A Radio Frequency Non-reciprocal Network Based on Switched Low-loss Acoustic Delay Lines

This work demonstrates the first non-reciprocal network based on switched low-loss acoustic delay lines. A 21 dB non-reciprocal contrast between insertion loss (IL=6.7 dB) and isolation (28.3 dB) has been achieved over a fractional bandwidth of 8.8% at a center frequency 155MHz, using a record low switching frequency of 877.22 kHz. The 4-port circulator is built upon a newly reported framework by the authors, but using two in-house fabricated low-loss, wide-band lithium niobate (LiNbO3) delay lines with single-phase unidirectional transducers (SPUDT) and commercial available switches. Such a system can potentially lead to future wide-band, low-loss chip-scale nonreciprocal RF systems with unprecedented programmability.Comment: 4 pages, 7 figure

Optimization and design of radio frequency piezoelectric MEMS resonators

Radio frequency (RF) microelectromechanical system (MEMS) resonators employing Lamb waves propagating in piezoelectric thin films have recently attracted much attention since they combine the advantages of the bulk acoustic wave (BAW) and surface acoustic wave (SAW) technologies: high phase velocity and multiple frequencies on a single chip. In particular, aluminum nitride (AlN) resonators based on fundamental symmetric (S0) Lamb mode have shown great promise because they can offer high phase velocities (10,000 m/s), low dispersive phase velocity characteristic, small temperature-induced frequency drift, low motional resistance, and monolithic integration compatibility with complementary metal–oxide–semiconductor (CMOS). However, there are still a few outstanding technical challenges, including spurious modes suppression, quality factor (Q) enhancement, frequency scalability, and electromechanical coupling improvement. These issues obstruct the wide deployment and commercialization of AlN Lamb mode resonators. This dissertation presents comprehensive investigations and solutions to these issues. This thesis is organized as follows: Chapter 1 gives a brief introduction of the basics on piezoelectric MEMS resonators and their promising applications. Chapter 2 first investigates the various available Lamb wave modes in AlN and then identifies the S0 mode as the promising resonator solution to overcome several challenges associated with SOA. Chapter 2 also discusses several outstanding challenges with S0 devices, including spurious mode suppression, Q enhancement, scaling resonant frequency, and enlarging fractional bandwidth. In response, Chapters 3-7 address these outstanding challenges by developing new designs and models, resorting to new acoustic mode, and incorporating new piezoelectric material. More specifically, Chapter 3 proposes two techniques to suppress the spurious modes in the responses of S0 resonators, namely mode conversion and mode shifting. Chapter 4 address the challenge of a conventionally vague question of reflection at the interface between released and unreleased regions in S0 resonators, and then demonstrates Q enhanced resonators with defined released regions achieved by a sandbox process. Chapter 5 first characterizes the S1 Lamb mode and optimizes its resonator configuration. A high-frequency S1 resonator at 3.5 GHz with a coupling of 3.5% is fabricated and demonstrated. Chapter 6 presents a hybrid filtering topology with a mode conversion AlN S0 resonator and lumped elements for widening the bandwidths of resonator-based filters. Chapter 7 proposes lithium niobate (LiNbO3) multilayered resonators with large electromechanical coupling, structure robustness, and good temperature stability. The analysis of Bragg reflectors, resonator simulation, stress control, fabrication, and measurements are covered in this chapter

Optimization and design of radio frequency piezoelectric MEMS resonators

Radio frequency (RF) microelectromechanical system (MEMS) resonators employing Lamb waves propagating in piezoelectric thin films have recently attracted much attention since they combine the advantages of the bulk acoustic wave (BAW) and surface acoustic wave (SAW) technologies: high phase velocity and multiple frequencies on a single chip. In particular, aluminum nitride (AlN) resonators based on fundamental symmetric (S0) Lamb mode have shown great promise because they can offer high phase velocities (10,000 m/s), low dispersive phase velocity characteristic, small temperature-induced frequency drift, low motional resistance, and monolithic integration compatibility with complementary metal–oxide–semiconductor (CMOS). However, there are still a few outstanding technical challenges, including spurious modes suppression, quality factor (Q) enhancement, frequency scalability, and electromechanical coupling improvement. These issues obstruct the wide deployment and commercialization of AlN Lamb mode resonators. This dissertation presents comprehensive investigations and solutions to these issues. This thesis is organized as follows: Chapter 1 gives a brief introduction of the basics on piezoelectric MEMS resonators and their promising applications. Chapter 2 first investigates the various available Lamb wave modes in AlN and then identifies the S0 mode as the promising resonator solution to overcome several challenges associated with SOA. Chapter 2 also discusses several outstanding challenges with S0 devices, including spurious mode suppression, Q enhancement, scaling resonant frequency, and enlarging fractional bandwidth. In response, Chapters 3-7 address these outstanding challenges by developing new designs and models, resorting to new acoustic mode, and incorporating new piezoelectric material. More specifically, Chapter 3 proposes two techniques to suppress the spurious modes in the responses of S0 resonators, namely mode conversion and mode shifting. Chapter 4 address the challenge of a conventionally vague question of reflection at the interface between released and unreleased regions in S0 resonators, and then demonstrates Q enhanced resonators with defined released regions achieved by a sandbox process. Chapter 5 first characterizes the S1 Lamb mode and optimizes its resonator configuration. A high-frequency S1 resonator at 3.5 GHz with a coupling of 3.5% is fabricated and demonstrated. Chapter 6 presents a hybrid filtering topology with a mode conversion AlN S0 resonator and lumped elements for widening the bandwidths of resonator-based filters. Chapter 7 proposes lithium niobate (LiNbO3) multilayered resonators with large electromechanical coupling, structure robustness, and good temperature stability. The analysis of Bragg reflectors, resonator simulation, stress control, fabrication, and measurements are covered in this chapter.LimitedAuthor requested closed access (OA after 2yrs) in Vireo ETD syste

Optimizing nitrifying community and achieving partial nitrification with real-time control

A pilot-plant sequencing batch reactor (SBR) with a working volume of 54 m was used in the experiment on biological nitrogen removal via nitrite from municipal wastewater with low COD/N ratio for saving energy and carbon sources. At normal water temperature, the feasibility of achieving and stabilizing nitrogen removal via nitrite from municipal wastewater with the low COD/N ratio (average 2.16) was investigated. The obtained resulted showed that the total nitrogen (TN) in the effluent was less than 3 mg/L and the advanced nitrogen removal was obtained through application of step-feed operation. Moreover, by using the real-time control strategies, the nitrifying communities were optimized. Thus, under normal dissolved oxygen (DO) condition, nitrogen removal via nitrite was successfully achieved at the range of temperature between 12°C to 26°C,. Nitrogen removal via nitrite kept the long-term stability (180 days) and the average NO-N/NOx-N ratio was above 95%. The fluorescence in situ hybridization (FISH) was performed to analyze the quantitative changes of nitrifying microbial communities in the activated sludge. The results also indicated that ammonia-oxidizing bacteria (AOB) became the dominant nitrifying bacteria and nitrite-oxidizing bacteria (NOB) had been washed out of the activated sludge. It indicated that the nitrifying microbial communities were optimized