Atomic observations of warm rolled low carbon steels alloyed with Cr and P

Extended abstract of a paper presented at Microscopy and Microanalysis 2005 in Honolulu, Hawaii, USA, July 31--August 4, 200

Microstructure and mechanical properties of thermomechanically processed C-Si-Mn steels

Comparison of the microstructures formed in the specimens produced by corresponding schedules in the dilatometer and by laboratory rolling has shown that a higher level of retained austenite was achieved in dilatometer specimens, whereas in rolled specimens a higher amount of martensite was present instead of retained austenite

Observation of Precipitation Evolution in Fe-Ni-Mn-Ti-Al Maraging Steel by Atom Probe Tomography

We describe the full decomposition sequence in an Fe-Ni-Mn-Ti-Al maraging steel during isothermal annealing at 550 °C. Following significant pre-precipitation clustering reactions within the supersaturated martensitic solid solution, (Ni,Fe)3Ti and (Ni,Fe)3(Al,Mn) precipitates eventually form after isothermal aging for ~60 seconds. The morphology of the (Ni,Fe)3Ti particles changes gradually during aging from predominantly plate-like to rod-like, and, importantly, Mn and Al were observed to segregate to these precipitate/matrix interfaces. The (Ni,Fe)3(Al,Mn) precipitates occurred at two main locations: uniformly within the matrix and at the periphery of the (Ni,Fe)3Ti particles. We relate this latter mode of precipitation to the Mn-Al segregation

A study of the strengthening mechanism in the thermomechanically processed TRIP/TWIP steel

The strengthening mechanism responsible for the unique combination of ultimate tensile strength and elongation in a multiphase Fe-0.2C-1.5Mn-1.2Si-0.3Mo-0.6Al-0.02Nb (wt%) steel was studied. The microstructures with different volume fraction of polygonal fenite, bainite and retained austenite were simulated by controlled thermomechanical processing. The interupted tensile test was used to study the bainitic ferrite, retained austenite and polygonal ferrite behavior as a function of plastic strain. X-ray analysis was used to characterize the volume fraction and carbon content of retained austenite. TEM and heat-tinting were utilized to analyze the effect of bainitic fenite morphology on the strain induced transformation of retained austenite and retained austenite twinning as a function of strain in the bulk material. The study has shown that the austenite twinning mechanism is more preferable than the transformation induced plasticity mechanism during the early stages of deformation for a microstructure containing I5% polygonal ferrite, while the transformation induced plasticity effect is the main mechanism in when there is 50% of polygonal ferrite in the microstructure. The baillitic fenite morphology affects the deformation mode of retained austenite during straining. The polygonal fenite behavior during straining depends on dislocation substructure tonned due to the deformation and the additional mobile dislocations caused by the TRIP effect. TRIP and TWIP effects depend not only on the chemical and mechanical stability of retained austenite, but also on the interaction of the phases during straining.<br /

Nanostructural Engineering of Steel

The concept of microstructural engineering of steels is well established and is the basis for a wide range of processes and products. Recently, though, there has been increasing emphasis in developing microstructures that have submicron length scales and also in understanding in far greater detail the structures and solute effects that are occurring at the nanoscale. In this review it is proposed that we are heading towards the situation where we are applying nanostructural engineering concepts in the development of new steels. A range of examples are given as well as a discussion of the potential impact of new processing routes. Clearly the future advances will be driven through improved characterization methods, such as atom probe tomography, in combination with advanced modeling

The effect of Nb, Mo, and A1 additions on the transformation behaviour and mechanical properties of thermomechanically processed C-Si-Mn trip steel

The effect of additions of Nb, A1 and Mo to Fe-C-Mn-Si TRIP steels on the final microstructure and mechanical properties after simulated thermomechanical processing (TMP) has been studied. Laboratory simulations of continuous cooling during TMP were performed using a quench deformation dilatometer, while laboratory simulations of discontinuous cooling during TMP were performed using a hot rolling mill. From this a comprehensive understanding of the structural and kinetic aspects of the bainite transformation in these types of TRIP steels has been developed. All samples were characterised using optical microscopy and XRD. The relationships between the morphology of bainitic structure, volume fraction, stability of RA and mechanical properties were investigated.<br /

Effect of niobium clustering and precipitation on strength of a NbTi-microalloyed ferritic steel

The microstructure-property relationship of an NbTi-microalloyed ferritic steel was studied as a function of thermo-mechanical schedule using Gleeble 3500 simulator, optical and scanning electron microscope, and atom probe tomography

Uloga dodataka Cr i P u razvoju mikrostrukture i teksture u žarenim niskougljičnim čelicima

The recrystallisation behaviour of four warm rolled steels was investigated during annealing. The extra-low carbon (ELC) steel displayed the highest rate of recrystallisation, the steels with additions of chromium and phosphorus (LC(Cr)), (LC(Cr,P)) recrystallised at intermediate rates, while the interstitial-free (IF) steel exhibited the lowest rate. The additions of Cr and Cr/P increased the fraction of g-fibre in the annealing textures compared to that present in the ELC steel; this effect was particularly pronounced up to 50 % recrystallisation. After the completion of recrystallisation, the steel textures were characterized by a dominant g-fibre in the IF steel, while in the three LC steels, the RD fibre was the principal one.Ispitivana je rekristalizacija četiri tipa toplo valjanih čelika tijekom žarenja. Čelik s ekstra niskim ugljikom (ELC) pokazao je najveću brzinu rekristalizacije, čelici s dodatkom kroma i fosfora (LC(Cr)), (LC(Cr,P)) pokazali su srednje brzine rekristalizacije, dok je intersticijski-slobodan čelik (IF) imao najmanju brzinu. Dodavanje Cr i Cr/P povećalo je frakciju -vlaknastog materijala u žarenim teksturama u usporedbi s onom koju susrećemo u ELC čeliku; taj efekt je posebno izražen u 50 %-postotnoj rekristalizaciji. Nakon završetka rekristalizacije, teksture čelika su obilježene dominacijom -vlaknastog tkiva u IF-čeliku, dok je u tri LC čelika RD-vlakno bilo glavno

Strengthening mechanisms in thermomechanically processed NbTi-microalloyed steel

The effect of deformation temperature on microstructure and mechanical properties was investigated for thermomechanically processed NbTi-microalloyed steel with ferrite-pearlite microstructure. With a decrease in the finish deformation temperature at 1348 K to 1098 K (1075 °C to 825 °C) temperature range, the ambient temperature yield stress did not vary significantly, work hardening rate decreased, ultimate tensile strength decreased, and elongation to failure increased. These variations in mechanical properties were correlated to the variations in microstructural parameters (such as ferrite grain size, solid solution concentrations, precipitate number density and dislocation density). Calculations based on the measured microstructural parameters suggested the grain refinement, solid solution strengthening, precipitation strengthening, and work hardening contributed up to 32 pct, up to 48 pct, up to 25 pct, and less than 3 pct to the yield stress, respectively. With a decrease in the finish deformation temperature, both the grain size strengthening and solid solution strengthening increased, the precipitation strengthening decreased, and the work hardening contribution did not vary significantly

Effect of deformation schedule on the microstructure and mechanical properties of a thermomechanically processed C-Mn-Si transformation-induced plasticity steel

Thermomechanical processing simulations were performed using a hot-torsion machine, in order to develop a comprehensive understanding of the effect of severe deformation in the recrystallized and nonrecrystallized austenite regions on the microstructural evolution and mechanical properties of the 0.2 wt pct C-1.55 wt pct Mn-1.5 wt pct Si transformation-induced plasticity (TRIP) steel. The deformation schedule affected all constituents (polygonal ferrite, bainite in different morphologies, retained austenite, and martensite) of the multiphased TRIP steel microstructure. The complex relationships between the volume fraction of the retained austenite, the morphology and distribution of all phases present in the microstructure, and the mechanical properties of TRIP steel were revealed. The bainite morphology had a more pronounced effect on the mechanical behavior than the refinement of the microstructure. The improvement of the mechanical properties of TRIP steel was achieved by variation of the volume fraction of the retained austenite rather than the overall refinement of the microstructure. <br /