Rapid method for determining nitrogen in tantalum and niobium alloys

Adaptation of commercial instrument which measures nitrogen and oxygen in steel gave results in less than four minutes. Sample is heated in helium atmosphere in single-use graphite crucible. Platinum flux facilitates melting of sample. Released gases are separated chromatographically and measured in thermal-conductivity cell

Procedure for rapid determination of nickel, cobalt, and chromium in airborne particulate samples

A rapid, selective procedure for the determination of 1 to 20 micrograms of nickel, chromium, and cobalt in airborne particulates is described. The method utilizes the combined techniques of low temperature ashing and atomic absorption spectroscopy. The airborne particulates are collected on analytical filter paper. The filter papers are ashed, and the residues are dissolved in hydrochloric acid. Nickel, chromium, and cobalt are determined directly with good precision and accuracy by means of atomic absorption. The effects of flame type, burner height, slit width, and lamp current on the atomic absorption measurements are reported

Comparison of inert-gas-fusion and modified Kjeldahl techniques for determination of nitrogen in niobium alloys

This report compares results obtained for the determination of nitrogen in a selected group of niobium-base alloys by the inert-gas-fusion and the Kjeldahl procedures. In the inert-gas-fusion procedure the sample is heated to approximately 2700 C in a helium atmosphere in a single-use graphite crucible. A platinum flux is used to facilitate melting of the sample. The Kjeldahl method consisted of a rapid decomposition with a mixture of hydrofluoric acid, phosphoric acid, and potassium chromate; distillation in the presence of sodium hydroxide; and highly sensitive spectrophotometry with nitroprusside-catalyzed indophenol. In the 30- to 80-ppm range, the relative standard deviation was 5 to 7 percent for the inert-gas-fusion procedure and 2 to 8 percent for the Kjeldahl procedure. The agreement of the nitrogen results obtained by the two techniques is considered satisfactory

Electrostatic forming and testing of polymer films on a 16-foot diameter test fixture

The large space systems technology program investigated different forms of large, lightweight, deployable structures which could be carried on the Space Shuttle. Different forms and concepts of antennas as a type of large space system were investigated. The electrostatically controlled membrane reflector made of metallized material concept was chosen. The concept is a good candidate for creating an antenna with high surface quality and has the ability to be packaged and deployed from the Shuttle with a significant reduction in weight compared to other antenna types

COMBINING TASTE PANELS WITH FOCUS GROUPS TO ELICIT CONSUMER PREFERENCES TOWARD A NEW SHRIMP PRODUCT

Consumer/Household Economics,

A Flattened Protostellar Envelope in Absorption around L1157

Deep Spitzer IRAC images of L1157 reveal many of the details of the outflow and the circumstellar environment of this Class 0 protostar. In IRAC band 4, 8 microns, there is a flattened structure seen in absorption against the background emission. The structure is perpendicular to the outflow and is extended to a diameter of 2 arcminutes. This structure is the first clear detection of a flattened circumstellar envelope or pseudo-disk around a Class 0 protostar. Such a flattened morphology is an expected outcome for many collapse theories that include magnetic fields or rotation. We construct an extinction model for a power-law density profile, but we do not constrain the density power-law index.Comment: ApJL accepte

Dynamical instabilities of Bose-Einstein condensates at the band-edge in one-dimensional optical lattices

We report on experiments that demonstrate dynamical instability in a Bose-Einstein condensate at the band-edge of a one-dimensional optical lattice. The instability manifests as rapid depletion of the condensate and conversion to a thermal cloud. We consider the collisional processes that can occur in such a system, and perform numerical modeling of the experiments using both a mean-field and beyond mean-field approach. We compare our numerical results to the experimental data, and find that the Gross-Pitaevskii equation is not able to describe this experiment. Our beyond mean-field approach, known as the truncated Wigner method, allows us to make quantitative predictions for the processes of parametric growth and thermalization that are observed in the laboratory, and we find good agreement with the experimental results.Comment: v2: Added several reference

Exact Solutions of a (2+1)-Dimensional Nonlinear Klein-Gordon Equation

The purpose of this paper is to present a class of particular solutions of a C(2,1) conformally invariant nonlinear Klein-Gordon equation by symmetry reduction. Using the subgroups of similitude group reduced ordinary differential equations of second order and their solutions by a singularity analysis are classified. In particular, it has been shown that whenever they have the Painlev\'e property, they can be transformed to standard forms by Moebius transformations of dependent variable and arbitrary smooth transformations of independent variable whose solutions, depending on the values of parameters, are expressible in terms of either elementary functions or Jacobi elliptic functions.Comment: 16 pages, no figures, revised versio

Determining the influence and effects of manufacturing variables on sulfur dioxide cells

A survey of the Li/SO2 manufacturing community was conducted to determine where variability exists in processing. The upper and lower limits of these processing variables might, by themselves or by interacting with other variables, influence safety, performance, and reliability. A number of important variables were identified and a comprehensive design experiment is being proposed to make the proper determinations

Role of material properties and mesostructure on dynamic deformation and shear instability in Al-W granular composites

Dynamic experiments with Al-W granular/porous composites revealed qualitatively different behavior with respect to shear localization depending on bonding between Al particles. Two-dimensional numerical modeling was used to explore the mesomechanics of the large strain dynamic deformation in Al-W granular/porous composites and explain the experimentally observed differences in shear localization between composites with various mesostructures. Specifically, the bonding between the Al particles, the porosity, the roles of the relative particle sizes of Al and W, the arrangements of the W particles, and the material properties of Al were investigated using numerical calculations. It was demonstrated in simulations that the bonding between the "soft" Al particles facilitated shear localization as seen in the experiments. Numerical calculations and experiments revealed that the mechanism of the shear localization in granular composites is mainly due to the local high strain flow of "soft" Al around the "rigid" W particles causing localized damage accumulation and subsequent growth of the meso/macro shear bands/cracks. The "rigid" W particles were the major geometrical factor determining the initiation and propagation of "kinked" shear bands in the matrix of "soft" Al particles, leaving some areas free of extensive plastic deformation as observed in experiments and numerical calculations.Comment: 10 pages, 14 figures, submitted to Journal of Applied Physic