The XQC microcalorimeter sounding rocket: a stable LTD platform 30 seconds after rocket motor burnout

The XQC microcalorimeter sounding rocket experiment is designed to provide a stable thermal environment for an LTD detector system within 30 s of the burnout of its second stage rocket motor. The detector system used for this instrument is a 36-pixel microcalorimeter array operated at 60 mK with a single-stage adiabatic demagnetization refrigerator (ADR). The ADR is mounted on a space-pumped liquid helium tank with vapor cooled shields which is vibration isolated from the rocket structure. We present here some of the design and performance details of this mature LTD instrument, which has just completed its third suborbital flight

Observations of the soft X-ray background with the XQC microcalorimeter sounding rocket

On March 28, 1999 the X-ray Quantum Calorimeter (XQC) sounding rocket instrument completed its third flight to observe the soft X-ray background in the 0.02–1.0 keV energy band. The detector system is a 36-pixel ion implanted microcalorimeter array with 0.5×2.0 mm HgTe absorbers that is operated at 60 mK with a single-stage adiabatic demagnetization refrigerator. The detector array, mounting system, thin film filters and dewar infrastructure have all undergone substantial improvements since the last flight. The result is a scientifically successful observation of the diffuse soft X-ray background that reveals several emission lines from highly ionized elements in the interstellar medium. Preliminary results show strong emission from both O VII and O VIII. In this paper, we discuss problems and their solutions for this mature Low-Temperature Detector (LTD) instrument and recent astrophysical results

Fabrication process responsible for fundamentally improving Silicon X-ray microcalorimeter arrays

We have developed an improved microcalorimeter array that will be used on the AstroE-2 satellite mission. The 6×6 array consists of a grid of 36 suspended pixels. Each 1.5μm thick pixel has an ion-implanted thermometer, four thermal links (support beams), and four X-ray absorber support tabs. Improvements in Silicon micro-machining capabilities and the availability of custom Silicon-on-Insulator (SOI) wafers has enabled us to precisely control pixel geometry, lead widths, and develop a more compact array. Knowing the silicon thickness, we can calculate a precise implant dose for the thermometer. Using a high-temperature anneal, we can uniformly diffuse the implant throughout the depth of the top layer of the SOI wafer. Defining the length, width, and thickness of the support beams, we can control the thermal conductance of the pixel. Advancements in polymer-photo resists have enabled us to develop a new absorber support tab attachment scheme resulting in more controlled heat dissipation from the absorber to the thermometer on the pixel. An overview of fabrication improvements focusing on these topics will be discussed

Cosmic ray effects in microcalorimeter arrays

We have identified signals resulting from cosmic rays and environmental gamma rays depositing energy in the pixels and in the silicon frame of the Astro-E2/X-Ray Spectrometer microcalorimeter array. Coincidences between pixels and between the array and an anti-coincidence detector determined the nature of the events. Pulse shapes and amplitudes from the cosmic ray events helped refine the thermal model of the array chip. We discuss how future arrays can be optimized either for the greatest background rejection or for the highest source count rates

Large area bismuth absorbers for X-ray microcalorimeters

Two challenges facing the use of large area (2mm×2mm) bismuth absorbers for microcalorimetry are uncertainties in the heat capacity of bismuth and the effects of lateral heat conduction and position dependence due to the absorber's large size. We have measured the heat capacity of three Bi samples to be 0.3−0.6JK−1m−3 at 100mK. These absorbers also exhibit response variations as phonons created by an X-ray event at an absorber edge will take longer to propagate to the thermometer attachment point than those at the absorber center. This effect may degrade the detector's energy resolution if the propagation time is not very short compared to the thermometer time constant. We show that the response of the largest absorber varies by ∼4% across its area

Laboratory Astrophysics Using a Spare XRS Microcalorimeter

The XRS instrument on Astro-E is a fully self-contained microcalorimeter x-ray instrument capable of acquiring optimally filtering, and characterizing events for 32 independent pixels. With the launch of the Astro-E spacecraft, a full flight spare detector system has been integrated into a laboratory cryostat for use on the electron beam ion trap (EBIT) at Lawrence Livermore National Laboratory. The detector system contains a microcalorimeter array with 32 instrumented pixels heat sunk to 60 mK using an adiabatic demagnetization refrio,erator. The instrument has a composite resolution of 8eV at 1 keV and 12eV at 6 keV with a minimum of 95% quantum efficiency. This will allow high spectral resolution, broadband observations of collisionally excited plasmas which are produced in the EBIT experiment. Unique to our instrument are exceptionally well characterized 1000 Angstrom thick aluminum on polyimide infrared blocking filters. The detailed transmission function including the edc,e fine structure of these filters has been measured in our laboratory using an erect field grating spectrometer. This will allow the instrument to perform the first broadband absolute flux measurements with the EBIT instrument. The instrument performance as well as the results of preliminary measurements will be discussed. Work performed under the auspices of the U.S. D.o.E. by Lawrence Livermore National Laboratory under contract W-7405-ENG-48 and was supported by the NASA High Energy Astrophysics Supporting Research and Technology Program

High-resolution calorimetry: limitations of doped semiconductor thermometers

Small thermal calorimeters operating at cryogenic temperatures have achieved an energy resolution for single X-ray photons that is a factor of 20 better than the theoretical limit for a silicon ionization detector. To determine the potential for further improvements and decide on likely routes for achieving them, we discuss detector design optimization, first for an ideal calorimeter, and then for the case where components exhibit non-ideal behavior. Two serious non-ideal properties of doped semiconductor thermometers are electron–phonon decoupling and excess noise. These have been characterized over a range of sensitivity and operating temperature, and their effects on design optimization and ultimate performance can be evaluated

Design of the second generation XRS detector

Microcalorimeter performance is limited by non-ideal effects that were not included in the standard theory of bolometers and microcalorimeters developed 20 years ago by Mather (Appl. Opt. 21 (1982) 1125). These include the hot-electron effect, absorber decoupling, thermometer non-ohmic behavior, and all related extra noise sources. Models that include these effects have been developed and can be used to optimize the design of microcalorimeters for best performance. The design of the array for the XRS detector on the Astro-E2 satellite was completely optimized based on the required performance and on the characteristics of the materials used. The characteristic heat capacity and thermal conductivity of all the detector components have been measured and the values have been used as input to the models to design the detector geometry for best performance. Mechanical modeling has also been carried out in parallel to ensure the mechanical integrity of the microcalorimeter. We report here the analysis involved in the optimization of the detectors, and the comparison between modeled and measured performance