258 research outputs found

    Evaluation of Kidney Transplant Candidates: An Update in 2012

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    Person Identification Using Multimodal Biometrics under Different Challenges

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    The main aims of this chapter are to show the importance and role of human identification and recognition in the field of human-robot interaction, discuss the methods of person identification systems, namely traditional and biometrics systems, and compare the most commonly used biometric traits that are used in recognition systems such as face, ear, palmprint, iris, and speech. Then, by showing and comparing the requirements, advantages, disadvantages, recognition algorithms, challenges, and experimental results for each trait, the most suitable and efficient biometric trait for human-robot interaction will be discussed. The cases of human-robot interaction that require to use the unimodal biometric system and why the multimodal biometric system is also required will be discussed. Finally, two fusion methods for the multimodal biometric system will be presented and compared

    Optimum Conditions for Oleuropein Extraction from Olive Leaves

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    In this study the effect of extraction solvent (type, composition, pH, and temperature), and the extraction method (maceration and soxhlet) on the amount of oleuropein extracted from olive leaves obtained from West Bank /Palestine was investigated. It was found that pure solvents (100% water, 100% methanol, and 100% ethanol) are not good solvents for oleuropein extraction, while mixtures of the solvents (methanol/water and ethanol/water) gave higher oleuropein content. It was found that 80% ethanol give the highest oleuropein content followed by 20% acetonitrile. Temperature of extraction was found to have a significant effect on the oleuropein content where higher temperature gave higher oleuropein content. It was found also that the amount of oleuropein extracted decreases with increase in pH where highest amount was obtained at pH 3. Soxhlet extraction was found to give higher oleuropein content compared to maceration method

    Effect of Olive Leaves Drying on the Content of Oleuropein

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    Oleuropein content in olive leaves dried at ambient temperature, and at elevated temperature (50ËšC) from Palestinian olive trees collected from West Bank in the middle of November was determined by HPLC and compared to naturally dry olive leaves (collected dry from the tree). Results showed that higher concentration was obtained from olive leaves dried at room temperature (10.0 mg per gram of dry olive leaves), compared to those dried at 50ËšC (1.7 mg/g), and those that collected dry from the tree (2.5 mg/g). Oleuropein content of dried olive leaves was compared with leaves that chopped and extracted fresh, and results show that fresh leaves showed the lowest oleuropein content (<0.1 mg/g) denoting that drying of leaves is required for high oleuropein recovery

    Development and Validation of a Reversed-Phase HPLC Method for Determination of Elaidic Acid in Oils and Fats

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    A simple, precise, accurate, and selective method with low limit of quantitation (LOQ) was developed and validated for analysis of elaidic acid which is the predominant trans fatty acids in partially hydrogenated vegetable oils. Separation was achieved on a reversed-phase C18 column, using mobile phase consisting of acetonitrile/water (80:20, v/v) containing 0.1% acetic acid, and using UV detection at 205 nm. This method was validated according to the requirements for new methods, which include accuracy, precision, selectivity, robustness, limit of detection (LOD), LOQ, linearity and range. The current method demonstrates good linearity over the range of 3-1000 mg L-1 of elaidic acid with r2 greater than 0.999. The recovery of elaidic acid in oils and fats ranges from 94.5 to 98.7%. The method is selective where elaidic acid is good separated from oleic acid and other components of fats and oils with good resolution. The method is also precise where the RSD of the peak areas of replicate injections of elaidic acid solution is less than 1%. The degree of reproducibility of the results obtained as a result of small deliberate variations in the method parameters and by changing analytical operators has proven that the method is robust and rugged

    Development and Validation of a Reversed-Phase HPLC Method for Determination of Elaidic Acid in Oils and Fats

    Get PDF
    A simple, precise, accurate, and selective method with low limit of quantitation (LOQ) was developed and validated for analysis of elaidic acid which is the predominant trans fatty acids in partially hydrogenated vegetable oils. Separation was achieved on a reversed-phase C18 column, using mobile phase consisting of acetonitrile/water (80:20, v/v) containing 0.1% acetic acid, and using UV detection at 205 nm. This method was validated according to the requirements for new methods, which include accuracy, precision, selectivity, robustness, limit of detection (LOD), LOQ, linearity and range. The current method demonstrates good linearity over the range of 3-1000 mg L-1 of elaidic acid with r2 greater than 0.999. The recovery of elaidic acid in oils and fats ranges from 94.5 to 98.7%. The method is selective where elaidic acid is good separated from oleic acid and other components of fats and oils with good resolution. The method is also precise where the RSD of the peak areas of replicate injections of elaidic acid solution is less than 1%. The degree of reproducibility of the results obtained as a result of small deliberate variations in the method parameters and by changing analytical operators has proven that the method is robust and rugged

    Optimum Conditions for Oleuropein Extraction from Olive Leaves

    Get PDF
    In this study the effect of extraction solvent (type, composition, pH, and temperature), and the extraction method (maceration and soxhlet) on the amount of oleuropein extracted from olive leaves obtained from West Bank /Palestine was investigated. It was found that pure solvents (100% water, 100% methanol, and 100% ethanol) are not good solvents for oleuropein extraction, while mixtures of the solvents (methanol/water and ethanol/water) gave higher oleuropein content. It was found that 80% ethanol give the highest oleuropein content followed by 20% acetonitrile. Temperature of extraction was found to have a significant effect on the oleuropein content where higher temperature gave higher oleuropein content. It was found also that the amount of oleuropein extracted decreases with increase in pH where highest amount was obtained at pH 3. Soxhlet extraction was found to give higher oleuropein content compared to maceration method

    Momentum images of continuum electrons from the molecular ionization and dissociation of H2 induced by slow He2+ ions

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    Cold target recoil ion momentum spectroscopy (COLTRIM) has been employed to image the momentum distributions of continuum electrons liberated in the impact of slow He2+ on He and H2. The distributions were measured for fully determined motion of the nuclei that is as a function of the impact parameter and in a well de ned scattering plane The single ionization (SI) of H2 leading to H2+ recoil ions in nondissociative states (He2+ + H+ -> He2+ + H+ + e-) and the transfer ionization (TI) of H2 leading to H2 dissociation into two free protons (He2+ H2 -> He+ + H+ + H+ + e-) were investigated. Similar measurements have been carried out for He target, the corresponding atomic two electron system, i.e. the single ionization (SI) (He2+ + He -> He+ + He2+ e- and the transfer ionization (TI) (He2+ + He -> He+ + He2+ + e-). These measurements have been exploited to understand the results obtained for H target. In comparing the continuum electron momentum distributions for H2 with that for He, a high degree of similarity is observed. In the case of transfer ionization of H2, the electron momentum distributions generated for parallel and perpendicular molecular orientations revealed no orientation dependence. The in scattering plane electron momentum distributions for the transfer ionization of H2 by He2+ and for the transfer ionization of He by He2e showed that the salient feature of these distributions for both collisions systems consists in the appearance of two groups of electrons with difeerent structures. In addition to the group of the saddle electrons forming two jets separated by a valley along the projectile axis we nd a new group of electrons moving with a velocity higher than the projectile velocity These new fast forward electrons result from a narrow range of impact parameters and appear as image saddle in the projectile frame. In contrast to the transfer ionization of He, the fast forward electrons group disappears in the in scattering plane electron momentum distribution generated for the single ionization of He. Instead of this group another new group of electrons appear These electrons exhibit an amount of backscattering These backward elec trons appear as image saddle in the target frame The structures that the saddle electrons show are owing to the quasi molecular nature of the collision process For the TI of H2, the TI of He and the SI of He, a pi-orbital shape of the electron momentum distribution is observed This indicates the importance of the rotational coupling 2-p-theta -> 2p-pi in the initial promotion of the ground state followed by further promotions to the continuum The backward electrons as well as the fast forward electrons are not discussed in the theoretical literature at all. However, a number of obvious indications of the existence of the backward and fast forward electrons could be seen in the experimental works of Abdallah et al. as well as in the theoretical calculations of Sidky et al One might speculate that electrons which are promoted on the saddle for some time during the collision could finally swing around the He+ ion in the way out of the collision, i.e. either around the projectile in the forward direction as in the TI case forming the fast forward electrons or around the recoil ion in the backward direction as in the SI case forming the backward electrons. This might be a result of the strong gradient, and hence the large acceleration of the screened He+ potential
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