Studies of cracking behavior in melt-processed YBCO bulk superconductors

An important phenomenon in bulk superconductors fabricated by top-seeded-melt growth (TSMG) is the formation of cracks due to the inherent brittleness of the YBa2Cu3O7-δ (Y-123) phase matrix. These form during the fabrication of the superconducting monolith and play an important role in the limitation of current flow. However, cracks may also form during cooling cycles of the sample to liquid nitrogen temperatures. In this investigation, macrocracks along the c-direction, in particular were analyzed microscopically before and after cooling. In addition we attempt to resolve the c-axis macrocrack formation pattern using the magnetoscan technique

A Novel Magnetoscan Setup

Due to a modification in the original magnetoscan setup, a significant improvement in resolution was obtained. The paper focuses on experimental results which should support the idea of the new setup using two magnets with opposite direction of magnetization. This contribution to the characterization techniques of melt-grown bulk superconductors should promote the easy installation of this technique in industry. The improved magnetoscan technique may further help to investigate growth-induced inhomogeneities of the top-seeded-melt-growth process in the submillimeter range, and it offers new possibilities to the characterization of smaller structures such as superconducting films or coated conductors.Comment: 7 pages, 7 figure

"Magnetoscan": A Modified Hall Probe Scanning Technique for the Detection of Inhomogeneities in Bulk High Temperature Superconductors

We present a novel technique for the investigation of local variations of the critical current density in large bulk superconductors. In contrast to the usual Hall probe scanning technique, the sample is not magnetized as a whole before the scan, but locally by a small permanent magnet, which is fixed near the Hall probe, during the scanning process. The resulting signal can be interpreted as a qualitative measure of the local shielding currents flowing at the surface.Comment: 8 pages, 4 figure

Quantitative assessment of pinning forces and the superconducting gap in NbN thin films from complementary magnetic force microscopy and transport measurements

Epitaxial niobium-nitride thin films with a critical temperature of Tc=16K and a thickness of 100nm were fabricated on MgO(100) substrates by pulsed laser deposition. Low-temperature magnetic force microscopy (MFM) images of the supercurrent vortices were measured after field cooling in a magnetic field of 3mT at various temperatures. Temperature dependence of the penetration depth has been evaluated by a two-dimensional fitting of the vortex profiles in the monopole-monopole model. Its subsequent fit to a single s-wave gap function results in the superconducting gap amplitude Delta(0) = 2.9 meV = 2.1*kB*Tc, in perfect agreement with previous reports. The pinning force has been independently estimated from local depinning of individual vortices by lateral forces exerted by the MFM tip and from transport measurements. A good quantitative agreement between the two techniques shows that for low fields, B << Hc2, MFM is a powerful and reliable technique to probe the local variations of the pinning landscape. We also demonstrate that the monopole model can be successfully applied even for thin films with a thickness comparable to the penetration depth.Comment: 6 pages, 6 figures, 2 table

Coulomb-correlated electron number states in a transmission electron microscope beam

We demonstrate the generation of Coulomb-correlated pair, triple and quadruple states of free electrons by femtosecond photoemission from a nanoscale field emitter inside a transmission electron microscope. Event-based electron spectroscopy allows a spatial and spectral characterization of the electron ensemble emitted by each laser pulse. We identify distinctive energy and momentum correlations arising from acceleration-enhanced interparticle energy exchange, revealing strong few-body Coulomb interactions at an energy scale of about two electronvolts. State-sorted beam caustics show a discrete increase in virtual source size and longitudinal source shift for few-electron states, associated with transverse momentum correlations. We observe field-controllable electron antibunching, attributed primarily to transverse Coulomb deflection. The pronounced spatial and spectral characteristics of these electron number states allow filtering schemes that control the statistical distribution of the pulse charge. In this way, the fraction of specific few-electron states can be actively suppressed or enhanced, facilitating the preparation of highly non-Poissonian electron beams for microscopy and lithography, including future heralding schemes and correlated multi-electron probing

Bulk high-Tc superconductors with drilled holes: how to arrange the holes to maximize the trapped magnetic flux ?

Drilling holes in a bulk high-Tc superconductor enhances the oxygen annealing and the heat exchange with the cooling liquid. However, drilling holes also reduces the amount of magnetic flux that can be trapped in the sample. In this paper, we use the Bean model to study the magnetization and the current line distribution in drilled samples, as a function of the hole positions. A single hole perturbs the critical current flow over an extended region that is bounded by a discontinuity line, where the direction of the current density changes abruptly. We demonstrate that the trapped magnetic flux is maximized if the center of each hole is positioned on one of the discontinuity lines produced by the neighbouring holes. For a cylindrical sample, we construct a polar triangular hole pattern that exploits this principle; in such a lattice, the trapped field is ~20% higher than in a squared lattice, for which the holes do not lie on discontinuity lines. This result indicates that one can simultaneously enhance the oxygen annealing, the heat transfer, and maximize the trapped field

Symmetry and disorder of the vitreous vortex lattice in an overdoped BaFe_{2-x}Co_xAs_2 superconductor: Indication for strong single-vortex pinning

The disordered flux line lattice in single crystals of the slightly overdoped aFe_{2-x}Co_xAs_2 (x = 0.19, Tc = 23 K) superconductor is studied by magnetization measurements, small-angle neutron scattering (SANS), and magnetic force microscopy (MFM). In the whole range of magnetic fields up to 9 T, vortex pinning precludes the formation of an ordered Abrikosov lattice. Instead, a vitreous vortex phase (vortex glass) with a short-range hexagonal order is observed. Statistical processing of MFM datasets lets us directly measure its radial and angular distribution functions and extract the radial correlation length \zeta. In contrast to predictions of the collective pinning model, no increase in the correlated volume with the applied field is observed. Instead, we find that \zeta decreases as 1.3*R1 ~ H^(-1/2) over four decades of the applied magnetic field, where R1 is the radius of the first coordination shell of the vortex lattice. Such universal scaling of \zeta implies that the vortex pinning in iron arsenides remains strong even in the absence of static magnetism. This result is consistent with all the real- and reciprocal-space vortex-lattice measurements in overdoped as-grown aFe_{2-x}Co_xAs_2 published to date and is thus sample-independent. The failure of the collective pinning model suggests that the vortices remain in the single-vortex pinning limit even in high magnetic fields up to 9 T.Comment: 11 pages, 6 figure

Symmetry and disorder of the vitreous vortex lattice in an overdoped BaFe_{2-x}Co_xAs_2 superconductor: Indication for strong single-vortex pinning

The disordered flux line lattice in single crystals of the slightly overdoped aFe_{2-x}Co_xAs_2 (x = 0.19, Tc = 23 K) superconductor is studied by magnetization measurements, small-angle neutron scattering (SANS), and magnetic force microscopy (MFM). In the whole range of magnetic fields up to 9 T, vortex pinning precludes the formation of an ordered Abrikosov lattice. Instead, a vitreous vortex phase (vortex glass) with a short-range hexagonal order is observed. Statistical processing of MFM datasets lets us directly measure its radial and angular distribution functions and extract the radial correlation length \zeta. In contrast to predictions of the collective pinning model, no increase in the correlated volume with the applied field is observed. Instead, we find that \zeta decreases as 1.3*R1 ~ H^(-1/2) over four decades of the applied magnetic field, where R1 is the radius of the first coordination shell of the vortex lattice. Such universal scaling of \zeta implies that the vortex pinning in iron arsenides remains strong even in the absence of static magnetism. This result is consistent with all the real- and reciprocal-space vortex-lattice measurements in overdoped as-grown aFe_{2-x}Co_xAs_2 published to date and is thus sample-independent. The failure of the collective pinning model suggests that the vortices remain in the single-vortex pinning limit even in high magnetic fields up to 9 T.Comment: 11 pages, 6 figure

DC superconducting quantum interference devices fabricated using bicrystal grain boundary junctions in Co-doped BaFe2As2 epitaxial films

DC superconducting quantum interference devices (dc-SQUIDs) were fabricated in Co-doped BaFe2As2 epitaxial films on (La, Sr)(Al, Ta)O3 bicrystal substrates with 30deg misorientation angles. The 18 x 8 micro-meter^2 SQUID loop with an estimated inductance of 13 pH contained two 3 micro-meter wide grain boundary junctions. The voltage-flux characteristics clearly exhibited periodic modulations with deltaV = 1.4 micro-volt at 14 K, while the intrinsic flux noise of dc-SQUIDs was 7.8 x 10^-5 fai0/Hz^1/2 above 20 Hz. The rather high flux noise is mainly attributed to the small voltage modulation depth which results from the superconductor-normal metal-superconductor junction nature of the bicrystal grain boundary

Epitaxial growth and anisotropy of La(O,F)FeAs thin films deposited by Pulsed Laser Deposition

LaFeAsO1-xFx thin films were deposited successfully on (001)-oriented LaAlO3 and MgO substrates from stoichiometric LaFeAsO1-xFx polycrystalline targets with fluorine concentrations up to x = 0.25 by PLD. Room temperature deposition and post annealing of the films yield nearly phase pure films with a pronounced c-axis texture and a strong biaxial in-plane orientation. Transport measurements show metallic resistance and onset of superconductivity at 11 K. Hc2(T) was determined by resistive measurements and yield Hc2 values of 3 T at 3.6 K for B||c and 6 T at 6.4 K for B||ab.Comment: 11 pages, 5 figure