26 research outputs found

    Intra-day (n = 8) accuracy and precision for TH, TAM and TAc in spiked lysed PCCL3 cell extracts in 6-well plates.

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    <p>Intra-day (n = 8) accuracy and precision for TH, TAM and TAc in spiked lysed PCCL3 cell extracts in 6-well plates.</p

    Thyronamine and thyronine chromatograms from Hep G2 cell lysate extracts spiked at 50 nM.

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    <p>2 MRM Traces per analyte, overlayed. Upper trace: T<sub>0</sub> (4.12 min); 3-T<sub>1</sub> (4.54 min); 3-T<sub>1</sub>‘ (4.80 min); 3,5-T<sub>2</sub> (4.60 min); 3,3‘-T<sub>2</sub> (5.16 min); 3‘,5‘-T<sub>2</sub> (5.35 min); T<sub>3</sub> (5.01 min); rT<sub>3</sub> (5.64 min); T<sub>4</sub> (5.36 min). Lower trace: T<sub>0</sub>AM (4.65 min); T<sub>1</sub>AM (5.30 min); 3,5-T<sub>2</sub>AM (5.34 min); T<sub>3</sub>AM (5.97 min); rT<sub>3</sub>AM (7.10 min); T<sub>4</sub>AM (inset, 6.56 min).</p

    Negative ion electrospray tandem mass spectrometry and retention time (R<sub>t</sub>) parameters for thyroacetic acids and internal standards.

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    <p>Negative ion electrospray tandem mass spectrometry and retention time (R<sub>t</sub>) parameters for thyroacetic acids and internal standards.</p

    Application of the LC-MS/MS method to extracts of PCCL3 rat thyrocytes.

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    <p>THM in extracts of PCCL3 (A, B) cell and supernatants (C, D) after incubation with 500 nM 3-T<sub>1</sub>AM (A, C) or 3-T<sub>1</sub> (B, D) in Krebs-Ringer buffer as measured by LC-MS/MS. Bars represent means of 3 independent experiments carried out on different days +/- SEM.</p

    Inter-day (n = 3) process efficiency, matrix effect and recovery for TH and TAM spiked lysed PCCL3 cell extracts in 6 well plates.

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    <p>Inter-day (n = 3) process efficiency, matrix effect and recovery for TH and TAM spiked lysed PCCL3 cell extracts in 6 well plates.</p

    Inter-day (n = 8) process efficiency, matrix effect and recovery for TH and TAM spiked lysed Hep G2 cell extracts in 24-well plates.

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    <p>Inter-day (n = 8) process efficiency, matrix effect and recovery for TH and TAM spiked lysed Hep G2 cell extracts in 24-well plates.</p
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