Modeling the deformation textures and microstructural evolutions of a Fe–Mn–C TWIP steel during tensile and shear testing

The high manganese austenitic steels with low stacking fault energy (SFE) present outstanding mechanical properties due to the occurrence of two strain mechanisms: dislocation glide and twinning. Both mechanisms are anisotropic. In this paper, we analyzed the effect of monotonous loading path on the texture, the deformation twinning and the stress–strain response of polycrystalline high Mn TWIP steel. Experimental data were compared to predicted results obtained by two polycrystalline models. These two models are based on the same single crystal constitutive equations but differ from the homogenization scheme. The good agreement between experiments and calculations suggest that the texture plays a key role in twinning activity and kinetics with regard to the intergranular stress heterogeneities. Rolling direction simple shear induces single twinning while rolling and transverse direction uniaxial tensions induce multi-twinning leading to lower twin volume fractions due to twin–twin interactions

Investigation of delamination mechanisms during a laser drilling on a cobalt-base superalloy

Temperatures in the high pressure chamber of aircraft engines are continuously increasing to improve the engine efficiency. As a result, constitutive materials such as cobalt and nickel-base superalloys need to be thermally protected. The first protection is a ceramic thermal barrier coating (TBC) cast on all the hot gas-exposed structure. The second protection is provided by a cool air layer realized by the use of a thousand of drills on the parts where a cool air is flowing through. The laser drilling process is used to realize these holes at acute angles. It has been shown on coated single crystal nickel-base superalloy that the laser drilling process causes an interfacial cracking (also called delamination), detected by a cross section observation. The present work aims at characterizing interfacial cracking induced by laser drilling on coated cobalt-base super alloy. On the one hand, this work attempted to quantify the crack by several microscopic observations with regards to the most significant process parameters related as the angle beam. On the other hand, we studied the difference of the laser/ceramic and the laser/substrate interaction with real time observation by using a fast movie camera

Impact of experimental conditions on material response during forming of steel in semi-solid state

Semi-solid forming is an effective near-net-shape forming process to produce components with complex geometry and in fewer forming steps. It benefits from the complex thixotropic behaviour of semi-solids. However, the consequences of such behaviour on the flow during thixoforming, is still neither completely characterized and nor fully understood, especially for high melting point alloys. The study described in this paper investigates thixoextrusion for C38 low carbon steel material using dies at temperatures much lower than the slug temperature. Four different process parameters were studied: the initial slug temperature, the die temperature, the ram speed and the presence of a ceramic layer at the tool/material interface. The extruded parts were found to have an exact shape and a good surface state only if the temperature was below a certain value. This critical temperature is not an intrinsic material property since its value depends on die temperature and the presence of the Ceraspray©layer. Two kinds of flow were highlighted: a homogeneous flow controlled by the behaviour of the solid skeleton characterized by a positive strain rate sensitivity, and a non homogeneous flow (macro liquid/solid phase separation) dominated by the flow of the free liquid. With decreasing ram speed, heat losses increase so that the overall consistency of the material improves, leading to apparent negative strain rate sensitivity. Finally, some ways to optimise thixoforming are proposed

Very high cycle fatigue of copper: Evolution, morphology and locations of surface slip markings

The surfaces of commercially pure polycrystalline copper specimens subjected to interrupted 20 kHz fatigue tests in the very high cycle fatigue regime were investigated. The stress amplitude needed to form the early slip markings was found twice lower than the stress amplitude required to fracture which confirmed the results obtained by Stanzl-Tschegg et al. (2007). Three types of slip markings were classified according to their morphology and their location in the polycrystalline material. They are compared to slip markings observed during fatigue tests at frequencies lower than 100 Hz and numbers of cycles lower than 107. For 20 kHz fatigue tests, stress amplitudes ranging from 45 MPa to 65 MPa produce straight and long early persistent slip markings located along twin boundaries. Stress amplitudes lower than 45 MPa produce clusters of fine early persistent slip markings mainly located at triple junctions

Modeling the deformation textures and microstructural evolutions of a Fe–Mn–C TWIP steel during tensile and shear testing

The high manganese austenitic steels with low stacking fault energy (SFE) present outstanding mechanical properties due to the occurrence of two strain mechanisms: dislocation glide and twinning. Both mechanisms are anisotropic. In this paper, we analyzed the effect of monotonous loading path on the texture, the deformation twinning and the stress–strain response of polycrystalline high Mn TWIP steel. Experimental data were compared to predicted results obtained by two polycrystalline models. These two models are based on the same single crystal constitutive equations but differ from the homogenization scheme. The good agreement between experiments and calculations suggest that the texture plays a key role in twinning activity and kinetics with regard to the intergranular stress heterogeneities. Rolling direction simple shear induces single twinning while rolling and transverse direction uniaxial tensions induce multi-twinning leading to lower twin volume fractions due to twin–twin interactions

Micromechanical modelling of twinning-induced plasticity steels

The paper discusses a number of issues related to the development of a micromechanical polycrystalline model for twinning-induced plasticity steels: twinning features that have to be incorporated, identification procedure, description of the work hardening, role of the texture and the role of the interaction law between grains. Monotonous and reverse strain paths are investigated

Microstructure and flow behaviour during backward extrusion of semi-solid 7075 aluminium alloy

The microstructure and flow behaviour during thixo backward extrusion of 7075 aluminium alloy were investigated. Reheating the steel die and the aluminium billet placed into the die at the same time using an induction furnace provides rapidly a very homogeneous microstructure suitable for thixoforming. During thixoextrusion, despite the high solid fraction, the solid globules are weakly connected and slide over each other without any plastic deformation. The flow remains quasi homogeneous resulting in homogeneous induced microstructure of the component

Impact of experimental conditions on material response during forming of steel in semi-solid state

Semi-solid forming is an effective near-net-shape forming process to produce components with complex geometry and in fewer forming steps. It benefits from the complex thixotropic behaviour of semi-solids. However, the consequences of such behaviour on the flow during thixoforming, is still neither completely characterized and nor fully understood, especially for high melting point alloys. The study described in this paper investigates thixoextrusion for C38 low carbon steel material using dies at temperatures much lower than the slug temperature. Four different process parameters were studied: the initial slug temperature, the die temperature, the ram speed and the presence of a ceramic layer at the tool/material interface. The extruded parts were found to have an exact shape and a good surface state only if the temperature was below a certain value. This critical temperature is not an intrinsic material property since its value depends on die temperature and the presence of the Ceraspray©layer. Two kinds of flow were highlighted: a homogeneous flow controlled by the behaviour of the solid skeleton characterized by a positive strain rate sensitivity, and a non homogeneous flow (macro liquid/solid phase separation) dominated by the flow of the free liquid. With decreasing ram speed, heat losses increase so that the overall consistency of the material improves, leading to apparent negative strain rate sensitivity. Finally, some ways to optimise thixoforming are proposed

Effect of Experimental Conditions on 7075 Aluminium Response During Thixoextrusion

The deformation behavior of semi-solid aluminum alloy is strongly dependent on the microstructure. This paper illustrates several experimental research works concerning thixoextrusion of 7075 aluminum alloy which was carried out at “Arts et Métiers ParisTech” of Metz. Inductive re-heating of the aluminum billet is the method used in order to obtain the target liquid fraction for thixoextrusion. To minimize the heat losses, a sample obtained from a direct extruded bar is inserted in a die for reheating in semisolid state and thixoextrusion. During the experimental re-heating process, the temperature was directly controlled by using thermocouples for temperature measurements in the sample and also in the die. The influence of different working ram speeds and reheating temperature on the microstructure evolution was studied by optical microscopy. The experimental results on extrusion load and microstructure evolution of the component are reported

Analysis of semi-solid response under rapid compression tests using multi-scale modelling and experiments

Simulating semi-solid metal forming requires modelling semi-solid behaviour. However, such modelling is difficult because semi-solid behavior is thixotropic and depends on the liquid-solid spatial distribution within the material. In order to better understand and model relationships between microstructure and behavior, a model based on micromechanical approaches and homogenisation techniques is presented. This model is an extension of a previous model established in a pure viscoplastic framework to account for elasticity. Indeed, experimental load-displacement signals reveal the presence of an elastic-type response in the earlier stages of deformation when semi-solids are loaded under rapid compression. This elastic feature of the behaviour is attributed to the response of the porous solid skeleton saturated by incompressible liquid. A good quantitative agreement is found between the elastic-viscoplastic predicted response and the experimental data. More precisely, the strong initial rising part of the load-displacement curve, the peak load and the subsequent fall in load are well captured. The effect of solid fraction on mechanical response is in qualitative agreement with experiments