118 research outputs found

    The challenge of balance (1996)

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    "3/96/3M.""Stress management. ""Information from Human Environmental Sciences Extension.

    Positive discipline and child guidance (2007)

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    "Information from Human Environmental Sciences Extension.""Child development."New 10/98, Revised 4/07/Web

    Synthesis and characterization of some heterocyclic including oxazoles,Thiazoles, Pyridazines, phthalizines and Pyrazoles with evaluating of biological activity.

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    A series of new compounds including p-bromo methyl pheno acetate [2]. N-( aminocarbonyl)–p-bromo pheno acetamide [3] , N-( aminothioyl) -p-bromo phenoacetyl amide [4], N-[4-(p-di phenyl)-1,3-oxazol-2-yl]-p-bromopheno acetamide [5],N-[4-p-di phenyl]-1,3-thiazol-2-yl-p-bromo phenoacet amide [6], p-bromopheno acetic acid hydrazide [7] , 1-N-(p-bromo pheno acetyl)-1,2-dihydro-pyridazin-3,6- dione [8], 1-N-(p-bromo pheno acetyl)-1,2-dihydro-phthalazin-3,8- dione[ 9], 1-(p-bromo pheno acetyl)-3-methylpyrazol-5-one [10] and 1-(p-bromo phenol acetyl)- 3,5-dimethyl pyrazole [11] have been synthesized. The prepared compounds were characterized by m.p.,FT-IR and 1H-NMR spectroscopy. Also ,the biological activity was evaluated

    Automatic Diagnosis of Distortion Type of Arabic /r/ Phoneme Using Feed Forward Neural Network

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    The paper is not for recognizing normal formed speech but for distorted speech via examining the ability of feed forward Artificial Neural Networks (ANN) to recognize speech flaws. In this paper we take the Arabic /r/ phoneme distortion that is somewhat common among native speakers as a case study.To do this, r-Distype program is developed as a script written using Praat speech processing software tool. r-Distype program automatically develops a feed forward ANN that tests the spoken word (which includes /r/ phoneme) to detect any possible type of distortion. Multiple feed forward ANNs of different architectures have been developed and their achievements reported. Training data and testing data of the developed ANNs are sets of spoken Arabic words that contain /r/ phoneme in different positions so they cover all distortion types of Arabic /r/ phoneme. These sets of words were produced by different genders and different ages.The results obtained from developed ANNs were used to draw a conclusion about automating the detection of pronunciation problems in general.Such computerised system would be a good tool for diagnosing speech flaws and gives a great help in speech therapy. Also, the idea itself may open a new research subarea of speech recognition that is automatic speech therapy. Keywords: Distortion, Arabic /r/ phoneme, articulation disorders, Artificial Neural Network, Praa

    Synthesis and Characterization of Five, Sevene Heterocyclic Membered Rings

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    New compounds containing heterocyclic units have been synthesized. These compounds include 2-amino 5- phenyl-1,3,4-thiadiazole (1) as starting material to prepare the Schiff bases 2N[3-nitrobenzylidene -2 hydroxy benzylidene and 4-N,N-dimethyl aminobenzylidene] -5-phenyl-1,3,4-thiadiazole (2abc) , 2N[3-nitrophenyl, 2-hydroxyphenyl or 4-N,N-dimethylaminophenyl] 3-]2-amino-5-phenyl-1,3,4-thiadiazole]-2,3-dihydro-[1,3]oxazepine-benzo-4,7-dione] (3abc), 2N[3-nitrophenyl,2-hydroxyphenyl,4-N,N-dimethylaminophenyl]-3-[2-amino-5-phenyl-1,3,4-thiadiazole-2-yl]-2,3-dihydro-[1,3]oxazepine-4,7-dione[(4abc), 2-N-[3-nitrophenyl, 2-hydroxyphenyl or 4-N,N-dimethylaminophenyl]-3-[2-amino-5-phenyl-1,3,4-thiadiazole-2yl]-1,2,3-trihydro-benzo-[1,2-e][1,3] diazepine-4,7-dione (5abc) ,2N[2-(3-nitrophenyl,2-hydroxyphenyl or 4-N,N-dimethylaminophenyl)]-4-oxo-1,3-thiazolidine-3-yl]-2-amino-5-phenyl-1,3,4-thiadiazole (6abc), 2-N-[5-(3-nitrophenyl,2-hydroxyphenyl or 4-N,N-dimethylaminophenyl)-tetrazolo-1-yl]-2-amino-5-phenyl-1,3,4-thiadiazole (7abc) , 2-N-[5-(3-nitrophenyl,2-hydroxyphenyl or 4-N,N-dimethylaminophenyl)-3-[2-amino-5-phenyl-1,3,4-thiadiazole-2-yl]-2,3-dihydro-[1,3]oxazepine-benzo-4,7-dithione (8abc) , 2-N-[5-(3-nitrophenyl,2-hydroxyphenyl or 4-N,N-dimethylaminophenyl)-3-[2-amino-5-phenyl-1,3,4-thiadiazole-2-yl]-2,3-dihydro-[1,3]oxazepine -4,7-dithione -5-ene (9abc) and 2-N-[5-(3-nitrophenyl,2-hydroxyphenyl or 4-N,N-dimethylaminophenyl)-3-[2-amino-5-phenyl-1,3,4-thiadiazole-2-yl] -1,2,3-trihydro-benzo-[1,2-e][1,3] diazepine -4,7-dithione - (10abc) . the structures of these compounds were characterized by FT-IR, 1H,13C-NMR,Uv/vis spectroscopy and the melting points were determined besides the evaluation of its biological activity

    Molecularly imprinted nanoparticles based sensor for cocaine detection

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    The development of a sensor based on molecularly imprinted polymer nanoparticles (nanoMIPs) and electrochemical impedance spectroscopy (EIS) for the detection of trace levels of cocaine is described in this paper. NanoMIPs for cocaine detection, synthesized using a solid phase, were applied as the sensing element. The nanoMIPs were first characterized by Transmission Electron Microscopy (TEM) and Dynamic Light Scattering and found to be ~148.35 ± 24.69 nm in size, using TEM. The nanoMIPs were then covalently attached to gold screen-printed electrodes and a cocaine direct binding assay was developed and optimized, using EIS as the sensing principle. EIS was recorded at a potential of 0.12 V over the frequency range from 0.1 Hz to 50 kHz, with a modulation voltage of 10 mV. The nanoMIPs sensor was able to detect cocaine in a linear range between 100 pg mL−1 and 50 ng mL−1 (R2 = 0.984; p-value = 0.00001) and with a limit of detection of 0.24 ng mL−1 (0.70 nM). The sensor showed no cross-reactivity toward morphine and a negligible response toward levamisole after optimizing the sensor surface blocking and assay conditions. The developed sensor has the potential to offer a highly sensitive, portable and cost-effective method for cocaine detection

    Effect of cytokinins and auxins on micropropagation of shoot tip and nodal explants of two cultivars of sweet potato (Ipomoea batatas (L) Lam)

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         In vitro propagation of two selected cultivars of sweet potato (Ipomoea batatas (L) Larn), Baladi White (BW) and Nigerian (N) were investigated using shoot tips and nodal explants during the period March, 1997 to July, 1998. Shoot regeneration from both cultivars was best on Murashige and Skoog (1962) medium without plant growth regulators. Morphogenetic response varied with the different types of explants and genotypes of sweet potato. Shoot morphogenesis from the sweet potato cv. BW was better than that from cv. N. Shoot tip explant was better for in vitro propagation of sweet potato cv. N. , while nodal cuttings were. better for cv. BW. The shoot regeneration rate induced on benzylaminopurine (BAP) was higher than that on kinetin. BAP in combination with naphthalene acetic acid (NAA) resulted in shoot and root morphogenesis from nodal explants of the sweet potato cv. N. The best shoot length was found on Murashige and Skoog medium (MS) supplemented with NAA at both 0.25 and 1.0 mg/l combined with 0.5 mg/l BAP

    2D-HEC-RAS Modeling of Flood Wave Propagation in a Semi-Arid Area Due to Dam Overtopping Failure

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    Dam overtopping failure and the resulting floods are hazardous events that highly impact the inundated areas and are less predictable. The simulation of the dam breach failure and the flood wave propagation is necessary for assessing flood hazards to provide precautions. In the present study, a two-dimensional HEC-RAS model was used to simulate the flood wave resulting from the hypothetical failure of Al-Udhaim Dam on Al-Udhaim River, Iraq, and the propagation of the resulting dam-break wave along 100 km downstream the dam site for the overtopping scenario. The main objective is to analyze the propagation of the flood wave so that the failure risk on dam downstream areas can be assessed and emergency plans may be provided. The methodology consisted of two sub-models: the first is the dam breach failure model for deriving the breach hydrograph, and the second is the hydrodynamic model for propagating the flood wave downstream of the dam. The breach hydrograph is used as an upstream boundary condition to derive the flood impact in the downstream reach of Al- Udhaim River. The flood inundation maps were visualized in RAS-Mapper in terms of water surface elevation, water depth, flow velocity, and flood arrival time. The maximum recorded values were: 105 m (a.m.s.l.), 18 m, 5.5 m/s, and, respectively. The flow velocity decreased from upstream to downstream of the terrain, which means less risk of erosion in the far reaches downstream of the study area. The inundation maps indicated that the water depth and flow velocity were categorized as Catastrophic limits on the terrain's area. The results offer a way to predict flood extent and showed that the impact of a potential dam break at Al-Udhiam Dam will be serious, therefore, suitable management is needed to overcome this risk. Moreover, the maps produced by this study are useful for developing plans for sustainable flood management. Doi: 10.28991/cej-2021-03091739 Full Text: PD

    Determination of the Levels of Polycyclic Aromatic Hydrocarbons in Toasted Bread Using Gas Chromatography Mass Spectrometry

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    Concentration of 16 polycyclic aromatic hydrocarbons (PAHs) in eighteen baked bread samples using gas oven toasting were evaluated in this study. Samples were classified into the following categories: (1) bread baked from white wheat flour, (2) bread baked from brown wheat flour, and (3) sandwich bread baked from white wheat flour. Analysis was performed by GC-MS after Soxhlet extraction of the sample and clean up of the extract. The levels of B[a]P was not detected in ten of eighteen samples. In the rest of the samples, B[a]P are varied from 2.83 to 16.54 μg/kg. B[a]A, CHR, B[b]FA, B[k] FA, IP, DB[a,h]A, and B[ghi]P concentrations were found to be less than 10.0 μg/kg. However, B[a]P are not detected in original white and brown wheat flour. The total PAHs were varied in the range 1.06–44.24 μg/kg and 3.08–278.66 μg/kg for H-PAH and L-PAH, respectively. Reproducibility and repeatability of the proposed method was calculated and presented in terms of recovery and relative standard deviations (RSD, %). Recoveries were varied from 72.46% to 99.06% with RSD ± 0.28–15.01% and from 82.39% to 95.01% with RSD ±1.91–13.01% for repeatability and reproducibility, respectively. Different commercialized samples of toasted bread were collected and analyzed
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