Synthesize and Characterization of Aluminum- Tungsten Carbide Nanocomposite

This research focuses on developing metal matrix composite reinforced by polymer-derived ceramic fibers. The force-spun AMT nanofibers were heat treated into tungsten carbide and then mixed with aluminum powder using cold pressing and sintering to produce the composites. The basic mechanical properties of this composite are investigated by density measurement, hardness and compression testing. SEM, EDS and XRD were used to test the morphology of tungsten carbide fibers. EDS identified a near-perfect W-C ratio in tungsten carbide fibers 1000 °C. Tungsten Carbide fibers were crushed using ball milling technique. Tungsten carbide nanofibers powder had a variety of particle size. Results show an increase in mechanical properties as fiber wt % increases in the polymer-ceramic composites made

A 19-year-old boy with intra-oral discharging sinus for 28 days

Abstract not available BSMMU J 2022; 15(2): 138-14

Dilaton Dark Energy Model in f(R), f(T) and Horava-Lifshitz Gravities

In this work, we have considered dilaton dark energy model in Weyl-scaled induced gravitational theory in presence of barotropic fluid. It is to be noted that the dilaton field behaves as a quintessence. Here we have discussed the role of dilaton dark energy in modified gravity theories namely, f(R); f(T) and Horava-Lifshitz gravities and analyzed the behaviour of the dilaton field and the corresponding potential in respect to these modified gravity theories instead of Einstein's gravity. In f(R) and f(T) gravities, we have considered some particular forms of f(R) and f(T) and we have shown that the potentials always increase with the dilaton fields. But in Horava-Lifshitz gravity, it has been seen that the potential always decreases as dilation field increases

Determination of titanium in environmental samples followed by its separation with monothioxo β-diketone liquid exchanger

249-250Titanium has been extracted using monothioxo- β-diketone liquid exchanger and amyl alcohol as solvent, and finally estimated spectrophotometrically. The effects of solvents, pH and various ions on the extraction of the analyte have also been investigated. The method has been applied for the estimation of titanium in bauxite, bentonite, red mud and coal fly ash

Pubertal Development in Girls with Beta Thalassaemia and Assessment of the Adequacy of Chelation Therapy: A Quasi-experimental Study

Introduction: Beta thalassaemia is the most prevalent hereditary autosomal disorder, significantly impacting endocrine function during pubertal development. The pathology is rooted in the excessive deposition of iron in vital organs. If left untreated, this condition leads to serious morbidity and mortality. Hypogonadism stands as the most common endocrine complication. Aim: To observe pubertal development in girls with thalassaemia and evaluate the adequacy of chelation therapy in such patients by measuring levels of Follicle Stimulating Hormone (FSH), Luteinising Hormone (LH), oestrogen, and serum ferritin. Materials and Methods: A quasi-experimental study was conducted at the Thalassaemia Clinic at the Department of Obstetrics and Gynaecology, Burdwan Medical College, Purba Bardhaman, West Bengal, India involving 300 diagnosed Beta Thalassaemia Major (BTM) (case) patients aged 13 to 17 years over a period of one and a half years (January 2020 to June 2021). The girls in the study groups were sequentially enrolled from the Outpatient Department of the Thalassaemia Clinic after meeting inclusion and exclusion criteria. Demographic data, anthropometric measurements, and Sexual Maturity Rating (SMR) were recorded. Hormonal assays of serum FSH, LH, oestrogen, and serum ferritin levels were conducted. Thalassaemic girls with serum ferritin levels exceeding 500 ng/mL received chelation therapy. Serum ferritin levels were measured at two-month intervals for up to six months, with reassessment of serum FSH, LH, oestrogen, and ferritin levels at the end of the six-month period. Statistical analysis was conducted using Statistical Package for Social Sciences (SPSS) version 27.0, Microsoft excel spreadsheet, and Epi Info 7. Results: A total of 190 (63.3%) of the thalassaemic girls were aged 13 to 15 years, with a mean Body Mass Index (BMI) of 22.5000±2.6100 kg/m2, and 74 of them (38.94%) experienced menarche in this age group. Out of 300 cases, 269 thalassaemic girls (89.6%) received chelation therapy, and 89 cases (33.09%) reached menarche after chelation therapy. A significant (p<0.0001) increase in mean LH and FSH levels was observed after chelation therapy. The mean ferritin level decreased from 3168.85 ng/mL to 2227.24 ng/mL following chelation therapy. Conclusion: Pubertal development failure is common in beta thalassaemic girls. Intervention in the form of adequate chelation therapy in girls with high serum ferritin levels yielded favourable outcomes, as evident from serum gonadotropin and oestrogen levels

Antibacterial and toxicological evaluation of ß-lactams synthesized by immobilized ß-lactamase-free penicillin amidase produced by <i style="">Alcaligenes</i> sp.

1068-1072Search for anti-ß-lactamase and synthesis of newer penicillin were suggested to overcome resistance to penicillin in chemotherapy. It was found that clavulanic acid, an ant-ß-lactamase was ineffective due to its structural modification by bacteria. Thus, there is a need for the synthesis of newer pencillins. Retro-synthesis was inspired by the success of forward reaction i.e.conversion of penicillin G to 6-aminopenicillanic acid (6-APA) by biological process. In the present study a better enzymatic method of synthesis of newer pencillin by a ß-lactamase-free penicillin amidase produced by Alcaligenes sp. is attempted. Antibacterial and toxicological evaluation of the enzymatically synthesized ß-lactams are reported. Condensation of 6-APA with acyl donor was found to be effective when the reaction is run in dimethyl formamide (DMF 50% v/v) in acetate buffer (25 mM pH 5.0) at 37°C. Periplasm entrapped in calcium alginate exihibited the highest yield (~34%) in synthesis. The minimum inhibitory concentration of the synthetic products against Staphylococcus aureus and Salmonella typhi varied between 20–80 µg/ml. Some of the products exhibited antibacterial activity against enteric pathogens. It was interesting to note that product A was potent like penicillin G. LD50 value of three products (product A, B and C) was more than 12mg/kg. Furthermore, these synthetic ß-lactams did not exihibit any adverse effect on house keeping enzymes viz., serum glutamate oxalacetate-trans-aminase, serum glutamate pyruvate -trans-aminase, acid phosphatase, alkaline phosphatase of the test animals. The hematological profile (RBC and WBC) of the test animals also remained unaffected