112 research outputs found
Furosemide determination by first-derivative spectrophotometric method
Furosemide was analyzed in tablet and liquid pharmaceutical preparations entirely and after photolitic degradation, by direct ultraviolet first derivative spectrophotometry D-1 at 262 nm. At this wavelength, it was possible to eliminate the decomposition product interference. A linear response range between 1.0 and 10.0 mu g mL(-1) was obtained in optimized conditions. The estimation of relative standard deviation was within the range 0.37-2.4% (n = 10). The method was applied in pharmaceutical preparation samples, and the results were compared with those obtained with normal spectrophotometric method to determine furosemide with advantages as high selective, accuracy and precision.3871159116
Lasersystem fuer die flexible Fertigung (LASFLEX) Abschlussbericht
Scientific and technical results were obtained investigating different methods, techniques and systems, i.e. discharge techniques, measuring methods for analysis of the discharge homogeneity, high-frequency discharge, microwave excitation, medium-frequency excitation with switched-mode power supply units, optical resonators, active media, resonator components, interaction of active and optical components with reactor radiation fields, empty resonators, optical perturbations and modulation techniques, gain switch modulation, optomechanical modulation, oscillator amplifyer systems, units for laser beam diagnosis, beam position detectors, sensors for the time-resolved measurement of overall laser ratings, laser calorimeters, rapid pyroelectric detector rows, beam-scanning intensity measurement uses, control of laser beam parameters. (HK)Die wissenschaftlichen und technischen Ergebnisse der ausfuehrlich dargestellten Arbeiten lassen sich, nach den Arbeitsgebieten gegliedert, wie folgt zusammenfassen: Im einzelnen beschrieben werden Entladungstechniken, Messverfahren zur Analyse der Entladungshomogenitaet, Hochfrequenzentladung, Mikrowellenanregung, Mittelfrequenzanregung mit Schaltnetzteilen, Untersuchung von optischen Resonatoren und des aktiven Mediums und von Resonator Komponenten, Wechselwirkung von aktiven und optischen Komponenten mit Reaktorstrahlungsfeld, leere Resonatoren, Untersuchung der optischen Rueckwirkung und von Modulationstechniken, Modulation ueber Gain-Switch, optomechanische Modulation, Untersuchung von Oszillator-Verstaerkersystemen, Entwicklung und Untersuchung von Einheiten zur Laserstrahldiagnostik, Strahllagedetektor, Sensor zur zeitaufgeloesten Messung der Lasergesamtleistung, Laserkalorimeter, schnelle pyroelektrische Detektorzeile, Charakterisierung des Einsatzbereichs von strahlabtastenden Intensitaetsmessverfahren, und Regelung von Laserstrahlparametern. (HK)Available from TIB Hannover: F94B467+a / FIZ - Fachinformationszzentrum Karlsruhe / TIB - Technische InformationsbibliothekSIGLEBundesministerium fuer Forschung und Technologie (BMFT), Bonn (Germany)DEGerman
Prozessueberwachung und Qualitaetssicherung in der Lasermaterialbearbeitung
The present volume contains lecture documents (viewgraphs) of the symposium ''Process Monitoring and Quality Assurance in Laser Material Processing''. Addressed are, among others: - Methods and Equipment for Beam Diagnostics; -Detection of Seam Incidence, Edge Offset, and Degree of Root Penetration; -Spectroscopic Monitoring of the Welding Process; - Detection of Welding Chips; -Monitoring of the Cutting Process; - Controlled Laser Beam Soldering; -Temperature Control for Transformation Hardening by Means of CO_2 Lasers; -Method for the Control of the Hole Punching Process for Laser Beam Cutting. (HM)Available from TIB Hannover: F94B1141 / FIZ - Fachinformationszzentrum Karlsruhe / TIB - Technische InformationsbibliothekSIGLEDEGerman
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