Teachers\u27 Perceptions of the Leadership to Tk Pagaran Tapah District Darussalam Rokan Hulu

Every organization, including school certainly has a vision and mission. Inachieving the vision and mission have to be supported by the ability of a leaderwho not only lead, but also should have the competence and in accordance withhis position as a leader. This is consistent with the fact that leaders who succeedare those who have the ability and drive themselves to the objectives of theinstitution he leads. Phenomenon which is discovered in kindergarten in PagaranTapah Darussalam Rokan Hulu such as(1) the presence of some principals who donot want to work on improving the ability of educational personnel in improvingteacher performance, when there are seminars held outside the school, (2) themost principals do not have a good ability in cooperating with the teacher, (3) theprincipals who are less able to manage the facilities and infrastructure of existingschools, (4) the principal who did not want to attend a meeting at school andoutside school, and asked his representative to attend the meeting. The purpose ofthis study is to investigate teachers\u27 perceptions of the leadership of TK. The studywas descriptive, which used quantitative as the technique of collecting file.Collection used questionnaire approach. The number of samples in this studywere33teachers. Based on the results of data processing, obtained a description ofthe leadership of the head teacher\u27s perception TK in Pagaran Tapah DarussalamRokan Hulu in terms of indicators(1) leadership oriented to the duties of 49,62%,(2) leadership oriented to the relationship between humans by 58,71%. Thus, itcan be concluded that the perception of the leadership of the head of thekindergarten teachers are pretty good

Validasi Metode Analisis Multiresidu Pestisida Organoklor dalam Salak Menggunakan Kromatografi Gas-Detektor Penangkap Elektron

Validation of methods is a key step in the accreditation process of the method. Validation of organoklor pesticide residues method in snakefruit based on the method recommended by FAO-WHO, conducted in LPPT-UGM reported in this study. Snake fruit was homogenized, extracted using toluene/2-propanol (2:1), cleaned up using activated carbon and Celite 545, followed by analysis using gas chromatography-electron capture detector. Validation covered specificity and selectivity, limits of detection and quantification, linear range, precision and accuracy. Validation results showed good specificity and selectivity shown by the inter-peak chromatogram resolution greater than 1.5. Limits of detection and quantification for heptaklor, endosulfan, dieldrin and p, p-DDT were 0.002 and 0.006, 0.5 and 1.7; 0.0006 and 0.002, as well as 0.014 and 0.047 ppm respectively. The linear range for heptaklor, endosulfan, dieldrin, and p,p-DDT were 0.0017 to 2 ppm, 0.165 to 2 ppm, 0.023 to 2 ppm and 0.229 to 2 ppm, respectively. Precision methods meet the acceptance of Horwitz RSD value less than 12.78% at a concentration of 0.3 ppm. Accuracy is indicated by recovery, for each pesticide in the range of 80-110% acceptance at a concentration of 0.1 ppm. Analysis of organochlorine pesticides in three commercial snakefruit samples showed no pesticide residues at concentrations higher than the detection limit.ASBTRAKValidasi metode merupakan tahap kunci dalam proses akreditasi suatu metode. Validasi metode uji residu pestisida organoklor dalam salak berdasarkan metode yang direkomendasikan FAO-WHO, di LPPT-UGM dilaporkan pada penelitian ini. Buah salak dihomogenisasi, diekstraksi menggunakan toluen/2-propanol (2:1), clean up menggunakan karbon aktif dan Celite 545, dilanjutkan analisis menggunakan kromatografi gas-detektor penangkap elektron. Validasi mencakup spesifisitas dan selektivitas, batas deteksi dan kuantifikasi, range linier, presisi serta akurasi. Hasil validasi menunjukkan spesifisitas dan selektivitas yang baik ditunjukkan dengan resolusi antar puncak kromatogram lebih besar dari 1,5. Batas deteksi dan batas kuantifikasi untuk heptaklor, endosulfan, dieldrin dan p,p-DDT secara berturut-turut adalah 0,002 dan 0,006; 0,5 dan 1,7; 0,0006 dan 0,002; serta 0,014 dan 0,047 ppm. Range linier untuk heptaklor adalah 0,0017-2 ppm, endosulfan 0,165-2 ppm, dieldrin 0,023-2 ppm dan p,p-DDT 0,229-2 ppm. Presisi metode memenuhi batas keberterimaan Horwitz dengan nilai RSD lebih kecil dari 12,78% pada konsentrasi 0,3 ppm. Akurasi ditunjukkan dengan recovery, untuk tiap pestisida masuk dalam rentang keberterimaan 80-110% pada konsentrasi 0,1 ppm. Analisis pestisida organoklorin pada 3 sampel salak komersial menunjukkan tidak adanya residu pestisida dengan konsentrasi lebih tinggi dari batas deteksi