½ΠΎΠ΅" Π»Π΅Π³ΠΈΡΠΎΠ²Π°Π½ΠΈΠ΅ Nb-Π²ΠΎΠ»ΠΎΠΊΠΎΠ½ ΡΠΏΠ»Π°Π²ΠΎΠΌ ΠΠ’50 ΠΈΠ»ΠΈ Π»Π΅Π³ΠΈΡΠΎΠ²Π°Π½ΠΈΠ΅ ΡΠΈΡΠ°Π½ΠΎΠΌ Π±ΡΠΎΠ½Π·ΠΎΠ²ΠΎΠΉ ΠΌΠ°ΡΡΠΈΡΡ) ΠΈ Π²Π½Π΅ΡΠ½Π΅Π³ΠΎ Π΄ΠΈΠ°ΠΌΠ΅ΡΡΠ° ΠΊΠΎΠΌΠΏΠΎΠ·ΠΈΡΠ° Π½Π° ΠΌΠΎΡΡΠΎΠ»ΠΎΠ³ΠΈΡ Nb-Π²ΠΎΠ»ΠΎΠΊΠΎΠ½ ΠΈ Π΄ΠΈΡΡΡΠ·ΠΈΠΎΠ½Π½ΡΡ
ΡΠ»ΠΎΠ΅Π²
Nb3Sn ΠΈ Π½Π° ΡΡΠ΅Π΄Π½ΠΈΠΉ ΡΠ°Π·ΠΌΠ΅Ρ Π·Π΅ΡΠ΅Π½ ΡΠ²Π΅ΡΡ
ΠΏΡΠΎΠ²ΠΎΠ΄ΡΡΠ΅ΠΉ ΡΠ°Π·Ρ. ΠΡΡΠ²Π»Π΅Π½Π° ΠΊΠΎΡΡΠ΅Π»ΡΡΠΈΡ ΠΌΠ΅ΠΆΠ΄Ρ ΡΡΠ΅Π΄Π½ΠΈΠΌ
ΡΠ°Π·ΠΌΠ΅ΡΠΎΠΌ Π·Π΅ΡΠ΅Π½ ΡΠ°Π·Ρ Nb3Sn ΠΈ ΠΊΡΠΈΡΠΈΡΠ΅ΡΠΊΠΎΠΉ ΠΏΠ»ΠΎΡΠ½ΠΎΡΡΡΡ ΡΠΎΠΊΠ° ΡΠ²Π΅ΡΡ
ΠΏΡΠΎΠ²ΠΎΠ΄Π½ΠΈΠΊΠ°.Multifilamentary superconducting bronze-processed Nb/Cu-Sn composites doped with Ti have been studied
by transmission and scanning electron microscopy. The effect of doping mode (artificial doping of Nb
filaments by inserts of NbTi alloy or Ti doping of the bronze matrix) and external wire diameter on the
morphology of Nb filaments and Nb3Sn layers and on grain sizes of the superconducting phase has been
revealed. Correlation between the average grain size of Nb3Sn phase and critical current density of a
composite is demonstrated