New approach for modelling strain induced precipitation of Nb(C,N) in HSLA steels during multipass hot deformation in austenite

A new model for strain induced precipitation of Nb(C,N) is developed from the existing model for single pass hot deformation. This new model can be extended to multipass deformation to explain the microstructural evolution during the hot deformation of Nb supersaturated high strength low alloy (HSLA) steels. The key feature of this model is the microband geometry employed, which leads to determination of the local solute concentration at microbands, and hence the potential for carbonitride precipitation on the microbands. The model also validates the need for concurrent growth and coarsening processes, even at the early stages of precipitation. The evolution of the precipitate radius, number density and volume fraction are compared with the experimental results obtained from thin foil TEM micrographs on Fe-30 wt-%Ni alloys ( that are austenitic at room temperature and are similar to HSLA steels in deformation behaviour) subjected to deformation by plane strain compression. The model predictions are in good agreement with experimental results

Effect of austenite grain size on acicular ferrite transformation in a HSLA steel

Austenite grain size is well known to have a significant influence on various phase transformations in steels. Although the effects of many thermomechanical processing parameters on acicular ferrite (AF) transformation in HSLA steels have been investigated, little attention has been paid to the influence of austenite grain size. Therefore, in this research, different parameters of solid-solution heat treatment and rough deformation were adopted to generate austenite with different grain sizes and the effects of austenite grain size before deformation on the AF transformation and grain refinement were investigated. It was found that the reduction of prior-austenite grain size (PAGS) from 62.8 μm to 37.0 μm before austenite deformation promotes the AF transformation and simultaneously refines and homogenises the transformed microstructures. A reciprocally increased density of deformation induced dislocations with the reduction of PAGS was proposed to account for these results, which not only increase the nucleation sites of AF but also suppress the lengthening of BF laths. Further reducing PAGS from 37.0 μm to 22.3 μm, the fraction of AF is not increased and the transformed microstructure is not refined. Possible differences in the type, distribution, and density of austenite deformation substructures between austenite with PAGSs of 37.0 μm and 22.3 μm were argued to be responsible for the cease of grain refinement. The relationship between effective grain sizes and the Sv parameter was investigated and an equation relating effective grain sizes with processing parameters was also proposed

Softening Kinetics of Plain Carbon Steels Containing Dilute Nb Additions

The recrystallisation and precipitation kinetics of a plain carbon steel with 0.017 % Nb were studied using the double-hit deformation technique for interpass holding of 5 and 20s. The present study focuses on the effect of prestrain and deformation temperature on recrystallisation behaviour of the investigated steel. The fractional softening was calculated based on the percentage difference between the areas under the interrupted and uninterrupted deformations flow curves. The T5% and T95%, marking the beginning and end of recrystallisation, respectively, are determined as a function of strain. Quantitative microstructural studies validated the findings from the softening studies. The predicated results of recrystallisation regime are found to be in agreement with industrial observation and other experimental measurement for this steel. It can be seen that the dilute additions of Nb can influence the static recrystallisation of austenite under certain rolling condition which may lead to improved mechanical properties of steel

Influence of cooling rate on the grain-refining effect of austenite deformation in a HSLA steel

Effective grain size is a direct indicator of the high angle grain boundary (HAGB) density of microstructures. A small effective grain size suggests a high density of HAGBs, which provide effective barriers to cleavage fracture. There have been many investigations concerning the effect of processing parameters on the effective grain sizes of steel microstructures. However, contradicting results were found for the influence of austenite deformation. In this research, to understand the influence of austenite deformation on effective grain size refinement, a low carbon Nb microalloyed steel was subjected to different austenite deformation conditions and was continuously cooled at a wide range of cooling rates (0.5–50 °C/s). Characteristics of transformed microstructures from recrystallised and deformed austenite were analysed through optical microscopy observation and EBSD mapping. In the whole cooling rate range adopted in this research, effective grain sizes were found to be refined by austenite deformation. However, with the rise of cooling rate higher than 10 °C/s. With the rise of the cooling rate higher than 10 °C/s, effective grain sizes are reduced for recrystallised austenite, while increasingly large effective grain sizes were found for deformed austenite. According to these experimental results, the influence of austenite deformation on effective grain size in a wider cooling rate range was proposed to be cooling rate dependent, and possible explanations for the contradicting results in the literature were discussed based on that

The effect of thermomechanical controlled processing on recrystallisation and subsequent deformation-induced ferrite transformation textures in microalloyed steels

The evolution of texture components for two experimental 0.06 wt% C steels, one containing 0.03 wt% Nb (Nb steel) and the second containing both 0.03 wt% Nb and 0.02 wt% Ti (Nb–Ti steel), was investigated following a new thermomechanical controlled process route, comprising first deformation, rapid reheat to 1200 °C and final deformation to various strains. Typical deformation textures were observed after first deformation for both steels. Following subsequent reheating to 1200 °C for various times, the recrystallisation textures consisted primarily of the α-(Formula presented.)//RD texture fibre with a weak γ-{111}//ND texture fibre, similar to deformation textures, indicative of the dominance of a strain-induced boundary migration mechanism. The texture components after finish deformation were different from the rough deformation textures, with a strong α-(Formula presented.)//RD texture fibre at the beginning, and then the strong peaks move to (111)(Formula presented.) and (111)(Formula presented.) textures due to the deformation-induced ferrite (DIF) transformation. The effect of Ti on the recrystallisation textures and deformation textures has also been analysed in this study. The results illustrate that Ti significantly influences the γ-{111}//ND texture fibre. Finally, the textures after deformation and recrystallisation in the austenite were calculated based on the K–S orientation relationship between the austenite and ferrite. This allowed the understanding of the mechanism of recrystallisation between first and final deformation and the DIF textures during phase transformation

A phase quantification method based on EBSD data for a continuously cooled microalloyed steel

Mechanical properties of steels depend on the phase constitutions of the final microstructures which can be related to the processing parameters. Therefore, accurate quantification of different phases is necessary to investigate the relationships between processing parameters, final microstructures and mechanical properties. Point counting on micrographs observed by optical or scanning electron microscopy is widely used as a phase quantification method, and different phases are discriminated according to their morphological characteristics. However, it is difficult to differentiate some of the phase constituents with similar morphology. Differently, for EBSD based phase quantification methods, besides morphological characteristics, other parameters derived from the orientation information can also be used for discrimination. In this research, a phase quantification method based on EBSD data in the unit of grains was proposed to identify and quantify the complex phase constitutions of a microalloyed steel subjected to accelerated coolings. Characteristics of polygonal ferrite/quasi-polygonal ferrite, acicular ferrite and bainitic ferrite on grain averaged misorientation angles, aspect ratios, high angle grain boundary fractions and grain sizes were analysed and used to develop the identification criteria for each phase. Comparing the results obtained by this EBSD based method and point counting, it was found that this EBSD based method can provide accurate and reliable phase quantification results for microstructures with relatively slow cooling rates

Influence of strain reversal on dynamic transformation in microalloyed steels deformed above the Ae₃ temperature

In the present work, the effect of strain path reversals on dynamic transformation (DT) above Ae3 temperature was studied using an API grade X-70 microalloyed steel deformed by torsion with single and multiple strain path reversals. The results revealed the important role played by strain path reversals on influencing the evolution of austenite grain boundaries through inhomogeneous deformation, therefore, affecting DT behaviours. In addition to flow stress–strain analysis and microstructure investigation, finite element method combined with 3D digital materials representation approach was used to gain insights into the effects of deformation with strain path reversals on the development of microstructural features in the prior-austenite grains

A new approach to etching low‐carbon microalloyed steels to reveal prior austenite grain boundaries and the dual‐phase microstructure

A modification to picric acid solutions has been undertaken to reveal the prior-austenite grain boundaries in microalloyed steels as a result of elemental segregation. It has been found the maximum addition of sodium dodecyl sulphate plus hydrochloric acid to fully reveal both the prior austenite grain boundaries and the final post-processed structures in these steels

Tensile Behaviour of Galvanised Grade 8.8 Bolt Assemblies in Fire

In structural fire engineering, the importance of bolt assemblies is often overlooked. Connection design uses the temperature-dependent bolt strength-reduction factors prescribed in Eurocode 3, despite the existence of two distinct failure modes under tension; necking of the bolt shank, and thread-stripping. While literature exists to predict failure modes at ambient temperature, there is no method for failure mode prediction for elevated temperatures where ductility is critical to avoid collapse. Galvanised M20 structural bolt assemblies and bolt material from a single batch have been tested under tension at a range of temperatures and strain-rates typical of those experienced in fire. Turned-down bolt test data produced stress-strain curves characteristic of different microstructures at ambient temperature, despite a tempered-martensitic microstructure being specified in the standards. The failure modes of bolt assemblies were found to be dependent on the as-received microstructure at ambient temperature. At elevated temperatures, however, only thread-stripping was observed

Influence of thermomechanical processing parameters on critical temperatures to develop an Advanced High-Strength Steel microstructure

A good selection of the thermomechanical processing parameters will optimize the function of alloying elements to get the most of mechanical properties in Advanced High-Strength Steels for automotive components, where high resistance is required for passenger safety. As such, critical processing temperatures must be defined taking into account alloy composition, in order for effective thermomechanical processing schedules to be designed. These critical temperatures mainly include the recrystallization stop temperature (T5%) and the transformation temperatures (Ar1, Ar3, Bs, etc.). These critical processing temperatures were characterized using different thermomechanical conditions. T5% was determined through the softening evaluation on double hit tests and the observation of prior austenite grain boundaries on the microstructure. Phase transformation temperatures were measured by dilatometry experiments at different cooling rates. The results indicate that the strain per pass and the interpass time will influence the most on the determination of T5%. The range of temperatures between the recrystallized and non-recrystallized regions can be as narrow as 30 °C at a higher amount of strain. The proposed controlled thermomechanical processing schedule involves getting a severely deformed austenite with a high dislocation density and deformation bands to increase the nucleation sites to start the transformation products. This microstructure along with a proper cooling strategy will lead to an enhancement in the final mechanical properties of a particular steel composition